Na4 O18 P6 Pb Averbuch-Pouchot M, Durif A Zeitschrift fur Kristallographie 164 (1983) 307-313 Crystal structure of lead-tetrasodium trimetaphosphate: PbNa4(P3O9)2, Crystal data for Ba Na4 (P3 O9)2 _cod_database_code 1007084 _database_code_amcsd 0010857 CELL PARAMETERS: 7.2680 8.1510 7.8510 121.520 102.060 73.000 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 378.259 Density (g/cm3): 3.393 MAX. ABS. INTENSITY / VOLUME**2: 9.030138359 RIR: 0.867 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.77 44.07 6.9340 1 0 0 2 13.06 29.99 6.7786 0 1 0 2 13.24 25.12 6.6848 0 -1 1 2 13.26 56.95 6.6768 0 0 1 2 15.57 21.54 5.6928 -1 -1 1 2 16.15 13.38 5.4871 1 1 0 2 19.08 9.33 4.6523 1 0 1 2 20.23 60.79 4.3891 -1 1 0 2 20.93 38.54 4.2449 1 -1 1 2 22.67 3.37 3.9229 -1 -2 1 2 23.17 7.61 3.8389 0 -1 2 2 24.11 90.35 3.6920 -1 -1 2 2 25.26 13.28 3.5260 1 1 1 2 25.34 29.04 3.5151 -2 -1 1 2 26.08 23.94 3.4165 -1 -2 2 2 26.17 12.35 3.4048 2 1 0 2 26.29 29.18 3.3893 0 2 0 2 26.62 1.05 3.3491 1 2 0 2 26.70 11.14 3.3384 0 0 2 2 27.22 32.80 3.2759 -1 1 1 2 28.17 81.50 3.1673 -2 0 1 2 28.87 1.81 3.0922 -1 0 2 2 29.03 86.02 3.0757 -2 -2 1 2 29.40 65.05 3.0385 1 -2 1 2 29.84 4.69 2.9938 2 0 1 2 30.51 100.00 2.9302 1 0 2 2 31.04 5.65 2.8811 -2 -1 2 2 31.43 1.74 2.8464 -2 -2 2 2 31.46 9.74 2.8438 -2 1 0 2 31.83 3.63 2.8111 -1 2 0 2 32.30 15.11 2.7712 2 -1 1 2 32.64 32.68 2.7435 2 2 0 2 32.90 28.61 2.7221 1 -2 2 2 33.09 9.53 2.7071 2 1 1 2 33.85 37.47 2.6478 -1 -3 1 2 34.89 46.48 2.5715 -1 -2 3 2 35.08 21.44 2.5578 0 -3 1 2 35.11 39.31 2.5556 0 2 1 2 35.30 13.84 2.5425 0 -3 2 2 35.35 13.18 2.5390 0 1 2 2 36.04 4.19 2.4920 -2 0 2 2 37.06 2.09 2.4260 -2 -3 2 2 37.35 3.21 2.4076 1 1 2 2 37.52 2.03 2.3972 -2 -3 1 2 38.11 13.98 2.3615 -1 1 2 2 38.28 17.38 2.3511 3 1 0 2 38.36 6.73 2.3464 2 -1 2 2 38.71 13.74 2.3261 2 0 2 2 38.76 20.20 2.3234 -1 -3 3 2 38.84 9.09 2.3186 -2 -2 3 2 38.97 4.44 2.3113 3 0 0 2 39.06 8.78 2.3061 -3 -2 1 2 39.12 8.32 2.3025 1 3 0 2 39.23 8.32 2.2963 -1 2 1 2 39.53 5.40 2.2799 2 -2 1 2 40.05 3.76 2.2515 1 -1 3 2 40.41 10.51 2.2321 -3 0 1 2 40.48 6.60 2.2283 0 -3 3 2 40.53 20.60 2.2256 0 0 3 2 40.63 7.73 2.2207 -3 -2 2 2 40.82 7.03 2.2105 1 -3 1 2 41.13 5.20 2.1946 -2 2 0 2 41.29 7.24 2.1865 -3 -1 2 2 41.32 1.22 2.1849 1 -3 2 2 41.76 8.15 2.1629 -1 0 3 2 42.21 7.71 2.1410 3 2 0 2 42.25 6.95 2.1391 3 0 1 2 42.60 8.22 2.1224 2 -2 2 2 42.70 5.42 2.1177 2 3 0 2 43.55 1.13 2.0783 2 1 2 2 43.56 8.01 2.0779 1 0 3 2 43.80 20.85 2.0669 3 1 1 2 44.09 11.26 2.0541 -3 1 0 2 44.37 2.60 2.0416 -3 -3 2 2 44.46 26.05 2.0376 -1 -4 2 2 44.84 3.84 2.0215 -1 3 0 2 45.01 6.85 2.0140 3 -1 1 2 45.06 3.39 2.0121 -3 -3 1 2 46.22 2.82 1.9643 1 -3 3 2 46.29 3.17 1.9614 -2 -4 2 2 46.45 2.54 1.9550 -1 -2 4 2 46.52 3.06 1.9522 -3 -2 3 2 46.56 4.84 1.9507 -1 -4 3 2 46.61 4.38 1.9485 0 -4 2 2 46.65 3.16 1.9470 -1 -4 1 2 46.67 1.19 1.9461 0 2 2 2 46.97 10.34 1.9344 -2 0 3 2 47.02 3.73 1.9325 -2 2 1 2 47.42 1.75 1.9171 1 2 2 2 47.44 3.49 1.9163 -3 1 1 2 47.94 2.26 1.8976 -3 -3 3 2 47.96 5.67 1.8969 2 -1 3 2 48.05 7.29 1.8936 -2 -4 3 2 48.10 8.96 1.8916 1 3 1 2 48.46 5.65 1.8785 0 -4 1 2 48.68 2.33 1.8704 -2 -4 1 2 49.11 10.09 1.8550 -3 -1 3 2 49.33 7.51 1.8475 0 -3 4 2 49.34 9.64 1.8470 3 2 1 2 49.36 6.97 1.8461 0 -1 4 2 49.37 4.66 1.8460 -2 -2 4 2 49.62 1.16 1.8371 -2 -3 4 2 49.64 7.28 1.8366 2 -2 3 2 49.74 3.73 1.8331 -1 2 2 2 50.21 3.17 1.8169 2 0 3 2 50.47 2.74 1.8082 2 -3 2 2 50.87 3.27 1.7951 -1 1 3 2 51.01 4.55 1.7904 -4 -2 1 2 51.43 4.86 1.7767 2 3 1 2 51.46 2.37 1.7757 4 1 0 2 51.54 4.80 1.7732 3 -2 1 2 51.86 3.19 1.7630 2 2 2 2 51.95 2.10 1.7601 1 -2 4 2 52.03 5.59 1.7575 -4 -2 2 2 52.36 1.80 1.7473 1 -4 2 2 52.54 2.37 1.7418 -1 3 1 2 52.60 4.01 1.7399 -3 2 0 2 52.81 1.34 1.7335 4 0 0 2 52.93 1.71 1.7300 -2 -1 4 2 53.01 9.20 1.7274 -2 3 0 2 53.04 3.80 1.7266 1 -1 4 2 53.13 4.01 1.7237 -3 -4 3 2 53.81 3.27 1.7037 1 -4 1 2 54.40 5.77 1.6866 -4 -3 2 2 54.48 1.93 1.6842 -3 1 2 2 54.58 10.06 1.6814 1 -3 4 2 54.82 12.69 1.6746 2 4 0 2 54.94 10.14 1.6712 0 -4 4 2 54.98 3.43 1.6701 2 -3 3 2 55.13 6.70 1.6658 -3 -3 4 2 55.67 5.47 1.6510 -3 -2 4 2 55.69 9.00 1.6505 4 0 1 2 55.75 6.45 1.6489 -1 0 4 2 56.16 3.80 1.6379 -2 2 2 2 56.19 1.97 1.6370 -2 1 3 2 57.71 1.88 1.5973 -4 1 0 2 57.84 1.70 1.5942 -2 -5 2 2 58.15 1.27 1.5863 -3 -4 4 2 58.26 3.47 1.5837 -4 0 2 2 58.38 5.18 1.5808 3 -1 3 2 58.72 1.15 1.5724 4 -1 1 2 59.39 6.14 1.5561 3 2 2 2 59.57 1.86 1.5519 1 3 2 2 59.60 2.29 1.5511 0 -5 2 2 59.62 5.11 1.5508 2 -2 4 2 59.67 1.30 1.5496 4 3 0 2 59.71 1.96 1.5487 -1 -2 5 2 59.79 4.91 1.5469 -4 -1 3 2 59.82 3.59 1.5461 -2 0 4 2 59.85 1.21 1.5454 0 -5 3 2 59.94 2.86 1.5433 0 2 3 2 60.20 1.66 1.5372 3 4 0 2 60.29 8.46 1.5352 -4 1 1 2 60.48 9.88 1.5307 -2 -3 5 2 60.59 1.31 1.5283 1 -4 4 2 60.71 4.85 1.5255 0 -2 5 2 60.80 5.03 1.5235 1 2 3 2 60.93 5.69 1.5204 -2 -5 4 2 61.19 1.96 1.5147 -4 -4 3 2 61.60 3.56 1.5055 -1 -4 5 2 61.81 4.31 1.5010 3 -3 2 2 61.84 4.20 1.5003 1 4 1 2 61.88 2.40 1.4994 -3 -5 2 2 62.07 1.99 1.4952 2 -4 1 2 62.39 5.01 1.4885 -2 -4 5 2 62.64 2.39 1.4830 -4 -4 1 2 62.70 1.53 1.4817 2 3 2 2 62.85 2.22 1.4786 0 -5 1 2 62.89 4.41 1.4778 0 4 1 2 63.00 10.06 1.4754 -1 3 2 2 63.19 4.18 1.4715 4 -1 2 2 63.36 1.39 1.4679 2 -4 3 2 63.50 1.54 1.4651 2 0 4 2 63.60 1.23 1.4630 -3 3 0 2 63.65 1.46 1.4619 0 1 4 2 63.98 2.25 1.4552 2 4 1 2 64.01 2.86 1.4545 0 -4 5 2 64.19 1.94 1.4510 3 1 3 2 64.38 7.07 1.4470 -3 1 3 2 64.41 1.43 1.4465 -3 -5 4 2 64.62 4.55 1.4423 -5 -1 1 2 64.71 2.40 1.4406 -4 -2 4 2 64.97 1.20 1.4355 4 -2 1 2 65.25 1.87 1.4299 1 -5 2 2 65.28 1.98 1.4293 -3 2 2 2 65.41 1.42 1.4267 1 1 4 2 65.55 1.96 1.4240 1 -3 5 2 65.60 1.20 1.4232 -4 -4 4 2 65.69 2.28 1.4213 5 1 0 2 65.71 2.50 1.4211 1 -5 3 2 65.73 1.55 1.4207 -3 -5 1 2 65.99 2.36 1.4156 -4 0 3 2 66.42 1.22 1.4076 -5 -3 2 2 66.68 2.83 1.4027 -2 -1 5 2 67.07 1.50 1.3954 5 2 0 2 67.27 2.81 1.3918 -3 -2 5 2 67.41 1.97 1.3893 1 5 0 2 67.55 1.13 1.3868 5 0 0 2 67.74 1.90 1.3833 -2 2 3 2 68.10 2.71 1.3768 -5 0 1 2 68.39 2.12 1.3718 4 4 0 2 68.82 6.29 1.3641 3 3 2 2 68.84 2.20 1.3638 -4 -5 2 2 69.00 3.18 1.3611 2 -4 4 2 69.31 2.10 1.3557 0 5 0 2 69.44 2.59 1.3536 4 2 2 2 69.63 1.96 1.3503 -1 -6 3 2 69.77 2.14 1.3479 3 -2 4 2 70.19 1.20 1.3408 2 1 4 2 70.76 1.74 1.3315 4 -1 3 2 70.90 2.79 1.3292 -2 -6 4 2 71.20 3.17 1.3243 -1 -6 2 2 71.21 1.70 1.3241 4 0 3 2 71.22 3.51 1.3239 -2 -6 2 2 71.30 2.67 1.3227 -1 -6 4 2 71.59 4.64 1.3181 5 3 0 2 72.25 1.28 1.3076 -3 -6 3 2 72.40 1.83 1.3054 -5 -1 3 2 72.48 1.80 1.3041 -3 -1 5 2 72.72 3.70 1.3004 -4 -5 1 2 72.94 1.14 1.2970 5 2 1 2 73.03 1.58 1.2956 1 3 3 2 73.08 1.11 1.2948 1 0 5 2 73.33 3.80 1.2910 3 -3 4 2 73.42 1.08 1.2896 4 -2 3 2 73.48 1.06 1.2888 -3 -6 4 2 73.61 1.62 1.2868 5 -1 1 2 73.63 1.53 1.2865 2 -5 2 2 73.68 1.50 1.2858 -2 -4 6 2 74.22 2.00 1.2778 -3 -6 2 2 74.66 2.02 1.2713 0 -6 4 2 74.76 4.19 1.2698 4 1 3 2 75.53 1.16 1.2588 -2 -6 5 2 75.57 2.14 1.2583 -5 -4 4 2 75.74 2.33 1.2559 -1 3 3 2 76.05 1.85 1.2515 -5 -2 4 2 76.29 2.45 1.2482 1 -5 5 2 76.57 2.57 1.2443 -4 -5 5 2 76.69 1.99 1.2427 -3 4 0 2 76.70 2.18 1.2424 -4 2 2 2 77.09 2.34 1.2372 -1 -5 6 2 77.85 1.37 1.2269 5 -1 2 2 77.93 1.41 1.2259 -4 -6 3 2 78.51 2.54 1.2183 2 0 5 2 78.60 1.35 1.2172 0 -6 1 2 78.77 2.23 1.2150 1 -3 6 2 78.83 2.85 1.2141 5 3 1 2 79.27 1.54 1.2086 -6 -2 1 2 79.62 1.29 1.2041 0 -6 5 2 79.75 1.60 1.2024 0 1 5 2 79.93 1.85 1.2002 5 -2 1 2 80.14 1.09 1.1976 -6 -1 1 2 80.83 1.51 1.1891 -5 -1 4 2 81.05 1.67 1.1864 -3 -2 6 2 81.40 1.20 1.1822 -6 -3 1 2 81.49 1.21 1.1811 -4 3 1 2 81.52 1.81 1.1807 -2 2 4 2 82.62 1.52 1.1678 3 -1 5 2 83.00 1.68 1.1635 -4 -6 5 2 83.36 1.68 1.1593 -4 -4 6 2 83.52 1.21 1.1575 1 -1 6 2 83.68 1.94 1.1557 6 0 0 2 83.92 1.59 1.1531 -6 -4 2 2 84.10 1.99 1.1510 1 -6 1 2 84.36 1.81 1.1482 -2 4 2 2 84.45 1.30 1.1471 -4 -3 6 2 84.72 1.38 1.1442 -2 1 5 2 84.85 1.80 1.1427 2 -5 5 2 85.21 1.84 1.1388 -3 -6 6 2 85.24 2.75 1.1386 -5 -5 5 2 86.06 1.35 1.1298 0 6 0 2 86.21 2.44 1.1282 2 -3 6 2 86.76 3.42 1.1224 3 -5 1 2 87.33 1.80 1.1165 -6 -3 4 2 87.35 1.38 1.1164 3 6 0 2 87.38 2.65 1.1161 -6 0 2 2 87.62 1.37 1.1137 4 -4 3 2 87.70 3.70 1.1128 0 0 6 2 87.90 1.49 1.1108 -1 0 6 2 88.32 1.19 1.1066 0 3 4 2 88.51 1.10 1.1047 4 4 2 2 89.09 2.73 1.0990 5 -3 1 2 89.21 1.41 1.0978 3 -5 4 2 89.45 1.19 1.0955 4 5 1 2 89.51 1.58 1.0949 -4 0 5 2 89.75 2.24 1.0926 -4 3 2 2 89.78 1.99 1.0923 2 4 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.