Bosoite Gerke H, Gies H Zeitschrift fur Kristallographie 166 (1984) 11-22 Studies on clathrasils. IV. Crystal structure of dodecasil 1H, a synthetic clathrate compound of silica Locality: synthetic _database_code_amcsd 0020684 CELL PARAMETERS: 13.7830 13.7830 11.1900 90.000 90.000 120.000 SPACE GROUP: P6/mmm X-RAY WAVELENGTH: 1.541838 Cell Volume: 1840.976 Density (g/cm3): 1.842 MAX. ABS. INTENSITY / VOLUME**2: 9.652564083 RIR: 1.706 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.41 55.41 11.9364 1 0 0 6 7.90 13.39 11.1900 0 0 1 2 10.84 31.57 8.1637 1 0 1 12 12.85 34.64 6.8915 1 1 0 6 14.84 25.35 5.9682 2 0 0 6 15.10 60.01 5.8680 1 1 1 12 15.84 22.68 5.5950 0 0 2 2 16.84 100.00 5.2660 2 0 1 12 17.51 36.19 5.0661 1 0 2 12 19.68 9.98 4.5115 2 1 0 12 21.23 5.38 4.1843 2 1 1 24 21.77 2.22 4.0818 2 0 2 12 22.34 5.37 3.9788 3 0 0 6 23.73 25.17 3.7489 3 0 1 12 23.86 4.92 3.7300 0 0 3 2 25.01 4.54 3.5602 1 0 3 12 25.36 48.48 3.5120 2 1 2 24 25.86 14.14 3.4457 2 2 0 6 26.93 27.86 3.3106 3 1 0 12 27.08 19.02 3.2932 2 2 1 12 27.18 21.64 3.2803 1 1 3 12 28.11 1.17 3.1746 3 1 1 24 28.21 11.48 3.1631 2 0 3 12 29.94 1.83 2.9841 4 0 0 6 31.11 3.06 2.8747 2 1 3 24 31.40 4.90 2.8492 3 1 2 24 32.70 1.15 2.7384 3 2 0 12 32.88 2.82 2.7237 1 0 4 12 34.05 1.34 2.6330 4 0 2 12 35.38 2.86 2.5369 4 1 1 24 35.44 4.22 2.5330 2 0 4 12 35.47 1.20 2.5310 2 2 3 12 36.53 9.00 2.4596 3 2 2 24 37.68 5.82 2.3873 5 0 0 6 37.84 1.88 2.3775 2 1 4 24 38.56 2.14 2.3347 5 0 1 12 38.64 1.78 2.3302 4 0 3 12 39.22 3.95 2.2972 3 3 0 6 39.37 6.79 2.2885 3 0 4 12 40.88 3.83 2.2074 3 2 3 24 41.11 1.19 2.1958 5 0 2 12 46.56 1.42 1.9506 3 0 5 12 47.08 3.57 1.9302 4 2 3 24 48.57 2.85 1.8744 6 0 2 12 48.83 1.20 1.8650 0 0 6 2 50.11 1.88 1.8203 6 1 0 12 51.01 1.20 1.7904 4 0 5 12 51.47 1.22 1.7753 3 3 4 12 52.08 1.58 1.7560 4 2 4 24 52.71 2.00 1.7367 4 3 3 24 52.83 1.06 1.7329 3 2 5 24 53.14 1.89 1.7235 2 1 6 24 54.33 1.07 1.6887 3 0 6 12 54.43 4.10 1.6857 5 3 1 24 56.35 1.10 1.6327 5 0 5 12 56.78 1.32 1.6213 6 0 4 12 57.49 1.27 1.6030 3 3 5 12 58.11 2.28 1.5873 6 2 2 24 58.48 2.24 1.5782 5 2 4 24 60.02 1.72 1.5415 3 2 6 24 60.70 1.12 1.5257 6 1 4 24 61.55 1.24 1.5068 2 1 7 24 63.94 2.51 1.4560 5 3 4 24 67.63 2.15 1.3853 8 0 3 12 68.02 2.59 1.3783 5 5 0 6 70.17 1.31 1.3412 5 4 4 24 70.96 2.92 1.3283 5 0 7 12 81.53 2.15 1.1807 8 2 4 24 82.13 1.21 1.1736 5 5 5 12 84.20 1.51 1.1499 6 2 7 24 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.