Bi H18 Na3 O27 P6 Bagieu-Beucher M, Durif A Zeitschrift fur Kristallographie 178 (1987) 239-247 Preparation and crystal structure of bismuth trisodium trimetaphosphate nonahydrate: Bi Na3 (P3 O9)2 * 9 H2 O _cod_database_code 1007264 _database_code_amcsd 0015945 CELL PARAMETERS: 30.8450 30.8450 13.0850 90.000 90.000 120.000 SPACE GROUP: R-3c X-RAY WAVELENGTH: 1.541838 Cell Volume: 10781.362 Density (g/cm3): 2.483 MAX. ABS. INTENSITY / VOLUME**2: 16.74646509 RIR: 2.196 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.93 56.29 8.9042 3 0 0 6 11.07 62.46 7.9935 2 1 1 12 11.48 100.00 7.7112 2 2 0 6 13.74 92.85 6.4470 1 3 1 12 15.08 11.58 5.8755 2 0 2 6 15.97 70.30 5.5498 3 2 1 12 17.25 25.10 5.1408 3 3 0 6 18.09 4.16 4.9040 3 1 2 12 18.84 1.98 4.7098 2 4 1 12 18.99 1.57 4.6735 0 4 2 6 19.85 8.33 4.4726 2 3 2 12 19.94 41.54 4.4521 6 0 0 6 21.34 6.15 4.1633 4 3 1 12 22.99 4.99 3.8689 1 5 2 12 23.07 19.52 3.8556 4 4 0 6 23.43 27.23 3.7964 2 2 3 12 24.30 19.21 3.6635 3 5 1 12 24.98 2.00 3.5643 6 2 1 12 25.17 21.57 3.5382 7 1 0 12 25.51 14.81 3.4923 1 4 3 12 25.51 7.59 3.4923 4 1 3 12 25.76 14.04 3.4581 6 1 2 12 26.81 18.10 3.3259 3 3 3 12 26.94 6.06 3.3090 5 4 1 12 27.05 9.39 3.2963 0 7 2 6 27.47 28.83 3.2470 1 0 4 6 28.18 5.91 3.1665 2 7 1 12 28.69 16.58 3.1120 2 1 4 12 28.95 1.23 3.0845 5 5 0 6 29.24 1.40 3.0539 2 5 3 12 29.24 1.41 3.0539 5 2 3 12 29.47 1.59 3.0310 4 5 2 12 29.86 2.22 2.9925 1 3 4 12 29.95 7.17 2.9834 4 6 1 12 30.52 6.41 2.9291 7 3 1 12 30.61 5.00 2.9203 7 2 2 12 30.96 35.90 2.8888 4 4 3 12 30.99 4.27 2.8858 3 2 4 12 31.72 5.25 2.8209 1 8 2 12 32.08 1.20 2.7898 0 5 4 6 32.32 3.23 2.7700 7 4 0 12 32.70 10.98 2.7382 1 9 1 12 32.70 1.33 2.7382 6 5 1 12 32.79 7.25 2.7310 3 7 2 12 33.15 5.69 2.7028 5 1 4 12 33.64 2.47 2.6645 6 3 3 12 33.75 11.52 2.6558 3 8 1 12 34.18 3.35 2.6234 4 3 4 12 34.77 9.16 2.5804 9 2 1 12 34.85 23.15 2.5743 5 6 2 12 34.85 3.83 2.5743 9 1 2 12 34.91 2.84 2.5704 6 6 0 6 35.19 14.44 2.5506 1 6 4 12 35.40 3.91 2.5354 10 1 0 12 35.43 2.82 2.5333 1 2 5 12 35.65 1.38 2.5184 5 5 3 12 35.84 3.02 2.5055 8 3 2 12 36.17 5.85 2.4836 7 0 4 6 36.25 5.16 2.4784 8 4 1 12 36.41 1.83 2.4676 3 1 5 12 36.65 3.29 2.4520 6 2 4 12 36.81 2.50 2.4419 2 9 2 12 37.10 7.97 2.4233 2 8 3 12 37.10 12.69 2.4233 8 2 3 12 37.36 3.89 2.4067 2 3 5 12 37.75 1.33 2.3829 7 5 2 12 38.14 1.46 2.3595 2 10 1 12 38.27 1.47 2.3519 8 5 0 12 38.50 3.49 2.3383 4 7 3 12 38.53 1.69 2.3367 0 8 4 6 38.76 1.61 2.3234 4 2 5 12 39.51 1.28 2.2808 4 9 1 12 40.11 3.37 2.2481 3 4 5 12 40.48 4.59 2.2286 6 7 2 12 40.52 4.21 2.2260 12 0 0 6 40.77 4.98 2.2132 7 3 4 12 40.96 5.06 2.2032 7 7 0 6 41.18 2.98 2.1920 1 10 3 12 41.35 3.12 2.1835 1 11 2 12 41.40 1.83 2.1808 0 0 6 2 42.04 1.24 2.1490 3 9 3 12 42.04 3.01 2.1490 9 3 3 12 42.21 4.67 2.1410 3 10 2 12 42.26 6.13 2.1387 10 4 0 12 42.49 2.49 2.1273 6 5 4 12 42.49 6.38 2.1273 1 9 4 12 43.11 1.17 2.0985 2 2 6 12 43.34 2.36 2.0879 3 8 4 12 43.47 1.27 2.0816 8 6 2 12 43.55 5.96 2.0784 4 5 5 12 43.82 5.64 2.0660 3 11 1 12 44.16 2.96 2.0507 9 2 4 12 44.35 2.19 2.0426 4 1 6 12 44.71 5.10 2.0270 12 1 2 12 44.98 1.43 2.0154 5 7 4 12 45.45 10.16 1.9957 5 10 1 12 45.96 6.09 1.9746 13 1 0 12 46.25 4.44 1.9631 11 4 1 12 46.31 3.94 1.9604 0 13 2 6 46.36 2.42 1.9585 0 6 6 6 46.36 5.90 1.9585 6 0 6 6 47.34 4.13 1.9203 4 10 3 12 47.34 4.68 1.9203 10 4 3 12 47.36 7.69 1.9194 7 6 4 12 47.56 1.54 1.9120 5 6 5 12 47.56 3.91 1.9120 9 1 5 12 47.81 6.08 1.9024 7 9 1 12 48.20 1.37 1.8881 10 6 1 12 48.30 5.58 1.8842 11 5 0 12 48.33 2.57 1.8833 8 3 5 12 48.90 1.05 1.8626 10 3 4 12 49.09 3.83 1.8558 2 9 5 12 49.40 2.27 1.8448 9 7 2 12 49.72 1.96 1.8339 4 12 1 12 49.78 1.81 1.8317 14 0 2 6 50.03 4.79 1.8231 6 8 4 12 50.22 1.38 1.8168 4 8 5 12 50.34 3.51 1.8125 1 3 7 12 50.83 1.51 1.7962 9 8 1 12 51.08 5.70 1.7880 3 2 7 12 51.14 2.59 1.7861 1 12 4 12 51.49 1.92 1.7749 12 3 3 12 51.57 1.22 1.7723 6 11 1 12 51.85 3.05 1.7633 8 8 3 12 52.18 1.10 1.7530 2 4 7 12 52.36 1.31 1.7475 8 9 2 12 52.60 3.69 1.7400 13 0 4 6 52.94 1.30 1.7297 11 5 3 12 53.32 2.01 1.7183 5 10 4 12 54.03 2.03 1.6973 11 4 4 12 54.44 1.77 1.6855 3 14 1 12 54.53 2.20 1.6827 12 6 0 12 54.68 3.89 1.6787 3 5 7 12 55.03 1.29 1.6688 6 2 7 12 55.24 3.63 1.6629 6 6 6 12 55.78 3.29 1.6482 0 14 4 6 55.83 4.32 1.6466 15 2 1 12 56.07 7.42 1.6403 5 4 7 12 56.29 2.16 1.6342 11 3 5 12 56.36 2.63 1.6326 0 1 8 6 56.96 1.29 1.6167 11 8 0 12 57.15 1.43 1.6118 4 12 4 12 57.26 2.02 1.6089 2 15 2 12 57.26 1.89 1.6089 13 5 2 12 57.66 3.47 1.5987 10 5 5 12 57.81 2.29 1.5949 9 9 3 12 58.11 2.13 1.5873 7 3 7 12 58.17 1.32 1.5860 9 8 4 12 58.34 5.26 1.5818 4 11 5 12 59.28 1.70 1.5588 12 7 2 12 59.32 1.49 1.5578 12 0 6 6 59.32 2.27 1.5578 0 12 6 6 59.45 1.03 1.5547 1 9 7 12 59.95 4.30 1.5431 6 13 2 12 60.12 1.43 1.5391 3 8 7 12 60.77 2.71 1.5240 9 2 7 12 60.93 1.20 1.5204 16 2 2 12 61.05 1.63 1.5178 6 1 8 12 61.13 1.14 1.5159 1 16 3 12 61.70 1.52 1.5034 0 7 8 6 61.79 3.39 1.5015 3 15 3 12 61.79 2.84 1.5015 15 3 3 12 62.29 1.67 1.4905 8 9 5 12 62.29 1.12 1.4905 3 13 5 12 62.59 1.18 1.4840 18 0 0 6 63.05 1.22 1.4745 2 10 7 12 63.79 2.61 1.4591 11 10 1 12 64.69 1.30 1.4409 7 12 4 12 64.85 1.04 1.4378 15 1 5 12 65.31 1.16 1.4287 2 2 9 12 65.32 2.02 1.4285 13 6 4 12 65.48 1.20 1.4254 14 3 5 12 66.37 1.46 1.4085 18 1 2 12 66.94 2.05 1.3979 5 16 1 12 68.18 1.77 1.3755 17 4 1 12 68.23 1.60 1.3745 0 19 2 6 69.87 1.47 1.3462 6 7 8 12 70.07 1.63 1.3429 15 7 2 12 70.56 1.43 1.3348 11 11 3 12 70.98 1.09 1.3279 6 16 2 12 71.23 1.14 1.3238 9 14 1 12 72.64 1.43 1.3016 9 8 7 12 73.09 1.26 1.2947 8 15 2 12 74.03 1.35 1.2805 10 11 5 12 74.09 1.12 1.2797 0 13 8 6 74.16 1.05 1.2786 5 17 3 12 74.16 1.23 1.2786 17 5 3 12 75.71 1.22 1.2562 8 16 1 12 75.95 1.42 1.2529 3 9 9 12 76.39 1.55 1.2468 7 13 6 12 78.29 1.45 1.2212 15 9 3 12 79.52 1.13 1.2053 21 2 1 12 79.76 1.23 1.2024 4 10 9 12 79.76 1.05 1.2024 10 4 9 12 80.01 1.10 1.1992 2 16 7 12 82.63 1.46 1.1677 2 3 11 12 83.37 1.09 1.1592 19 1 6 12 86.65 1.43 1.1235 4 5 11 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.