Tokkoite Rozhdestvenskaya I V, Nikishova L V, Lazebnik Yu D, Lazebnik K A Zeitschrift fur Kristallographie 189 (1989) 195-204 The crystal structure of tokkoite and its relation to the structure of tinaksite Locality: Murun massif, southwestern Yakutia, Russia Note: anisotropic temperature factors taken from ICSD _database_code_amcsd 0010996 CELL PARAMETERS: 10.4380 12.5110 7.1120 89.920 99.750 92.890 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 914.152 Density (g/cm3): 2.736 MAX. ABS. INTENSITY / VOLUME**2: 4.103758424 RIR: 0.488 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.07 23.69 12.4948 0 1 0 2 8.61 100.00 10.2739 1 0 0 2 10.87 1.90 8.1417 -1 1 0 2 11.43 17.31 7.7446 1 1 0 2 14.18 3.58 6.2474 0 2 0 2 14.54 1.47 6.0941 0 1 1 2 15.89 4.62 5.5767 -1 -1 1 2 16.23 3.02 5.4629 -1 2 0 2 16.47 1.61 5.3810 1 0 1 2 16.98 32.75 5.2212 1 2 0 2 17.26 1.08 5.1369 2 0 0 2 17.74 1.24 5.0011 1 -1 1 2 18.16 8.05 4.8853 1 1 1 2 18.34 14.82 4.8385 -2 1 0 2 19.01 15.64 4.6682 2 1 0 2 19.10 1.37 4.6470 0 2 1 2 19.75 3.39 4.4952 -1 2 1 2 20.25 2.65 4.3854 -1 -2 1 2 21.15 1.13 4.2010 -2 -1 1 2 21.33 4.85 4.1649 0 3 0 2 21.44 3.10 4.1437 1 -2 1 2 21.83 3.26 4.0708 -2 2 0 2 22.62 4.89 3.9301 -1 3 0 2 22.97 5.96 3.8723 2 2 0 2 24.51 5.22 3.6316 2 1 1 2 24.79 2.52 3.5920 0 -3 1 2 24.95 22.43 3.5691 0 3 1 2 25.33 4.15 3.5161 -1 3 1 2 25.42 2.64 3.5045 0 0 2 2 25.42 2.19 3.5033 -1 0 2 2 25.92 27.15 3.4370 -1 -3 1 2 26.02 16.65 3.4246 3 0 0 2 26.35 9.01 3.3821 -1 1 2 2 26.36 10.24 3.3807 0 -1 2 2 26.46 3.27 3.3680 0 1 2 2 26.49 3.03 3.3644 -1 -1 2 2 26.64 24.27 3.3465 -3 1 0 2 26.64 16.57 3.3462 1 -3 1 2 26.71 1.16 3.3374 2 -2 1 2 26.86 45.99 3.3189 -2 3 0 2 26.97 2.54 3.3059 -3 0 1 2 27.35 38.54 3.2608 3 1 0 2 27.50 13.13 3.2434 1 3 1 2 28.24 13.05 3.1604 -3 -1 1 2 28.26 30.01 3.1575 2 3 0 2 28.26 35.39 3.1574 1 0 2 2 28.29 35.30 3.1546 -2 0 2 2 28.54 18.08 3.1277 -2 3 1 2 28.58 31.12 3.1237 0 4 0 2 29.02 36.07 3.0774 1 -1 2 2 29.02 36.06 3.0767 -2 1 2 2 29.09 3.94 3.0696 -3 2 0 2 29.31 40.63 3.0471 0 2 2 2 29.33 4.40 3.0452 1 1 2 2 29.36 42.09 3.0425 -1 -2 2 2 29.37 5.17 3.0408 -2 -1 2 2 29.46 8.86 3.0319 -1 4 0 2 29.73 1.57 3.0049 -2 -3 1 2 30.00 5.17 2.9789 -3 2 1 2 30.33 20.84 2.9471 1 4 0 2 30.40 2.00 2.9406 3 2 0 2 30.94 6.68 2.8898 3 0 1 2 30.99 13.96 2.8861 2 -3 1 2 31.45 8.01 2.8444 -2 2 2 2 31.45 1.29 2.8444 3 -1 1 2 31.46 7.67 2.8435 1 -2 2 2 32.04 3.72 2.7931 1 2 2 2 32.10 2.77 2.7884 -2 -2 2 2 32.11 8.75 2.7875 3 1 1 2 33.01 30.71 2.7139 -3 3 0 2 33.25 2.01 2.6944 -1 3 2 2 33.29 1.65 2.6912 0 -3 2 2 33.30 19.37 2.6905 2 0 2 2 33.34 17.63 2.6876 -3 0 2 2 33.54 14.07 2.6720 0 3 2 2 33.56 6.19 2.6700 3 -2 1 2 33.59 13.06 2.6677 -1 -3 2 2 33.84 6.81 2.6490 -3 3 1 2 34.32 12.15 2.6129 2 1 2 2 34.35 20.34 2.6106 2 4 0 2 34.37 11.37 2.6091 -3 -1 2 2 34.75 5.05 2.5815 3 3 0 2 34.93 8.42 2.5685 4 0 0 2 35.11 5.55 2.5556 -4 0 1 2 35.26 1.97 2.5452 -2 3 2 2 35.29 1.56 2.5434 1 -3 2 2 35.51 3.34 2.5278 -4 1 1 2 35.91 10.20 2.5005 2 -2 2 2 35.92 10.58 2.5003 -3 2 2 2 35.94 4.18 2.4990 0 5 0 2 36.21 2.40 2.4805 -4 -1 1 2 36.57 8.82 2.4571 -1 5 0 2 36.80 2.04 2.4426 2 2 2 2 36.86 1.58 2.4386 -3 -2 2 2 37.04 2.01 2.4271 3 -3 1 2 37.37 2.79 2.4062 -4 2 1 2 37.47 12.02 2.4003 1 5 0 2 37.87 1.57 2.3758 2 4 1 2 37.99 14.91 2.3687 -3 4 0 2 38.15 2.40 2.3592 0 -5 1 2 38.42 2.80 2.3433 -1 5 1 2 38.53 1.18 2.3364 0 0 3 2 38.57 4.38 2.3341 4 2 0 2 38.76 8.81 2.3235 0 4 2 2 38.82 8.93 2.3199 -1 -4 2 2 39.28 4.63 2.2936 -2 5 0 2 39.35 3.66 2.2895 4 0 1 2 39.68 1.69 2.2714 4 -1 1 2 39.80 3.95 2.2650 3 0 2 2 39.84 3.94 2.2626 -4 0 2 2 40.05 4.77 2.2515 3 4 0 2 40.12 3.69 2.2476 -2 4 2 2 40.16 4.32 2.2456 1 -4 2 2 40.30 3.47 2.2377 -4 3 0 2 40.50 3.42 2.2275 2 3 2 2 40.52 1.07 2.2264 -4 3 1 2 40.57 4.23 2.2237 -3 -3 2 2 40.63 5.60 2.2204 -3 -4 1 2 40.76 1.93 2.2138 3 1 2 2 40.82 2.13 2.2108 -4 -1 2 2 41.10 7.56 2.1964 1 4 2 2 41.17 8.77 2.1927 -2 -4 2 2 41.84 1.55 2.1592 1 1 3 2 41.90 16.69 2.1560 3 -2 2 2 41.92 16.30 2.1552 -4 2 2 2 42.71 1.14 2.1173 4 2 1 2 43.00 15.79 2.1036 3 2 2 2 43.06 16.88 2.1005 -4 -2 2 2 43.64 4.44 2.0743 3 4 1 2 43.76 1.14 2.0687 -5 0 1 2 43.83 2.15 2.0656 -3 -1 3 2 43.92 8.31 2.0615 -1 6 0 2 44.07 3.88 2.0548 5 0 0 2 44.31 1.66 2.0443 -5 1 0 2 44.43 1.57 2.0389 -3 5 1 2 44.51 1.60 2.0354 -4 4 0 2 44.81 1.04 2.0226 3 -3 2 2 44.81 1.20 2.0225 -4 3 2 2 45.08 1.03 2.0112 -2 3 3 2 45.18 6.19 2.0068 2 4 2 2 45.26 5.24 2.0035 -3 -4 2 2 45.70 2.10 1.9851 -2 -3 3 2 45.78 5.07 1.9821 -5 2 0 2 46.09 1.39 1.9694 2 1 3 2 46.24 1.76 1.9635 1 -6 1 2 46.35 1.44 1.9590 1 -3 3 2 46.86 2.51 1.9387 1 5 2 2 46.94 3.01 1.9357 -2 -5 2 2 46.96 1.20 1.9347 3 -5 1 2 47.01 1.49 1.9330 -4 -4 1 2 47.07 3.19 1.9305 1 3 3 2 47.31 1.04 1.9213 -2 6 1 2 48.14 1.83 1.8903 -1 4 3 2 48.49 1.34 1.8775 0 -4 3 2 48.85 1.75 1.8645 0 4 3 2 49.93 1.10 1.8267 -2 -4 3 2 50.25 1.91 1.8158 4 2 2 2 50.32 2.16 1.8134 -5 -2 2 2 50.54 1.14 1.8060 4 4 1 2 50.68 2.37 1.8011 3 4 2 2 50.77 2.42 1.7984 -4 -4 2 2 50.78 2.91 1.7981 -1 6 2 2 50.84 2.69 1.7960 0 -6 2 2 51.18 1.38 1.7850 0 7 0 2 51.39 48.95 1.7780 -1 0 4 2 51.52 2.30 1.7739 -1 7 0 2 51.52 3.51 1.7739 4 -3 2 2 51.53 3.41 1.7735 -5 3 2 2 51.80 1.57 1.7649 -3 4 3 2 52.01 3.60 1.7583 -5 4 0 2 52.02 1.96 1.7580 -2 6 2 2 52.07 1.80 1.7564 1 -6 2 2 52.20 2.00 1.7523 0 0 4 2 52.22 1.77 1.7516 -2 0 4 2 52.23 1.21 1.7514 5 -3 1 2 52.37 1.47 1.7472 4 5 0 2 52.48 3.04 1.7437 1 7 0 2 53.33 1.10 1.7180 4 3 2 2 53.48 8.14 1.7133 -2 7 0 2 53.52 1.53 1.7123 6 0 0 2 53.55 1.01 1.7112 3 -5 2 2 53.61 2.02 1.7094 3 2 3 2 53.72 3.50 1.7063 2 -4 3 2 53.92 1.68 1.7005 0 5 3 2 54.34 1.05 1.6884 5 3 1 2 54.38 1.19 1.6870 -5 -4 1 2 54.46 4.66 1.6850 6 1 0 2 54.70 1.11 1.6779 5 4 0 2 54.83 8.73 1.6743 -3 6 2 2 54.87 8.38 1.6731 2 -6 2 2 55.34 3.71 1.6601 2 7 0 2 55.72 3.75 1.6497 5 -1 2 2 55.76 4.03 1.6485 -6 1 2 2 55.82 3.51 1.6471 3 5 2 2 55.87 1.72 1.6456 2 -7 1 2 55.90 3.76 1.6447 -4 -5 2 2 55.94 1.64 1.6438 -4 4 3 2 56.52 2.94 1.6283 -5 5 0 2 56.91 1.27 1.6180 -5 -2 3 2 56.94 6.59 1.6172 5 -2 2 2 56.97 6.74 1.6164 -6 2 2 2 57.33 8.97 1.6071 4 4 2 2 57.42 9.32 1.6049 -5 -4 2 2 57.55 1.65 1.6016 -3 7 1 2 57.73 5.92 1.5970 -1 7 2 2 57.80 5.98 1.5952 0 -7 2 2 58.17 3.31 1.5859 0 7 2 2 58.25 3.01 1.5840 -1 -7 2 2 58.73 1.76 1.5721 -6 -3 1 2 58.79 1.77 1.5706 2 -1 4 2 58.83 2.08 1.5697 -4 1 4 2 58.92 2.54 1.5676 -3 3 4 2 58.94 2.43 1.5670 1 -3 4 2 59.07 1.46 1.5639 -4 6 2 2 59.10 1.67 1.5632 3 -6 2 2 59.15 1.33 1.5619 2 1 4 2 59.23 1.25 1.5601 -4 -1 4 2 59.40 2.86 1.5561 6 3 0 2 59.62 1.56 1.5508 3 7 0 2 59.63 2.46 1.5504 1 3 4 2 59.70 3.28 1.5489 5 5 0 2 59.70 1.00 1.5488 -2 6 3 2 59.73 2.53 1.5481 -3 -3 4 2 59.81 2.44 1.5462 -1 4 4 2 59.90 2.70 1.5443 -1 -4 4 2 60.30 4.85 1.5348 -6 4 0 2 60.70 2.29 1.5256 1 -6 3 2 60.73 1.44 1.5250 -2 -6 3 2 60.80 1.51 1.5235 0 4 4 2 60.90 1.62 1.5213 -2 -4 4 2 61.35 2.62 1.5111 -3 7 2 2 61.40 2.68 1.5100 2 -7 2 2 61.76 1.25 1.5020 -4 7 0 2 61.79 3.92 1.5014 -5 6 0 2 61.91 1.01 1.4988 1 6 3 2 61.93 2.14 1.4984 -3 6 3 2 62.44 3.52 1.4873 -4 3 4 2 62.45 3.34 1.4872 2 -3 4 2 63.09 1.77 1.4736 2 8 0 2 63.22 3.18 1.4707 1 4 4 2 63.34 3.22 1.4683 -3 -4 4 2 63.37 4.55 1.4677 7 0 0 2 63.46 2.78 1.4658 2 7 2 2 63.49 1.10 1.4652 -5 -4 3 2 63.56 2.91 1.4639 -3 -7 2 2 64.47 3.47 1.4453 -7 2 0 2 64.59 5.77 1.4429 6 -1 2 2 64.64 5.99 1.4420 -7 1 2 2 65.41 3.63 1.4268 5 6 0 2 66.14 2.80 1.4129 7 2 0 2 66.18 1.25 1.4121 5 1 3 2 66.45 6.54 1.4069 -7 3 0 2 66.51 1.39 1.4058 -3 5 4 2 66.57 1.38 1.4046 1 -5 4 2 66.69 1.49 1.4024 4 4 3 2 67.01 1.21 1.3966 2 4 4 2 67.46 1.28 1.3883 0 9 0 2 67.72 1.43 1.3837 4 6 2 2 67.81 1.34 1.3820 -5 -6 2 2 67.92 2.74 1.3801 6 5 0 2 68.73 1.89 1.3657 -4 8 0 2 69.81 2.16 1.3472 -2 6 4 2 69.91 2.09 1.3456 0 -6 4 2 69.93 1.69 1.3453 -1 3 5 2 70.44 2.37 1.3368 -2 -3 5 2 70.76 1.14 1.3315 0 -3 5 2 71.23 1.16 1.3239 4 -2 4 2 71.27 1.07 1.3231 -6 2 4 2 72.09 1.93 1.3102 -4 8 2 2 72.13 1.85 1.3095 3 -8 2 2 72.40 1.33 1.3053 4 8 0 2 73.35 1.41 1.2908 6 6 0 2 73.55 1.15 1.2877 -7 -4 2 2 73.90 1.68 1.2824 -2 9 2 2 73.97 1.71 1.2814 1 -9 2 2 73.98 1.15 1.2814 4 7 2 2 74.08 1.04 1.2798 -5 -7 2 2 74.37 1.00 1.2755 2 -2 5 2 74.40 1.49 1.2751 -5 8 0 2 75.02 1.31 1.2661 7 1 2 2 75.09 1.36 1.2651 -8 -1 2 2 75.32 1.08 1.2618 -5 0 5 2 76.14 1.38 1.2503 4 -4 4 2 76.15 1.44 1.2501 -6 4 4 2 76.19 1.03 1.2495 0 10 0 2 76.30 1.50 1.2480 -1 10 0 2 77.28 1.04 1.2346 -2 5 5 2 77.30 1.03 1.2344 -3 7 4 2 77.39 1.06 1.2331 1 -7 4 2 77.73 1.23 1.2285 -2 10 0 2 78.81 1.55 1.2144 1 7 4 2 78.82 1.28 1.2143 -4 -4 5 2 78.84 1.05 1.2140 5 8 0 2 78.97 1.45 1.2124 -3 -7 4 2 84.44 1.09 1.1472 -6 6 4 2 84.47 1.24 1.1470 4 -6 4 2 85.17 1.27 1.1392 1 0 6 2 85.23 1.02 1.1386 -4 0 6 2 85.53 1.29 1.1353 -1 11 0 2 85.80 1.27 1.1325 6 0 4 2 85.92 1.14 1.1313 -8 0 4 2 86.09 1.06 1.1294 7 2 3 2 86.44 1.38 1.1257 6 8 0 2 86.73 1.30 1.1228 1 11 0 2 87.23 2.04 1.1176 8 -3 2 2 87.27 2.23 1.1171 -9 3 2 2 87.43 1.44 1.1155 -9 3 0 2 87.85 1.40 1.1113 5 8 2 2 87.96 1.46 1.1102 -6 -8 2 2 88.29 1.23 1.1069 6 2 4 2 88.44 1.61 1.1054 -8 -2 4 2 88.62 1.76 1.1036 6 -3 4 2 88.68 1.88 1.1030 -8 3 4 2 88.74 1.03 1.1025 -5 -9 2 2 89.76 1.06 1.0926 -5 10 0 2 89.83 1.16 1.0918 8 -4 2 2 89.87 1.18 1.0915 -9 4 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.