As6 K6 Na4 Sn2 Eisenmann B, Klein J Zeitschrift fur Kristallographie 196 (1991) 213-229 Dimere Zintl-Anionen (Sn2 As6)10- und (Sn2 Sb6)10- in Alkaliverbindungen _cod_database_code 1008873 _database_code_amcsd 0016740 CELL PARAMETERS: 20.4350 6.8200 15.3510 90.000 90.000 90.000 SPACE GROUP: Cmca X-RAY WAVELENGTH: 1.541838 Cell Volume: 2139.418 Density (g/cm3): 3.146 MAX. ABS. INTENSITY / VOLUME**2: 22.65263859 RIR: 2.344 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.65 23.23 10.2175 2 0 0 2 11.53 96.90 7.6755 0 0 2 2 14.43 13.42 6.1368 2 0 2 4 14.86 100.00 5.9615 1 1 1 8 17.36 11.80 5.1087 4 0 0 2 20.89 6.30 4.2528 4 0 2 4 21.77 50.59 4.0816 3 1 2 8 22.15 19.97 4.0133 1 1 3 8 23.18 2.61 3.8377 0 0 4 2 24.78 2.60 3.5927 2 0 4 4 26.07 12.89 3.4177 5 1 1 8 26.13 14.90 3.4100 0 2 0 2 26.16 18.79 3.4058 6 0 0 2 27.58 1.17 3.2346 2 2 0 4 27.98 1.92 3.1888 5 1 2 8 28.19 4.84 3.1651 2 2 1 8 28.65 29.52 3.1163 0 2 2 4 28.68 27.43 3.1131 6 0 2 4 29.76 90.20 3.0022 3 1 4 8 29.98 1.89 2.9807 2 2 2 8 30.92 13.57 2.8921 5 1 3 8 32.09 4.71 2.7890 4 2 1 8 32.27 1.83 2.7737 1 1 5 8 32.75 4.29 2.7341 2 2 3 8 33.69 3.94 2.6604 4 2 2 8 34.66 1.33 2.5884 5 1 4 8 35.07 2.66 2.5585 0 0 6 2 35.21 69.87 2.5491 0 2 4 4 35.23 73.12 2.5474 6 0 4 4 35.43 1.93 2.5334 7 1 2 8 36.21 4.83 2.4807 4 2 3 8 36.32 1.09 2.4733 2 2 4 8 37.32 97.33 2.4098 6 2 0 4 37.85 3.73 2.3767 7 1 3 8 39.00 12.72 2.3097 5 1 5 8 39.18 17.64 2.2991 6 2 2 8 39.39 1.49 2.2877 4 0 6 4 39.51 7.55 2.2809 4 2 4 8 39.89 24.00 2.2598 3 1 6 8 42.51 1.21 2.1264 8 0 4 4 43.58 2.48 2.0769 1 1 7 8 43.60 4.37 2.0760 3 3 2 8 43.64 6.77 2.0742 9 1 2 8 43.80 4.43 2.0669 1 3 3 8 44.26 12.68 2.0465 0 2 6 4 44.28 13.57 2.0456 6 0 6 4 44.31 1.54 2.0444 8 2 0 4 44.86 5.90 2.0206 7 1 5 8 45.19 1.92 2.0067 2 2 6 8 45.96 1.18 1.9747 10 0 2 4 46.07 10.50 1.9702 5 3 1 8 47.38 2.84 1.9189 0 0 8 2 47.88 1.63 1.8998 4 2 6 8 48.42 13.78 1.8800 3 3 4 8 48.46 17.24 1.8786 9 1 4 8 48.99 4.40 1.8592 5 1 7 8 49.20 3.24 1.8520 5 3 3 8 49.20 1.02 1.8518 7 1 6 8 50.13 13.15 1.8197 1 3 5 8 50.49 1.21 1.8077 8 0 6 4 50.61 3.36 1.8037 10 0 4 4 50.83 2.22 1.7963 4 0 8 4 51.24 19.27 1.7828 3 1 8 8 51.28 7.26 1.7815 7 3 1 8 51.32 4.80 1.7803 11 1 1 8 52.14 3.29 1.7542 6 2 6 8 52.18 2.89 1.7529 10 2 0 4 52.42 1.75 1.7455 11 1 2 8 52.55 1.21 1.7415 10 2 1 8 52.77 1.03 1.7349 4 2 7 8 53.63 1.88 1.7089 10 2 2 8 53.76 10.86 1.7050 0 4 0 2 53.83 13.78 1.7029 12 0 0 2 54.00 1.55 1.6982 7 1 7 8 54.22 3.24 1.6916 11 1 3 8 54.90 3.35 1.6723 0 2 8 4 54.92 3.24 1.6718 6 0 8 4 54.92 1.86 1.6717 2 4 1 8 55.18 2.72 1.6644 0 4 2 4 55.25 2.82 1.6625 12 0 2 4 55.41 1.63 1.6583 10 2 3 8 55.70 1.40 1.6503 2 2 8 8 55.73 3.17 1.6493 1 1 9 8 55.75 5.62 1.6489 3 3 6 8 55.78 6.72 1.6479 9 1 6 8 56.94 1.27 1.6173 4 4 0 4 57.28 2.30 1.6084 4 4 1 8 57.70 2.19 1.5977 2 4 3 8 58.30 1.03 1.5826 4 4 2 8 58.67 2.74 1.5736 1 3 7 8 58.72 1.49 1.5724 9 3 2 8 59.74 1.38 1.5479 11 1 5 8 59.99 2.95 1.5421 4 4 3 8 60.29 6.99 1.5351 0 0 10 2 60.77 1.10 1.5242 13 1 1 8 60.80 1.24 1.5235 12 2 0 4 61.80 4.36 1.5011 6 2 8 8 62.06 5.04 1.4954 6 4 2 8 62.11 4.04 1.4944 12 2 2 8 62.69 4.78 1.4819 9 3 4 8 63.61 2.16 1.4627 3 1 10 8 65.07 5.53 1.4335 3 3 8 8 65.10 7.27 1.4329 9 1 8 8 65.82 1.22 1.4188 0 4 6 4 65.92 11.93 1.4169 6 4 4 8 65.97 13.80 1.4160 12 2 4 8 67.49 1.21 1.3878 11 1 7 8 67.65 1.37 1.3848 11 3 3 8 68.82 1.35 1.3642 1 1 11 8 69.03 2.22 1.3605 9 3 6 8 69.31 3.93 1.3557 1 5 1 8 72.12 3.32 1.3097 6 4 6 8 72.16 4.12 1.3090 12 2 6 8 72.46 1.24 1.3044 10 4 1 8 72.57 2.95 1.3026 11 3 5 8 72.64 1.08 1.3016 4 4 7 8 73.09 11.86 1.2947 6 2 10 8 73.12 2.01 1.2942 10 2 8 8 73.13 2.62 1.2941 5 3 9 8 74.12 1.42 1.2793 0 0 12 2 74.44 1.11 1.2746 0 4 8 4 74.87 1.79 1.2683 10 4 3 8 75.24 1.24 1.2630 3 5 4 8 75.33 2.76 1.2617 15 1 4 8 76.95 1.73 1.2391 10 4 4 8 77.14 1.61 1.2364 3 1 12 8 77.18 2.39 1.2360 7 3 9 8 77.20 1.27 1.2356 11 1 9 8 77.49 2.60 1.2318 9 3 8 8 79.56 4.25 1.2049 12 4 0 4 79.72 1.43 1.2028 11 3 7 8 80.45 1.73 1.1937 6 4 8 8 80.50 1.56 1.1932 12 2 8 8 80.57 3.41 1.1923 5 5 5 8 80.63 2.43 1.1916 13 3 5 8 80.73 1.24 1.1903 12 4 2 8 81.23 1.29 1.1842 15 1 6 8 83.76 1.01 1.1548 10 2 10 8 84.52 3.80 1.1464 7 5 5 8 84.92 1.40 1.1420 5 3 11 8 84.93 1.76 1.1419 16 2 4 8 85.03 2.67 1.1408 0 4 10 4 85.08 3.42 1.1402 12 0 10 4 86.04 3.13 1.1299 6 2 12 8 87.20 1.20 1.1179 15 3 4 8 87.55 1.12 1.1144 5 5 7 8 88.84 1.06 1.1014 7 3 11 8 89.33 1.29 1.0967 11 5 1 8 89.36 1.96 1.0964 15 1 8 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.