Ge P3 Rb5 Eisenmann B, Klein J, Somer M Zeitschrift fur Kristallographie 197 (1991) 263-264 Crystal structure of pentarubidium triphosphidogermanate _cod_database_code 1008461 _database_code_amcsd 0016365 CELL PARAMETERS: 13.9660 5.5820 15.2560 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 1189.330 Density (g/cm3): 3.311 MAX. ABS. INTENSITY / VOLUME**2: 27.59707931 RIR: 2.714 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.60 3.04 7.6280 0 0 2 2 12.68 7.06 6.9830 2 0 0 2 13.23 2.86 6.6945 1 0 2 4 20.37 3.63 4.3601 2 1 0 4 20.72 4.28 4.2872 1 1 2 8 21.62 20.05 4.1108 2 0 3 4 22.37 18.52 3.9738 3 0 2 4 23.50 6.06 3.7854 2 1 2 8 23.67 4.68 3.7592 0 1 3 4 25.51 1.64 3.4915 4 0 0 2 25.59 24.79 3.4809 3 1 1 8 25.95 15.24 3.4338 3 0 3 4 26.18 8.69 3.4035 4 0 1 4 26.63 5.58 3.3473 2 0 4 4 26.94 54.62 3.3101 2 1 3 8 29.07 100.00 3.0720 1 1 4 8 29.98 1.75 2.9809 1 0 5 4 30.19 68.76 2.9601 4 1 0 4 30.29 13.12 2.9503 3 0 4 4 30.57 22.62 2.9247 3 1 3 8 30.77 35.13 2.9059 4 1 1 8 31.16 11.09 2.8707 2 1 4 8 32.01 4.07 2.7959 2 0 5 4 32.07 78.68 2.7910 0 2 0 2 32.44 1.94 2.7596 4 1 2 8 34.10 26.68 2.6294 1 1 5 8 34.19 4.49 2.6229 5 0 2 4 34.38 14.77 2.6084 3 1 4 8 34.61 1.15 2.5917 2 2 0 4 35.08 3.81 2.5583 4 1 3 8 36.45 6.36 2.4651 5 1 1 8 36.71 4.30 2.4482 5 0 3 4 37.65 4.97 2.3892 2 0 6 4 38.68 3.56 2.3277 6 0 0 2 38.80 1.75 2.3209 3 1 5 8 39.01 8.26 2.3091 2 2 3 8 39.45 8.08 2.2839 3 2 2 8 39.47 4.29 2.2828 1 1 6 8 40.01 11.74 2.2535 5 0 4 4 41.09 2.75 2.1965 2 1 6 8 41.70 7.58 2.1658 3 2 3 8 41.86 4.38 2.1582 4 2 1 8 41.96 2.93 2.1534 1 0 7 4 42.16 2.84 2.1436 2 2 4 8 42.72 2.00 2.1165 6 0 3 4 43.30 4.37 2.0896 5 1 4 8 43.50 1.60 2.0805 2 0 7 4 43.68 1.17 2.0721 3 1 6 8 43.78 5.21 2.0679 6 1 2 8 43.95 6.43 2.0603 5 0 5 4 44.06 2.08 2.0554 4 0 6 4 44.47 1.02 2.0374 1 2 5 8 44.70 7.69 2.0275 3 2 4 8 45.87 2.32 1.9783 7 0 1 4 45.94 2.67 1.9753 2 2 5 8 45.98 1.05 1.9738 3 0 7 4 46.59 1.22 1.9495 2 1 7 8 47.08 1.92 1.9302 7 0 2 4 47.57 3.26 1.9113 5 2 2 8 47.69 7.47 1.9070 0 0 8 2 48.16 5.47 1.8895 1 0 8 4 48.41 10.25 1.8803 5 0 6 4 48.95 5.03 1.8609 3 1 7 8 49.05 8.09 1.8573 7 0 3 4 49.24 2.13 1.8506 6 0 5 4 49.53 3.25 1.8405 5 2 3 8 50.27 3.99 1.8150 2 2 6 8 51.10 2.91 1.7876 6 2 0 4 51.71 1.16 1.7679 7 0 4 4 51.88 4.79 1.7623 7 1 3 8 52.11 4.99 1.7550 4 1 7 8 52.17 9.90 1.7533 5 2 4 8 52.78 2.84 1.7344 8 0 1 4 53.36 2.80 1.7168 3 3 1 8 53.77 2.53 1.7049 1 2 7 8 54.10 6.57 1.6951 2 3 3 8 54.40 1.80 1.6864 6 2 3 8 54.54 2.14 1.6826 3 1 8 8 54.99 1.86 1.6698 7 0 5 4 55.05 1.45 1.6680 2 2 7 8 55.33 12.88 1.6604 1 3 4 8 55.43 5.88 1.6576 5 2 5 8 55.48 8.14 1.6563 8 1 1 8 55.52 1.94 1.6550 4 2 6 8 55.81 1.96 1.6473 2 0 9 4 56.00 1.35 1.6422 5 1 7 8 56.00 9.55 1.6421 4 3 0 4 56.23 3.23 1.6359 3 3 3 8 56.35 4.87 1.6326 4 3 1 8 56.54 1.63 1.6278 8 1 2 8 56.59 1.60 1.6263 2 3 4 8 56.76 1.81 1.6220 0 1 9 4 57.06 2.19 1.6140 7 2 1 8 57.49 3.98 1.6031 4 1 8 8 57.62 2.80 1.5998 7 1 5 8 58.10 1.93 1.5875 7 2 2 8 58.27 5.78 1.5833 8 1 3 8 58.47 4.64 1.5784 1 3 5 8 58.63 7.35 1.5746 0 2 8 4 58.66 2.51 1.5738 3 3 4 8 59.04 5.39 1.5646 1 2 8 8 59.26 10.02 1.5594 5 2 6 8 59.81 8.04 1.5462 7 2 3 8 59.98 2.08 1.5424 6 2 5 8 60.05 1.26 1.5406 5 3 1 8 60.44 6.25 1.5317 3 1 9 8 60.51 1.26 1.5300 6 1 7 8 61.14 1.10 1.5158 5 1 8 8 62.15 1.27 1.4935 7 2 4 8 63.11 2.98 1.4731 8 2 1 8 63.40 1.25 1.4672 9 1 2 8 65.00 1.09 1.4348 5 3 4 8 65.09 2.06 1.4330 7 2 5 8 65.36 1.18 1.4277 6 3 2 8 65.83 2.15 1.4186 2 2 9 8 66.68 1.52 1.4026 5 1 9 8 67.07 6.93 1.3955 0 4 0 2 69.29 1.60 1.3561 4 1 10 8 69.42 1.50 1.3539 3 3 7 8 70.26 1.25 1.3398 1 1 11 8 70.80 1.40 1.3308 6 1 9 8 71.24 2.59 1.3237 8 1 7 8 71.37 2.70 1.3217 2 1 11 8 71.68 1.02 1.3167 3 4 2 8 71.81 1.45 1.3145 7 3 3 8 72.01 1.56 1.3115 4 3 7 8 73.21 1.05 1.2928 3 4 3 8 73.28 1.10 1.2918 7 0 9 4 73.48 5.62 1.2888 9 1 6 8 74.84 2.87 1.2687 8 3 1 8 75.34 1.12 1.2615 3 4 4 8 76.57 1.47 1.2443 4 3 8 8 76.60 3.13 1.2439 6 1 10 8 76.68 1.03 1.2428 7 3 5 8 77.01 1.90 1.2383 10 1 5 8 77.25 2.20 1.2350 8 3 3 8 78.23 1.53 1.2220 11 1 2 8 79.15 2.45 1.2100 3 3 9 8 79.72 1.41 1.2029 11 1 3 8 79.94 1.07 1.2000 3 2 11 8 81.05 2.22 1.1864 5 4 4 8 82.23 1.49 1.1723 7 2 9 8 83.71 1.48 1.1554 5 4 5 8 84.33 1.06 1.1484 0 1 13 4 84.68 1.28 1.1446 1 1 13 8 85.61 1.67 1.1345 12 0 3 4 86.40 2.03 1.1262 0 4 8 4 86.75 1.47 1.1225 1 4 8 8 86.94 2.66 1.1206 5 4 6 8 87.42 2.23 1.1157 7 4 3 8 89.06 1.27 1.0993 8 3 7 8 89.18 1.32 1.0982 2 3 11 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.