As6 Na10 Si2 Eisenmann B, Klein J, Somer M Zeitschrift fur Kristallographie 197 (1991) 267-268 Crystal structure of decasodium di-mue-arsenidobis(diarsenidosilicate) _cod_database_code 1008462 _database_code_amcsd 0016366 CELL PARAMETERS: 13.4660 7.5290 8.1770 90.000 90.500 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 828.998 Density (g/cm3): 2.946 MAX. ABS. INTENSITY / VOLUME**2: 10.92049100 RIR: 1.207 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.62 9.73 7.0163 -1 0 1 2 12.71 32.67 6.9621 1 0 1 2 13.15 5.56 6.7327 2 0 0 2 13.47 17.91 6.5715 1 1 0 4 16.00 28.24 5.5386 0 1 1 4 17.28 20.29 5.1330 -1 1 1 4 17.67 18.01 5.0188 2 1 0 4 20.83 2.95 4.2650 2 1 1 4 21.74 7.89 4.0883 0 0 2 2 22.51 41.89 3.9492 -3 0 1 2 22.68 25.94 3.9202 3 0 1 2 23.63 65.93 3.7645 0 2 0 2 24.78 90.04 3.5928 0 1 2 4 25.47 38.57 3.4973 -3 1 1 4 25.59 5.17 3.4811 2 0 2 2 25.62 59.48 3.4771 3 1 1 4 25.71 3.95 3.4648 1 1 2 4 26.06 2.85 3.4195 0 2 1 4 28.06 7.89 3.1799 -2 1 2 4 28.24 1.34 3.1597 2 1 2 4 29.06 8.81 3.0732 4 1 0 4 29.25 4.17 3.0533 -2 2 1 4 31.17 1.49 2.8692 4 1 1 4 31.78 39.13 2.8155 -3 1 2 4 32.03 41.41 2.7945 3 1 2 4 32.33 17.84 2.7693 0 2 2 4 32.87 100.00 2.7249 -3 2 1 4 32.98 4.09 2.7157 -1 2 2 4 32.99 66.28 2.7153 3 2 1 4 33.06 3.45 2.7094 1 2 2 4 33.49 12.92 2.6759 -1 0 3 2 34.66 5.27 2.5877 4 0 2 2 35.01 9.01 2.5628 0 1 3 4 35.11 16.87 2.5558 2 2 2 4 35.18 8.34 2.5513 5 0 1 2 35.72 22.66 2.5138 1 1 3 4 35.78 1.09 2.5094 4 2 0 4 36.42 5.28 2.4672 1 3 0 4 36.43 19.31 2.4660 -4 1 2 4 36.72 7.51 2.4472 4 1 2 4 37.03 14.50 2.4276 -5 1 1 4 37.21 2.01 2.4164 5 1 1 4 37.42 3.16 2.4033 -4 2 1 4 37.45 1.95 2.4017 -2 1 3 4 37.49 52.00 2.3992 0 3 1 4 37.56 4.48 2.3946 4 2 1 4 37.66 1.17 2.3886 2 1 3 4 38.08 7.03 2.3630 -1 3 1 4 38.27 5.84 2.3516 2 3 0 4 38.49 38.05 2.3388 -3 0 3 2 38.80 39.50 2.3207 3 0 3 2 39.92 3.17 2.2582 2 3 1 4 40.18 64.25 2.2442 6 0 0 2 40.38 14.21 2.2335 -3 1 3 4 40.68 6.46 2.2178 3 1 3 4 41.22 1.67 2.1903 5 2 0 4 41.40 13.15 2.1811 -1 2 3 4 42.01 1.49 2.1507 6 1 0 4 42.25 36.67 2.1388 0 3 2 4 42.39 4.44 2.1325 4 2 2 4 42.69 11.84 2.1182 -3 3 1 4 42.78 20.48 2.1136 3 3 1 4 42.82 8.82 2.1120 5 2 1 4 42.84 3.26 2.1109 1 3 2 4 43.42 1.59 2.0843 -6 1 1 4 44.24 1.60 2.0472 -4 1 3 4 44.31 13.01 2.0442 0 0 4 2 44.61 1.22 2.0311 4 1 3 4 45.67 15.62 1.9866 -3 2 3 4 45.94 15.75 1.9755 3 2 3 4 46.30 5.04 1.9608 -2 0 4 2 46.98 6.28 1.9343 -3 3 2 4 47.15 10.36 1.9277 6 2 0 4 47.15 8.72 1.9274 3 3 2 4 47.24 2.80 1.9241 -5 0 3 2 47.61 9.46 1.9100 -6 1 2 4 47.94 1.02 1.8975 -2 1 4 4 47.96 5.62 1.8969 6 1 2 4 48.18 4.54 1.8889 2 1 4 4 48.36 6.73 1.8822 0 4 0 2 48.52 3.01 1.8762 -7 0 1 2 48.72 2.47 1.8689 7 0 1 2 49.28 5.79 1.8490 5 1 3 4 49.36 2.96 1.8462 0 3 3 4 49.90 3.02 1.8277 1 3 3 4 50.18 1.06 1.8180 -1 4 1 4 50.21 1.31 1.8170 1 4 1 4 50.34 1.00 1.8127 2 4 0 4 50.45 4.25 1.8090 -4 3 2 4 50.67 2.34 1.8016 4 3 2 4 50.83 5.79 1.7964 0 2 4 4 50.91 2.01 1.7937 -5 3 1 4 51.05 2.65 1.7891 5 3 1 4 51.23 1.76 1.7832 -2 3 3 4 51.36 1.50 1.7788 1 2 4 4 51.62 1.57 1.7707 -2 4 1 4 52.14 6.81 1.7541 -4 0 4 2 52.58 8.27 1.7405 4 0 4 2 52.63 2.62 1.7390 -2 2 4 4 52.64 4.94 1.7386 6 2 2 4 52.74 5.89 1.7358 3 4 0 4 52.85 1.47 1.7324 2 2 4 4 53.48 1.64 1.7133 -5 2 3 4 53.56 2.86 1.7110 -3 3 3 4 53.60 2.13 1.7098 0 4 2 4 53.65 1.60 1.7083 -4 1 4 4 53.96 1.23 1.6991 -3 4 1 4 54.08 4.16 1.6958 4 1 4 4 54.09 1.83 1.6954 1 4 2 4 54.10 3.08 1.6953 -6 1 3 4 54.52 2.91 1.6832 8 0 0 2 54.66 1.06 1.6792 -7 2 1 4 54.68 3.36 1.6786 -5 3 2 4 54.84 1.68 1.6740 7 2 1 4 54.88 1.54 1.6729 6 3 0 4 55.50 9.06 1.6557 2 4 2 4 55.98 7.54 1.6426 8 1 0 4 56.04 12.83 1.6411 -6 3 1 4 56.19 8.30 1.6369 6 3 1 4 56.73 2.21 1.6228 -4 3 3 4 56.77 4.92 1.6217 1 0 5 2 57.03 3.46 1.6147 4 3 3 4 57.14 3.69 1.6120 -4 4 1 4 57.24 2.34 1.6094 4 4 1 4 57.69 4.48 1.5981 0 1 5 4 58.01 7.64 1.5899 -4 2 4 4 58.06 8.48 1.5885 -1 1 5 4 58.41 5.47 1.5798 4 2 4 4 58.48 2.37 1.5781 -7 0 3 2 58.59 1.88 1.5755 7 2 2 4 59.18 1.78 1.5612 -8 0 2 2 59.57 10.54 1.5519 -6 3 2 4 59.70 1.84 1.5488 0 4 3 4 59.87 5.84 1.5448 6 3 2 4 59.88 3.66 1.5446 -7 1 3 4 59.96 1.38 1.5428 5 4 0 4 60.04 1.34 1.5409 -3 0 5 2 60.06 5.76 1.5404 2 3 4 4 60.10 7.01 1.5395 -1 4 3 4 60.23 2.74 1.5366 8 2 0 4 60.41 9.45 1.5324 7 1 3 4 60.41 1.47 1.5322 3 0 5 2 60.57 1.50 1.5287 -8 1 2 4 60.66 2.23 1.5267 7 3 0 4 60.66 2.38 1.5267 -4 4 2 4 60.96 3.52 1.5197 8 1 2 4 61.02 2.13 1.5186 5 3 3 4 61.05 3.75 1.5178 -6 0 4 2 61.07 2.54 1.5174 -5 4 1 4 61.19 4.55 1.5147 5 4 1 4 61.42 1.02 1.5096 -3 1 5 4 61.49 1.17 1.5080 8 2 1 4 61.64 2.71 1.5047 6 0 4 2 61.96 11.28 1.4977 -3 3 4 4 62.25 9.18 1.4913 3 3 4 4 62.34 6.22 1.4894 1 2 5 4 62.74 2.06 1.4809 0 5 1 4 63.07 1.06 1.4740 -9 0 1 2 63.15 4.09 1.4723 -1 5 1 4 63.28 2.78 1.4695 2 5 0 4 63.97 3.73 1.4554 -7 2 3 4 64.63 2.97 1.4422 6 4 0 4 64.63 2.87 1.4421 -8 2 2 4 64.85 2.40 1.4377 -4 3 4 4 65.01 4.21 1.4346 8 2 2 4 65.07 1.20 1.4335 -7 3 2 4 65.23 1.10 1.4302 4 3 4 4 65.68 1.98 1.4217 6 3 3 4 66.13 3.37 1.4130 0 5 2 4 66.41 2.44 1.4077 -6 2 4 4 66.45 2.71 1.4070 -3 5 1 4 66.52 5.96 1.4057 3 5 1 4 66.94 3.17 1.3979 8 3 0 4 67.65 1.86 1.3850 -9 1 2 4 67.66 1.18 1.3847 0 4 4 4 68.02 1.20 1.3782 -1 4 4 4 68.07 2.51 1.3774 9 1 2 4 68.12 2.38 1.3766 1 4 4 4 68.13 1.17 1.3763 8 3 1 4 68.34 6.91 1.3725 -9 2 1 4 68.48 1.73 1.3701 0 3 5 4 68.55 2.37 1.3689 9 2 1 4 68.71 1.46 1.3660 4 2 5 4 68.83 4.43 1.3641 -1 3 5 4 68.92 4.39 1.3624 -6 4 2 4 69.71 4.47 1.3490 -3 5 2 4 69.85 4.40 1.3466 3 5 2 4 69.97 1.17 1.3445 -2 3 5 4 70.26 3.03 1.3397 5 4 3 4 70.97 2.40 1.3281 7 3 3 4 71.60 1.06 1.3180 -7 2 4 4 71.64 2.33 1.3173 -2 1 6 4 71.69 1.39 1.3164 -9 0 3 2 71.90 1.40 1.3131 -3 3 5 4 71.95 1.13 1.3123 -1 5 3 4 72.29 1.30 1.3070 -6 1 5 4 72.31 1.96 1.3067 9 0 3 2 72.36 1.03 1.3060 5 2 5 4 72.95 2.65 1.2968 5 5 1 4 72.96 2.47 1.2967 -9 1 3 4 72.97 1.72 1.2966 6 1 5 4 73.97 2.58 1.2814 0 2 6 4 74.36 1.67 1.2756 7 4 2 4 74.88 1.80 1.2681 9 3 1 4 74.95 1.11 1.2671 -4 0 6 2 75.02 2.73 1.2661 -3 5 3 4 75.16 2.23 1.2641 -10 1 2 4 75.61 1.28 1.2577 10 1 2 4 76.13 1.21 1.2504 6 5 0 4 76.19 4.32 1.2495 -4 1 6 4 76.73 6.43 1.2421 4 1 6 4 76.84 2.44 1.2406 7 0 5 2 76.86 1.98 1.2403 0 6 1 4 77.26 1.26 1.2349 1 6 1 4 77.29 5.73 1.2344 -7 1 5 4 77.73 1.34 1.2286 1 4 5 4 77.96 1.13 1.2256 4 5 3 4 78.07 1.23 1.2241 7 1 5 4 78.12 1.07 1.2234 9 3 2 4 79.21 1.37 1.2093 -7 4 3 4 79.23 2.62 1.2091 11 0 1 2 79.27 1.92 1.2085 3 6 0 4 79.81 1.07 1.2017 -8 4 2 4 79.88 1.31 1.2009 -4 2 6 4 80.16 2.35 1.1974 -6 5 2 4 80.16 3.18 1.1973 8 4 2 4 80.21 5.21 1.1968 -11 1 1 4 80.28 1.87 1.1959 -3 6 1 4 80.45 1.16 1.1937 -1 3 6 4 80.58 3.50 1.1921 2 5 4 4 81.43 1.73 1.1819 5 5 3 4 81.46 1.73 1.1815 -6 4 4 4 81.53 1.08 1.1807 -2 3 6 4 81.54 5.07 1.1805 2 6 2 4 81.73 4.14 1.1783 7 2 5 4 82.80 1.50 1.1658 -9 3 3 4 82.90 1.56 1.1646 -1 0 7 2 83.60 1.42 1.1566 4 4 5 4 84.08 3.54 1.1512 11 2 1 4 84.19 1.22 1.1500 8 3 4 4 84.26 3.60 1.1492 1 1 7 4 84.87 1.35 1.1425 -4 5 4 4 85.12 1.82 1.1398 0 6 3 4 85.36 1.44 1.1372 10 3 2 4 85.46 2.21 1.1361 -1 6 3 4 85.93 2.01 1.1311 -4 3 6 4 85.95 1.83 1.1309 -4 6 2 4 86.13 1.99 1.1290 -10 0 4 2 86.31 1.60 1.1271 -5 6 1 4 86.32 1.67 1.1270 -7 4 4 4 86.45 3.00 1.1256 4 3 6 4 86.78 1.23 1.1223 8 5 0 4 86.79 1.61 1.1221 12 0 0 2 86.93 1.34 1.1207 7 4 4 4 86.96 1.68 1.1203 -11 0 3 2 86.99 2.16 1.1200 10 0 4 2 87.01 2.55 1.1199 -7 3 5 4 87.05 1.29 1.1194 5 4 5 4 87.71 1.18 1.1127 -8 5 1 4 87.72 2.14 1.1126 -1 2 7 4 88.21 1.37 1.1077 0 5 5 4 88.53 2.28 1.1045 -1 5 5 4 88.60 1.01 1.1038 0 4 6 4 88.88 2.90 1.1011 11 1 3 4 89.85 2.12 1.0917 -9 3 4 4 89.86 1.94 1.0915 -11 3 1 4 89.97 1.13 1.0905 -2 4 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.