As3 Ge K Na4 Eisenmann B, Klein J Zeitschrift fur Kristallographie 197 (1991) 279-280 Crystal structure of tetrasodium monopotassium triarsenidogermanate _cod_database_code 1008467 _database_code_amcsd 0016371 CELL PARAMETERS: 15.1610 4.8130 13.1680 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 960.868 Density (g/cm3): 2.961 MAX. ABS. INTENSITY / VOLUME**2: 22.76374886 RIR: 2.503 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.89 9.10 9.9417 1 0 1 4 11.67 14.83 7.5805 2 0 0 2 13.45 2.66 6.5840 0 0 2 2 13.48 2.09 6.5697 2 0 1 4 14.67 25.56 6.0391 1 0 2 4 17.84 6.69 4.9708 2 0 2 4 18.81 10.79 4.7181 3 0 1 4 19.64 23.47 4.5205 0 1 1 4 20.50 100.00 4.3320 1 1 1 8 21.87 16.18 4.0632 2 1 0 4 22.17 2.45 4.0089 3 0 2 4 22.91 5.77 3.8826 2 1 1 8 23.42 37.92 3.7985 2 0 3 4 23.47 14.82 3.7903 4 0 0 2 23.64 1.53 3.7639 1 1 2 8 25.77 2.50 3.4578 2 1 2 8 26.45 2.73 3.3693 3 1 1 8 26.90 1.38 3.3139 3 0 3 4 27.09 3.06 3.2920 0 0 4 2 28.99 20.78 3.0803 3 1 2 8 29.97 56.01 2.9818 2 1 3 8 30.01 16.12 2.9778 4 1 0 4 30.78 26.82 2.9044 4 1 1 8 33.01 5.05 2.7132 4 1 2 8 33.51 31.80 2.6746 1 1 4 8 34.57 2.31 2.5947 1 0 5 4 35.08 10.53 2.5578 2 1 4 8 35.65 23.55 2.5182 5 1 1 8 36.00 1.30 2.4948 5 0 3 4 36.20 2.00 2.4816 6 0 1 4 36.46 17.86 2.4642 4 1 3 8 37.37 52.91 2.4065 0 2 0 2 37.58 8.49 2.3932 3 1 4 8 37.63 12.96 2.3905 5 1 2 8 38.15 3.75 2.3591 6 0 2 4 38.98 2.10 2.3103 0 1 5 4 39.28 1.65 2.2937 2 2 0 4 39.45 18.61 2.2840 1 1 5 8 40.34 3.97 2.2355 1 2 2 8 40.44 1.68 2.2303 5 0 4 4 40.86 2.12 2.2084 4 1 4 8 41.13 20.39 2.1947 0 0 6 2 41.22 45.81 2.1899 6 0 3 4 41.70 1.44 2.1660 2 2 2 8 42.15 2.38 2.1437 3 2 1 8 42.29 2.49 2.1371 7 0 1 4 42.68 6.71 2.1183 6 1 2 8 42.90 4.70 2.1081 2 0 6 4 44.57 13.11 2.0329 2 2 3 8 44.60 5.40 2.0316 4 2 0 4 44.79 13.60 2.0236 5 1 4 8 45.24 3.67 2.0044 6 0 4 4 45.63 2.34 1.9883 5 0 5 4 46.76 1.17 1.9428 0 2 4 4 47.06 6.02 1.9310 2 1 6 8 47.90 4.39 1.8993 4 0 6 4 48.01 2.94 1.8951 8 0 0 2 48.10 9.73 1.8918 7 1 2 8 48.53 1.31 1.8758 8 0 1 4 48.78 4.42 1.8668 1 0 7 4 49.05 1.50 1.8571 3 1 6 8 49.24 4.59 1.8504 6 1 4 8 49.61 2.22 1.8377 5 1 5 8 50.44 1.39 1.8094 7 0 4 4 51.74 1.79 1.7667 4 1 6 8 51.81 1.22 1.7645 1 2 5 8 51.85 3.97 1.7634 8 1 0 4 52.21 1.08 1.7521 0 1 7 4 52.58 8.34 1.7405 1 1 7 8 52.60 3.68 1.7399 8 0 3 4 53.01 1.15 1.7276 6 2 1 8 54.15 7.03 1.6937 7 1 4 8 54.47 2.39 1.6846 6 2 2 8 54.88 2.08 1.6728 7 0 5 4 55.07 3.11 1.6677 5 1 6 8 55.51 1.08 1.6554 3 1 7 8 56.21 3.67 1.6364 1 0 8 4 56.22 3.17 1.6363 8 1 3 8 56.23 1.14 1.6358 5 2 4 8 56.77 14.59 1.6216 0 2 6 4 56.85 32.51 1.6197 6 2 3 8 57.69 1.76 1.5980 7 2 1 8 57.90 1.27 1.5926 0 3 1 4 57.99 3.48 1.5904 4 1 7 8 58.18 3.41 1.5857 2 2 6 8 58.25 5.49 1.5838 1 3 1 8 58.47 4.37 1.5785 9 1 1 8 58.83 1.06 1.5696 2 3 0 4 59.84 1.40 1.5456 9 1 2 8 60.07 2.74 1.5402 6 2 4 8 60.15 2.12 1.5383 8 0 5 4 60.39 1.96 1.5328 5 2 5 8 61.08 8.19 1.5170 5 1 7 8 61.87 1.11 1.4996 9 0 4 4 62.27 3.93 1.4909 4 2 6 8 62.34 1.75 1.4895 3 3 2 8 62.37 2.53 1.4889 8 2 0 4 62.81 1.23 1.4795 8 2 1 8 62.88 4.95 1.4779 2 3 3 8 62.91 1.37 1.4774 4 3 0 4 63.02 3.59 1.4750 1 2 7 8 63.35 2.54 1.4682 4 3 1 8 64.43 1.24 1.4462 7 2 4 8 64.43 1.93 1.4461 10 1 0 4 64.71 1.59 1.4406 4 1 8 8 64.87 1.33 1.4374 10 1 1 8 64.91 1.76 1.4366 2 0 9 4 64.95 3.68 1.4357 1 3 4 8 65.02 1.42 1.4344 8 0 6 4 65.09 1.51 1.4330 10 0 3 4 65.93 1.41 1.4168 2 3 4 8 66.29 3.36 1.4100 8 2 3 8 66.29 3.25 1.4099 5 3 1 8 66.81 2.58 1.4002 4 3 3 8 67.54 1.33 1.3868 3 3 4 8 67.57 1.95 1.3863 5 3 2 8 68.23 2.44 1.3746 8 1 6 8 68.29 2.01 1.3736 7 2 5 8 68.80 3.11 1.3646 1 3 5 8 69.46 3.57 1.3532 1 2 8 8 71.06 1.28 1.3266 6 3 2 8 71.22 1.09 1.3240 10 1 4 8 71.57 1.04 1.3184 11 1 1 8 71.90 1.48 1.3132 4 1 9 8 72.59 2.83 1.3024 5 3 4 8 72.81 3.15 1.2990 11 1 2 8 73.00 2.14 1.2961 8 2 5 8 74.29 1.33 1.2767 2 3 6 8 74.56 1.16 1.2727 9 2 4 8 74.92 2.07 1.2675 10 1 5 8 75.01 3.19 1.2662 6 0 9 4 75.05 2.74 1.2657 1 1 10 8 75.08 2.51 1.2652 7 3 2 8 75.13 2.85 1.2645 7 1 8 8 75.21 1.14 1.2634 12 0 0 2 75.61 1.05 1.2576 12 0 1 4 75.97 1.22 1.2525 6 3 4 8 77.36 2.00 1.2335 2 2 9 8 77.47 1.63 1.2321 8 2 6 8 77.53 1.75 1.2313 10 2 3 8 77.68 1.89 1.2292 11 1 4 8 78.63 1.19 1.2168 12 1 1 8 78.63 2.50 1.2167 1 3 7 8 79.35 1.30 1.2075 10 1 6 8 79.69 4.22 1.2033 0 4 0 2 79.91 2.28 1.2004 7 3 4 8 81.63 1.04 1.1794 8 3 3 8 82.30 1.49 1.1715 5 1 10 8 83.13 1.03 1.1619 4 3 7 8 83.45 1.01 1.1583 1 1 11 8 83.54 1.29 1.1573 9 3 1 8 84.45 1.99 1.1471 2 4 3 8 85.58 1.12 1.1348 6 1 10 8 85.81 2.61 1.1324 5 3 7 8 86.11 1.57 1.1293 13 1 1 8 86.94 4.14 1.1205 6 2 9 8 87.13 1.53 1.1186 12 2 0 4 87.52 1.37 1.1146 12 2 1 8 89.44 2.97 1.0956 7 1 10 8 89.51 1.66 1.0949 12 0 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.