IMA2008-067 Koennecke M, Miehe G, Fuess H Zeitschrift fur Kristallographie 201 (1992) 147-155 Static disorder of dodecasil 3C. A single-crystal study with synchrotron radiation Note: T = 523 K, conventional anisotropic refinement Locality: Synthetic _database_code_amcsd 0011021 CELL PARAMETERS: 19.3690 19.3690 19.3690 90.000 90.000 90.000 SPACE GROUP: Fd3m X-RAY WAVELENGTH: 1.541838 Cell Volume: 7266.438 Density (g/cm3): 1.867 MAX. ABS. INTENSITY / VOLUME**2: 12.75445097 RIR: 2.224 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.91 26.39 11.1827 1 1 1 8 12.93 50.09 6.8480 2 2 0 12 15.17 100.00 5.8400 3 1 1 24 15.85 49.54 5.5913 2 2 2 8 18.32 22.56 4.8422 4 0 0 6 19.98 11.88 4.4436 3 3 1 24 22.49 16.91 3.9537 4 2 2 24 23.87 39.63 3.7276 5 1 1 24 23.87 11.88 3.7276 3 3 3 8 26.02 18.54 3.4240 4 4 0 12 27.24 54.72 3.2740 5 3 1 48 27.63 4.11 3.2282 4 4 2 24 29.16 9.60 3.0625 6 2 0 24 30.26 6.81 2.9537 5 3 3 24 33.03 1.43 2.7122 5 5 1 24 35.60 4.95 2.5216 7 3 1 48 35.60 2.28 2.5216 5 5 3 24 38.03 7.19 2.3663 7 3 3 24 39.48 8.61 2.2827 8 2 2 24 39.48 6.27 2.2827 6 6 0 12 40.33 1.05 2.2365 7 5 1 48 40.33 2.34 2.2365 5 5 5 8 41.71 1.42 2.1655 8 4 0 24 45.91 1.16 1.9768 8 4 4 24 46.66 1.67 1.9467 7 7 1 24 46.66 1.07 1.9467 9 3 3 24 48.87 1.63 1.8638 6 6 6 8 48.87 3.45 1.8638 10 2 2 24 50.53 2.50 1.8062 9 5 3 48 51.70 3.00 1.7681 10 4 2 48 54.42 1.46 1.6859 8 8 2 24 55.31 1.91 1.6609 10 6 0 24 57.06 1.79 1.6141 8 8 4 24 57.71 3.40 1.5975 11 5 1 48 58.77 1.57 1.5710 12 2 2 24 58.77 2.63 1.5710 10 6 4 48 59.41 1.47 1.5558 9 7 5 48 63.74 1.03 1.4600 12 4 4 24 65.95 2.74 1.4164 13 3 3 24 66.94 1.65 1.3978 8 8 8 8 67.53 1.10 1.3870 11 7 5 48 68.51 2.74 1.3696 10 10 0 12 69.09 1.50 1.3594 13 5 3 48 79.67 1.07 1.2035 13 9 3 48 80.59 1.30 1.1921 14 8 2 48 82.06 1.49 1.1744 16 4 0 24 82.06 1.30 1.1744 12 8 8 24 82.61 1.33 1.1680 15 5 5 24 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.