RbCu2(SO4)2(OH)(H2O) Chevrier G, Giester G, Zemann J Zeitschrift fur Kristallographie 206 (1993) 7-14 Neutron refinements of NaCu2(H3O2)(SO4)2 and RbCu2(H3O2)(SeO4)2: Variation of the hydrogen bond system in the natrochalcite-type series Locality: synthetic _database_code_amcsd 0011041 CELL PARAMETERS: 9.2460 6.4830 7.9400 90.000 116.110 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 427.369 Density (g/cm3): 3.416 MAX. ABS. INTENSITY / VOLUME**2: 15.31612941 RIR: 1.460 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.41 40.20 7.1297 0 0 1 2 18.42 48.81 4.8167 -1 1 1 4 19.44 72.78 4.5661 -2 0 1 2 24.74 33.95 3.5981 -2 0 2 2 24.98 26.28 3.5649 0 0 2 2 26.33 80.25 3.3855 -1 1 2 4 27.52 4.92 3.2415 0 2 0 2 29.27 77.01 3.0508 2 0 1 2 30.29 100.00 2.9508 0 2 1 4 32.20 45.89 2.7797 -3 1 1 4 33.92 29.84 2.6432 -2 2 1 4 34.00 30.55 2.6368 -3 1 2 4 34.25 22.24 2.6184 -2 0 3 2 34.35 30.00 2.6106 1 1 2 4 35.12 30.03 2.5549 2 2 0 4 35.26 9.24 2.5453 3 1 0 4 37.34 66.63 2.4083 -2 2 2 4 39.47 4.11 2.2831 -4 0 2 2 39.93 11.54 2.2576 2 0 2 2 40.08 7.74 2.2497 -3 1 3 4 40.61 4.42 2.2216 2 2 1 4 42.26 5.36 2.1386 3 1 1 4 43.26 2.54 2.0913 1 3 0 4 43.61 14.41 2.0756 4 0 0 2 43.74 5.23 2.0697 -1 3 1 4 44.48 6.19 2.0369 -2 2 3 4 45.71 1.25 1.9849 -2 0 4 2 46.29 8.16 1.9613 1 1 3 4 47.43 21.68 1.9166 0 2 3 4 47.93 5.46 1.8980 -1 3 2 4 48.79 2.87 1.8666 -4 2 2 4 48.83 12.73 1.8651 -4 2 1 4 49.18 14.13 1.8526 2 2 2 4 50.75 19.23 1.7991 -4 0 4 2 50.95 1.03 1.7924 4 0 1 2 51.25 18.80 1.7824 0 0 4 2 51.40 1.13 1.7776 -5 1 2 4 51.69 13.36 1.7684 -3 3 1 4 51.91 1.46 1.7615 3 1 2 4 52.08 6.90 1.7560 2 0 3 2 52.22 35.07 1.7517 -4 2 3 4 52.34 4.86 1.7480 4 2 0 4 52.73 4.45 1.7360 -5 1 1 4 52.93 2.87 1.7299 -3 3 2 4 53.18 3.64 1.7224 1 3 2 4 53.82 4.72 1.7032 3 3 0 4 54.19 17.96 1.6927 -2 2 4 4 56.80 20.71 1.6207 0 4 0 2 57.27 1.73 1.6086 5 1 0 4 57.39 1.70 1.6056 -3 3 3 4 58.45 3.88 1.5789 -2 0 5 2 58.88 21.35 1.5686 4 2 1 4 59.91 6.45 1.5440 2 2 3 4 60.19 2.80 1.5373 -3 1 5 4 60.46 1.84 1.5312 -4 0 5 2 60.63 5.49 1.5274 -2 4 1 4 60.71 7.88 1.5254 4 0 2 2 60.86 8.11 1.5220 -6 0 3 2 62.31 5.22 1.4902 1 3 3 4 62.49 4.29 1.4862 -6 0 1 2 62.89 2.23 1.4778 -2 4 2 4 63.00 4.87 1.4754 0 4 2 4 63.45 6.28 1.4661 3 1 3 4 64.64 1.19 1.4418 -3 3 4 4 64.86 1.12 1.4375 -1 3 4 4 65.18 13.53 1.4313 2 4 1 4 66.55 4.26 1.4050 -5 1 5 4 67.38 14.69 1.3898 -6 2 2 4 67.67 3.04 1.3845 -4 2 5 4 67.71 3.67 1.3839 -5 3 1 4 68.03 5.30 1.3781 -2 4 3 4 69.59 3.00 1.3510 -6 2 1 4 71.04 3.07 1.3269 -6 0 5 2 71.37 2.37 1.3216 -4 4 2 4 71.57 2.46 1.3184 -6 2 4 4 71.68 1.17 1.3167 5 3 0 4 71.68 1.96 1.3166 2 4 2 4 72.40 4.34 1.3053 2 2 4 4 72.40 12.42 1.3052 0 2 5 4 72.46 1.44 1.3043 -2 0 6 2 72.97 5.66 1.2965 -3 1 6 4 74.24 4.01 1.2774 4 4 0 4 74.29 1.06 1.2767 -3 3 5 4 74.57 4.90 1.2726 6 2 0 4 75.53 1.80 1.2587 6 0 1 2 75.67 2.22 1.2568 -7 1 4 4 76.69 1.77 1.2427 3 1 4 4 77.25 4.78 1.2351 3 3 3 4 77.37 1.25 1.2335 -1 1 6 4 77.44 3.43 1.2325 -1 5 2 4 79.14 1.18 1.2102 4 2 3 4 79.15 2.58 1.2100 -2 2 6 4 79.61 6.43 1.2042 -4 4 4 4 80.02 6.89 1.1991 0 4 4 4 80.12 2.61 1.1979 -5 3 5 4 80.23 2.13 1.1965 2 0 5 2 80.36 1.65 1.1948 -3 5 1 4 80.68 2.17 1.1910 2 4 3 4 80.90 1.54 1.1883 0 0 6 2 81.36 2.21 1.1827 -3 5 2 4 81.56 2.24 1.1803 1 5 2 4 82.72 2.46 1.1667 7 1 0 4 85.95 2.53 1.1310 -2 4 5 4 86.18 2.27 1.1285 -3 3 6 4 86.53 4.88 1.1249 -6 2 6 4 87.90 4.65 1.1108 4 4 2 4 88.03 2.70 1.1095 -6 -4 3 4 89.77 1.07 1.0925 3 3 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.