Geschieberite Niinisto L, Toivonen J, Valkonen J Acta Chemica Scandinavica A33 (1979) 621-624 Uranyl(VI) compounds. II. The crystal structure of potassium uranyl sulfate dihydrate, K2UO2(SO4)2*2H2O Locality: synthetic _database_code_amcsd 0020637 CELL PARAMETERS: 13.8060 11.5770 7.2920 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 1165.495 Density (g/cm3): 3.309 MAX. ABS. INTENSITY / VOLUME**2: 53.76254533 RIR: 5.290 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.82 89.31 6.9030 2 0 0 2 14.36 10.63 6.1701 0 1 1 4 15.31 4.19 5.7885 0 2 0 2 15.73 100.00 5.6331 1 1 1 8 19.29 28.22 4.6003 2 1 1 8 20.02 38.33 4.4355 2 2 0 4 23.48 2.97 3.7895 2 2 1 8 24.13 36.54 3.6889 3 1 1 8 25.26 16.10 3.5251 1 0 2 4 25.81 6.62 3.4515 4 0 0 2 26.13 20.49 3.4108 0 3 1 4 26.93 26.68 3.3113 1 3 1 8 26.96 3.34 3.3076 4 1 0 4 27.67 2.07 3.2239 2 0 2 4 28.61 6.50 3.1197 4 0 1 4 28.94 24.76 3.0850 0 2 2 4 29.20 8.04 3.0579 2 3 1 8 29.66 7.60 3.0122 4 1 1 8 29.67 27.14 3.0108 1 2 2 8 30.15 20.38 2.9645 4 2 0 4 30.90 20.19 2.8942 0 4 0 2 31.30 5.72 2.8578 3 0 2 4 31.77 8.71 2.8166 2 2 2 8 32.61 6.87 2.7462 4 2 1 8 32.68 7.89 2.7402 3 3 1 8 33.58 7.77 2.6691 2 4 0 4 35.02 4.24 2.5625 3 2 2 8 35.62 9.83 2.5203 5 1 1 8 37.06 1.50 2.4261 4 3 1 8 37.82 11.20 2.3788 0 1 3 4 39.15 8.13 2.3010 6 0 0 2 39.16 3.37 2.3001 4 2 2 8 40.09 15.94 2.2490 2 1 3 8 40.32 11.08 2.2369 1 4 2 8 40.68 2.50 2.2177 4 4 0 4 41.00 2.76 2.2012 5 0 2 4 41.44 6.77 2.1792 1 5 1 8 41.90 2.56 2.1560 6 1 1 8 41.95 4.09 2.1537 2 4 2 8 42.10 2.54 2.1461 5 3 1 8 42.27 5.35 2.1383 6 2 0 4 42.41 1.28 2.1316 2 2 3 8 43.03 2.07 2.1020 4 3 2 8 43.03 7.44 2.1020 2 5 1 8 44.01 6.76 2.0575 5 2 2 8 44.03 4.86 2.0567 0 3 3 4 44.56 8.04 2.0335 3 4 2 8 45.59 6.08 1.9899 3 5 1 8 45.65 2.04 1.9873 4 0 3 4 46.05 14.18 1.9711 2 3 3 8 46.36 8.03 1.9587 4 1 3 8 47.10 3.15 1.9295 0 6 0 2 47.27 2.06 1.9228 4 5 0 4 47.68 1.89 1.9075 6 3 1 8 48.02 3.03 1.8947 4 4 2 8 48.43 1.62 1.8796 4 2 3 8 48.45 5.87 1.8786 7 1 1 8 48.99 4.89 1.8593 4 5 1 8 49.02 4.63 1.8583 2 6 0 4 49.41 2.51 1.8445 6 2 2 8 50.50 3.07 1.8073 1 0 4 4 50.68 3.72 1.8011 6 4 0 4 51.74 6.58 1.7668 4 3 3 8 52.21 5.20 1.7521 5 4 2 8 52.64 3.47 1.7388 0 2 4 4 52.77 1.93 1.7347 7 0 2 4 53.07 1.41 1.7257 8 0 0 2 53.09 3.91 1.7252 1 2 4 8 53.13 3.07 1.7239 5 5 1 8 53.68 4.25 1.7074 7 3 1 8 53.75 1.37 1.7054 0 6 2 4 54.19 6.54 1.6925 1 6 2 8 54.41 1.78 1.6861 2 2 4 8 54.48 3.06 1.6842 4 6 0 4 54.75 5.54 1.6765 0 5 3 4 55.27 2.37 1.6620 8 1 1 8 55.28 3.91 1.6617 7 2 2 8 55.50 1.21 1.6556 2 6 2 8 55.57 5.08 1.6539 6 1 3 8 55.57 4.27 1.6538 8 2 0 4 56.14 1.03 1.6383 4 4 3 8 56.49 4.70 1.6291 2 5 3 8 56.58 3.01 1.6266 3 2 4 8 57.03 1.90 1.6148 6 4 2 8 57.11 2.12 1.6129 0 7 1 4 57.53 3.42 1.6020 1 7 1 8 57.64 1.55 1.5991 3 6 2 8 57.90 1.95 1.5927 6 5 1 8 59.24 1.66 1.5598 8 0 2 4 59.53 1.21 1.5529 4 2 4 8 60.36 4.08 1.5334 6 3 3 8 60.38 2.14 1.5330 1 4 4 8 60.86 2.33 1.5221 3 7 1 8 61.49 2.63 1.5080 4 5 3 8 62.38 2.62 1.4887 9 1 1 8 62.41 2.59 1.4879 7 4 2 8 62.86 2.38 1.4785 6 6 0 4 63.19 2.14 1.4714 5 2 4 8 63.23 2.01 1.4706 7 5 1 8 63.62 1.19 1.4625 3 4 4 8 64.19 1.94 1.4510 5 6 2 8 64.38 1.09 1.4471 0 8 0 2 64.78 1.80 1.4391 1 1 5 8 65.95 1.70 1.4163 2 8 0 4 66.08 1.28 1.4139 9 0 2 4 66.88 2.16 1.3990 9 3 1 8 66.99 2.89 1.3969 8 1 3 8 67.22 1.38 1.3927 5 7 1 8 67.90 1.83 1.3803 3 1 5 8 68.29 1.24 1.3736 9 2 2 8 68.31 1.98 1.3731 8 4 2 8 69.09 3.07 1.3594 8 5 1 8 69.20 3.35 1.3576 1 3 5 8 69.35 2.40 1.3550 6 5 3 8 69.85 1.17 1.3466 5 4 4 8 70.07 1.15 1.3429 10 2 0 4 70.17 3.21 1.3413 2 7 3 8 70.32 1.15 1.3387 1 8 2 8 70.57 1.17 1.3346 4 8 0 4 71.34 5.52 1.3220 8 3 3 8 71.53 1.53 1.3190 1 6 4 8 72.23 1.69 1.3080 3 3 5 8 72.46 1.82 1.3043 7 2 4 8 73.33 1.05 1.2910 3 8 2 8 73.40 2.18 1.2900 7 6 2 8 73.64 1.75 1.2863 8 6 0 4 73.96 1.06 1.2816 5 1 5 8 74.66 2.66 1.2712 4 7 3 8 74.72 1.74 1.2704 9 4 2 8 75.34 1.59 1.2615 1 9 1 8 75.47 1.22 1.2596 9 5 1 8 75.92 1.03 1.2533 8 0 4 4 76.26 1.60 1.2486 7 7 1 8 78.00 1.01 1.2250 6 8 0 4 78.15 1.33 1.2231 5 3 5 8 78.28 1.12 1.2213 3 9 1 8 78.74 1.19 1.2153 0 0 6 2 79.22 1.04 1.2092 5 8 2 8 80.43 1.48 1.1941 10 1 3 8 80.60 1.50 1.1919 3 5 5 8 81.97 1.73 1.1755 6 7 3 8 82.25 1.63 1.1721 2 2 6 8 82.72 1.07 1.1667 7 1 5 8 84.16 1.09 1.1503 9 2 4 8 84.53 1.51 1.1463 10 3 3 8 85.06 1.13 1.1405 9 6 2 8 85.39 1.97 1.1369 0 9 3 4 86.07 1.20 1.1296 1 8 4 8 86.56 1.86 1.1245 4 2 6 8 86.80 1.52 1.1220 7 3 5 8 86.82 1.82 1.1218 2 9 3 8 86.94 1.64 1.1206 0 4 6 4 87.82 1.04 1.1115 9 7 1 8 88.37 1.72 1.1061 2 4 6 8 88.93 1.18 1.1005 3 8 4 8 89.00 1.21 1.0999 1 10 2 8 89.19 1.01 1.0980 11 4 2 8 89.98 1.25 1.0904 1 7 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.