data_global
_chemical_name_mineral 'Sayrite'
loop_
_publ_author_name
'Piret P'
'Deliens M'
'Piret-Meunier J'
'Germain G'
_journal_name_full 'Bulletin de Mineralogie'
_journal_volume 106 
_journal_year 1983
_journal_page_first 299
_journal_page_last 304
_publ_section_title
;
 La sayrite, Pb2[(UO2)5O6(OH)2]*4H2O, nouveau mineral; proprietes et structure cristalline
;
_database_code_amcsd 0012080
_chemical_compound_source 'Shinkolobwe, Shaba, Zaire'
_chemical_formula_sum 'Pb2 U5 O22 H10'
_cell_length_a 10.704
_cell_length_b 6.960
_cell_length_c 14.533
_cell_angle_alpha 90
_cell_angle_beta 116.81
_cell_angle_gamma 90
_cell_volume 966.323
_exptl_crystal_density_diffrn      6.759
_symmetry_space_group_name_H-M 'P 1 21/c 1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  'x,1/2-y,1/2+z'
  '-x,1/2+y,1/2-z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pb   0.28170   0.14730   0.89580   0.00410
U1   0.17910   0.04780   0.60420   0.00050
U2   0.42270   0.04160   0.21740   0.00130
U3   0.00000   0.00000   0.00000   0.00010
O5   0.13000   0.99900   0.70900   0.00440
O6   0.23800   0.09600   0.50900   0.00260
O7   0.40900   0.99700   0.33400   0.00920
O8   0.44500   0.08500   0.10100   0.00120
O9   0.09100   0.03100   0.91800   0.00070
O10   0.18700   0.10800   0.12300   0.00100
O11   0.38600   0.35600   0.23000   0.00010
O-H12   0.65600   0.22000   0.34700   0.00430
O13   0.96400   0.18200   0.49500   0.00830
Wat14   0.12100   0.42700   0.79500   0.02220
Wat15   0.69500   0.26400   0.56500   0.00270