Sayrite Piret P, Deliens M, Piret-Meunier J, Germain G Bulletin de Mineralogie 106 (1983) 299-304 La sayrite, Pb2[(UO2)5O6(OH)2]*4H2O, nouveau mineral; proprietes et structure cristalline Locality: Shinkolobwe, Shaba, Zaire _database_code_amcsd 0012080 CELL PARAMETERS: 10.7040 6.9600 14.5330 90.000 116.810 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 966.323 Density (g/cm3): 6.781 MAX. ABS. INTENSITY / VOLUME**2: 126.7208236 RIR: 6.085 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.57 100.00 7.0407 -1 0 2 2 14.44 6.06 6.1329 0 1 1 4 15.41 9.94 5.7482 -1 1 1 4 15.75 51.31 5.6254 1 1 0 4 17.40 1.27 5.0975 -2 0 2 2 18.58 2.71 4.7767 2 0 0 2 18.70 1.55 4.7448 0 1 2 4 18.79 2.39 4.7233 1 1 1 4 19.71 18.75 4.5042 1 0 2 2 21.00 3.16 4.2312 -2 1 1 4 21.61 1.46 4.1125 -2 1 2 4 22.36 4.13 3.9760 -1 1 3 4 24.26 1.03 3.6690 -2 1 3 4 24.69 2.78 3.6052 -1 0 4 2 24.98 15.21 3.5644 -3 0 2 2 25.30 79.62 3.5204 -2 0 4 2 25.60 29.63 3.4800 0 2 0 2 25.97 46.65 3.4305 2 1 1 4 27.07 6.20 3.2934 -1 2 1 4 27.51 1.13 3.2427 0 0 4 2 27.74 7.55 3.2154 2 0 2 2 27.87 9.87 3.2012 -1 1 4 4 28.61 56.37 3.1197 -1 2 2 4 28.70 79.45 3.1105 -3 1 1 4 29.12 1.16 3.0663 -3 0 4 2 29.20 77.41 3.0580 1 1 3 4 30.63 3.95 2.9190 2 1 2 4 30.68 23.13 2.9138 -2 2 1 4 31.66 1.86 2.8263 -1 2 3 4 31.81 5.20 2.8127 2 2 0 4 31.89 7.41 2.8061 -3 1 4 4 33.04 18.70 2.7110 0 2 3 4 33.56 1.77 2.6700 -2 1 5 4 33.63 2.29 2.6646 -4 0 2 2 34.00 1.47 2.6371 -1 1 5 4 35.43 1.15 2.5333 1 1 4 4 36.09 2.54 2.4884 -4 1 2 4 36.16 9.36 2.4838 -4 1 3 4 36.30 12.90 2.4749 -2 2 4 4 36.98 8.82 2.4308 0 1 5 4 37.93 1.59 2.3724 0 2 4 4 38.31 3.63 2.3493 3 2 0 4 38.32 2.24 2.3488 -1 0 6 2 38.35 5.64 2.3469 -3 0 6 2 38.92 6.97 2.3143 3 1 2 4 39.85 3.66 2.2622 -1 3 1 4 39.99 13.24 2.2545 1 3 0 4 40.04 1.96 2.2521 2 0 4 2 40.22 2.04 2.2419 -4 1 5 4 41.33 2.46 2.1844 0 3 2 4 41.78 2.60 2.1618 0 0 6 2 42.17 1.83 2.1430 1 2 4 4 42.46 3.52 2.1292 -3 2 5 4 42.76 7.27 2.1149 2 2 3 4 42.83 1.45 2.1116 -2 3 2 4 42.89 1.99 2.1087 -5 0 2 2 43.24 3.07 2.0924 -1 3 3 4 43.50 8.04 2.0806 4 1 1 4 43.85 1.08 2.0645 0 1 6 4 43.86 5.52 2.0641 -4 2 1 4 44.04 2.36 2.0563 -4 2 4 4 44.31 2.15 2.0443 0 3 3 4 44.92 3.08 2.0181 -5 1 2 4 45.36 25.23 1.9995 2 3 1 4 45.63 1.36 1.9880 -2 2 6 4 46.04 16.64 1.9713 4 0 2 2 46.38 5.83 1.9578 -4 2 5 4 46.40 19.81 1.9568 -5 1 5 4 46.55 5.54 1.9509 -1 3 4 4 46.68 14.29 1.9458 -3 2 6 4 47.09 3.26 1.9298 -3 3 1 4 47.18 4.51 1.9263 -5 0 6 2 47.40 20.91 1.9178 -1 1 7 4 47.42 3.06 1.9171 1 3 3 4 47.45 1.40 1.9161 -3 3 3 4 47.59 2.19 1.9107 5 0 0 2 48.25 2.23 1.8862 3 0 4 2 48.68 3.42 1.8703 2 1 5 4 48.99 3.65 1.8593 1 1 6 4 49.25 4.86 1.8501 -3 3 4 4 49.70 1.01 1.8345 -4 2 6 4 50.34 1.84 1.8128 -3 0 8 2 51.34 5.95 1.7797 -2 2 7 4 51.95 12.29 1.7602 -4 0 8 2 52.04 1.22 1.7574 -3 3 5 4 52.14 1.98 1.7543 -3 1 8 4 52.28 1.83 1.7497 -4 3 2 4 52.34 12.61 1.7481 -4 3 3 4 52.65 7.70 1.7385 -6 0 2 2 52.95 12.69 1.7293 0 3 5 4 53.15 1.32 1.7231 4 1 3 4 53.16 2.84 1.7228 5 1 1 4 53.22 5.53 1.7212 -6 1 3 4 53.42 5.62 1.7152 4 2 2 4 53.86 7.92 1.7021 2 0 6 2 54.31 7.00 1.6892 -1 4 2 4 54.42 6.33 1.6858 3 3 2 4 54.64 7.13 1.6796 1 4 1 4 54.81 7.41 1.6748 5 2 0 4 55.20 2.40 1.6641 4 3 0 4 55.41 7.58 1.6583 3 2 4 4 55.56 2.52 1.6541 -2 4 1 4 55.68 1.23 1.6507 -6 1 6 4 56.24 2.83 1.6356 0 2 7 4 56.27 2.55 1.6349 2 4 0 4 56.51 1.69 1.6286 3 1 5 4 56.78 1.55 1.6214 0 0 8 2 56.99 1.92 1.6159 2 3 4 4 57.06 1.66 1.6142 -5 1 8 4 57.06 2.43 1.6142 0 4 3 4 57.07 1.12 1.6139 -2 4 3 4 57.65 1.01 1.5990 5 1 2 4 58.27 2.13 1.5834 5 2 1 4 58.41 4.15 1.5800 -6 1 7 4 58.63 3.64 1.5744 3 3 3 4 58.69 1.53 1.5730 -3 1 9 4 58.79 5.07 1.5707 -4 2 8 4 58.94 2.13 1.5671 -6 2 5 4 59.21 3.66 1.5604 -5 3 2 4 59.43 2.80 1.5552 -6 2 2 4 59.55 3.97 1.5525 -2 1 9 4 59.70 4.55 1.5488 -3 4 3 4 60.17 1.50 1.5380 -3 3 7 4 60.37 1.62 1.5332 0 4 4 4 60.44 1.39 1.5316 -5 3 5 4 60.56 3.22 1.5290 2 2 6 4 60.67 3.83 1.5263 -5 3 1 4 61.28 1.26 1.5127 -1 3 7 4 61.43 1.04 1.5093 3 2 5 4 61.91 1.73 1.4989 -7 0 6 2 62.55 4.25 1.4850 -1 4 5 4 62.62 3.60 1.4835 1 3 6 4 62.80 1.75 1.4798 3 4 1 4 64.89 1.62 1.4371 -4 4 4 4 65.33 1.61 1.4284 -3 3 8 4 66.11 1.00 1.4133 -6 3 4 4 66.32 1.78 1.4094 -6 1 9 4 66.66 1.24 1.4030 -6 2 8 4 66.84 1.67 1.3998 -5 2 9 4 66.86 3.62 1.3993 -7 2 4 4 66.95 4.29 1.3977 -3 4 6 4 67.15 1.75 1.3940 5 0 4 2 67.55 2.05 1.3866 -7 2 3 4 68.01 1.18 1.3785 1 4 5 4 68.04 1.75 1.3780 6 2 1 4 68.44 1.88 1.3708 -6 3 6 4 68.44 3.67 1.3708 1 2 8 4 68.79 2.57 1.3648 7 0 0 2 68.94 1.90 1.3621 1 3 7 4 69.00 4.22 1.3610 0 5 2 4 69.66 1.45 1.3497 -5 3 8 4 69.89 1.74 1.3459 4 2 5 4 69.97 1.34 1.3445 -1 1 10 4 70.07 4.07 1.3428 -2 5 2 4 70.72 1.01 1.3322 -2 4 7 4 70.85 1.55 1.3300 -6 2 9 4 70.88 4.79 1.3295 -6 3 7 4 70.88 2.72 1.3295 -8 0 6 2 71.80 1.41 1.3147 1 1 9 4 71.91 5.04 1.3130 -2 3 9 4 71.93 4.39 1.3127 -7 1 9 4 72.40 2.90 1.3053 -5 2 10 4 72.49 1.70 1.3039 6 2 2 4 72.84 1.02 1.2986 -4 4 7 4 72.93 3.29 1.2971 0 0 10 2 73.21 4.81 1.2929 -3 1 11 4 73.31 1.08 1.2914 6 1 3 4 73.63 1.95 1.2865 5 4 0 4 73.72 3.18 1.2852 -8 1 7 4 74.14 2.18 1.2789 3 4 4 4 74.36 2.51 1.2757 7 1 1 4 74.37 1.73 1.2755 3 5 0 4 74.40 1.03 1.2750 -1 2 10 4 74.50 2.54 1.2736 -7 3 5 4 74.87 1.26 1.2683 -7 0 10 2 75.11 3.08 1.2648 5 1 5 4 75.52 1.22 1.2590 -7 3 6 4 76.20 1.89 1.2493 -5 4 7 4 76.74 1.34 1.2419 -8 2 6 4 77.23 1.18 1.2353 4 3 5 4 77.33 1.79 1.2339 -4 2 11 4 78.73 1.74 1.2154 0 2 10 4 79.32 1.11 1.2078 -2 2 11 4 79.40 2.59 1.2069 -2 5 6 4 79.43 1.12 1.2065 -6 4 1 4 79.72 1.91 1.2029 -8 2 2 4 79.74 3.96 1.2026 4 5 0 4 81.25 4.11 1.1841 2 5 4 4 81.28 1.96 1.1836 -3 4 9 4 81.60 1.53 1.1799 -1 3 10 4 82.44 2.28 1.1699 -4 5 6 4 83.01 1.41 1.1634 2 2 9 4 83.05 2.02 1.1629 -5 5 4 4 84.16 1.16 1.1503 -6 4 8 4 84.78 1.86 1.1435 6 3 3 4 84.93 2.33 1.1419 5 4 3 4 84.96 2.85 1.1416 1 6 1 4 85.44 1.37 1.1364 6 4 1 4 85.81 1.76 1.1324 1 4 8 4 87.00 2.11 1.1200 3 1 9 4 87.17 1.29 1.1182 4 4 5 4 89.21 2.38 1.0978 -3 6 3 4 89.29 1.30 1.0971 1 1 11 4 89.54 1.73 1.0946 -5 4 10 4 89.63 1.35 1.0938 6 4 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.