Dumontite Piret P, Piret-Meunier J Bulletin de Mineralogie 111 (1988) 439-442 Nouvelle determination de la structure cristalline de la dumonite Pb2[(UO2)3O2(PO4)2]*5H2O Locality: Shinkolobwe, Shaba, Zaire _database_code_amcsd 0012090 CELL PARAMETERS: 8.1180 16.8190 6.9830 90.000 109.030 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 901.328 Density (g/cm3): 5.624 MAX. ABS. INTENSITY / VOLUME**2: 63.53969210 RIR: 3.679 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.52 17.72 8.4095 0 2 0 2 11.53 41.56 7.6743 1 0 0 2 12.68 57.12 6.9819 1 1 0 4 13.41 15.63 6.6014 0 0 1 2 14.41 47.39 6.1450 0 1 1 4 14.57 29.02 6.0797 -1 0 1 2 15.63 46.21 5.6687 1 2 0 4 18.00 1.38 4.9270 -1 2 1 4 19.61 2.02 4.5270 1 3 0 4 20.41 5.18 4.3520 1 0 1 2 20.79 97.96 4.2732 0 3 1 4 21.09 3.12 4.2132 1 1 1 4 21.13 32.49 4.2048 0 4 0 2 21.56 5.72 4.1215 -1 3 1 4 22.69 18.85 3.9187 -2 0 1 2 23.01 1.06 3.8651 1 2 1 4 23.18 36.96 3.8372 2 0 0 2 23.31 4.45 3.8165 -2 1 1 4 23.78 100.00 3.7410 2 1 0 4 24.13 5.23 3.6875 1 4 0 4 25.07 3.29 3.5520 -2 2 1 4 25.67 59.10 3.4705 -1 0 2 2 25.76 1.10 3.4582 -1 4 1 4 25.92 1.44 3.4378 1 3 1 4 26.22 7.61 3.3989 -1 1 2 4 27.01 33.68 3.3007 0 0 2 2 27.54 1.62 3.2389 0 1 2 4 27.78 10.99 3.2119 -2 3 1 4 27.81 3.50 3.2081 -1 2 2 4 28.18 9.16 3.1665 2 3 0 4 29.06 6.13 3.0725 0 2 2 4 29.38 10.28 3.0398 -2 0 2 2 29.54 36.26 3.0239 1 4 1 4 29.81 59.31 2.9971 0 5 1 4 29.87 26.50 2.9914 -2 1 2 4 30.29 12.13 2.9509 -1 3 2 4 30.37 56.96 2.9433 -1 5 1 4 31.00 8.11 2.8850 2 1 1 4 31.20 48.60 2.8667 -2 4 1 4 31.29 6.10 2.8588 -2 2 2 4 31.45 9.88 2.8443 0 3 2 4 31.57 13.72 2.8343 2 4 0 4 31.93 2.98 2.8032 0 6 0 2 33.18 1.68 2.7003 -3 0 1 2 33.29 31.10 2.6914 1 1 2 4 33.48 2.09 2.6766 -1 4 2 4 33.53 6.84 2.6723 -2 3 2 4 33.68 9.54 2.6615 1 5 1 4 34.05 5.19 2.6330 1 6 0 4 34.55 3.87 2.5963 0 4 2 4 34.56 10.98 2.5957 2 3 1 4 34.58 1.04 2.5937 1 2 2 4 34.77 5.41 2.5802 0 6 1 4 35.08 3.03 2.5581 3 0 0 2 35.16 7.60 2.5524 -2 5 1 4 35.26 8.35 2.5456 -1 6 1 4 35.50 9.46 2.5290 3 1 0 4 36.65 9.34 2.4520 1 3 2 4 36.77 6.67 2.4443 -3 0 2 2 37.17 3.38 2.4189 -3 1 2 4 37.42 9.22 2.4031 2 4 1 4 38.19 5.22 2.3566 1 6 1 4 38.69 3.07 2.3273 3 3 0 4 38.72 2.34 2.3257 -1 0 3 2 39.10 5.79 2.3037 -1 1 3 4 39.67 1.80 2.2721 -3 4 1 4 39.83 1.22 2.2635 2 6 0 4 40.25 2.57 2.2406 -3 3 2 4 40.36 7.55 2.2345 -1 7 1 4 40.41 1.05 2.2319 -2 1 3 4 40.86 1.05 2.2087 2 5 1 4 41.31 1.55 2.1854 3 4 0 4 41.50 1.01 2.1760 2 0 2 2 41.86 5.48 2.1580 2 1 2 4 42.06 25.30 2.1482 -1 3 3 4 42.18 1.20 2.1422 3 1 1 4 42.69 1.04 2.1181 1 5 2 4 42.79 5.10 2.1132 -3 4 2 4 43.00 11.29 2.1034 1 7 1 4 43.02 14.22 2.1024 0 8 0 2 43.94 1.35 2.0607 -2 6 2 4 44.49 7.41 2.0364 2 7 0 4 44.52 7.47 2.0351 -1 4 3 4 44.67 2.13 2.0286 2 3 2 4 44.68 7.15 2.0281 -4 0 1 2 44.69 2.89 2.0277 1 8 0 4 44.75 8.32 2.0250 2 6 1 4 44.98 7.33 2.0154 3 3 1 4 45.06 3.64 2.0120 -3 1 3 4 45.70 4.68 1.9851 -2 4 3 4 45.94 4.10 1.9755 -1 7 2 4 46.34 2.03 1.9594 -4 0 2 2 46.49 5.69 1.9532 1 0 3 2 46.58 1.74 1.9496 0 4 3 4 46.67 14.43 1.9462 -4 1 2 4 46.71 19.34 1.9448 -3 6 1 4 46.76 2.30 1.9425 0 7 2 4 47.02 1.92 1.9325 2 4 2 4 47.32 6.81 1.9212 3 4 1 4 47.38 3.47 1.9186 4 0 0 2 47.53 21.25 1.9130 -1 5 3 4 47.69 2.38 1.9071 -4 3 1 4 47.71 16.59 1.9062 4 1 0 4 47.72 11.56 1.9059 -3 3 3 4 47.81 1.87 1.9026 1 2 3 4 48.16 1.69 1.8896 3 6 0 4 48.28 5.17 1.8850 -2 7 2 4 48.66 12.37 1.8712 -2 5 3 4 48.68 2.19 1.8705 4 2 0 4 49.04 3.82 1.8575 2 7 1 4 49.18 2.20 1.8526 -2 8 1 4 49.43 3.75 1.8438 2 8 0 4 49.50 4.79 1.8415 0 5 3 4 49.93 18.48 1.8267 -4 4 1 4 49.96 6.22 1.8256 -3 4 3 4 50.20 3.46 1.8174 3 5 1 4 50.25 4.64 1.8157 1 9 0 4 50.26 3.64 1.8152 4 3 0 4 50.64 5.28 1.8027 1 7 2 4 50.77 6.99 1.7982 -1 8 2 4 51.14 1.81 1.7863 -1 9 1 4 51.45 1.63 1.7760 -4 4 2 4 51.54 4.83 1.7732 0 8 2 4 51.60 20.10 1.7714 1 4 3 4 51.87 7.02 1.7627 3 0 2 2 52.17 6.29 1.7531 3 1 2 4 52.70 2.03 1.7368 -4 5 1 4 52.73 5.21 1.7359 -3 5 3 4 52.75 2.15 1.7353 -2 0 4 2 52.80 10.12 1.7338 -1 0 4 2 52.90 7.30 1.7309 0 6 3 4 52.95 1.69 1.7291 -2 8 2 4 53.10 2.10 1.7247 -1 1 4 4 53.35 2.00 1.7172 1 9 1 4 53.56 6.49 1.7109 3 6 1 4 53.94 1.74 1.6998 4 0 1 2 53.95 2.43 1.6995 -2 2 4 4 54.17 1.07 1.6931 -4 5 2 4 54.56 1.32 1.6819 0 10 0 2 54.63 4.99 1.6801 2 9 0 4 54.73 1.46 1.6771 -4 3 3 4 55.11 1.65 1.6666 4 5 0 4 55.56 6.62 1.6541 -3 0 4 2 55.85 3.21 1.6461 -3 1 4 4 55.97 3.70 1.6430 -2 7 3 4 55.97 12.42 1.6429 1 10 0 4 55.99 3.46 1.6425 0 1 4 4 55.99 2.67 1.6423 -3 6 3 4 56.46 1.33 1.6298 0 10 1 4 56.60 4.64 1.6262 0 9 2 4 56.62 2.30 1.6256 3 4 2 4 56.73 1.49 1.6228 0 7 3 4 56.77 5.13 1.6216 -4 4 3 4 56.79 1.86 1.6210 -1 10 1 4 57.38 1.38 1.6059 -4 6 2 4 57.49 3.59 1.6029 -1 4 4 4 57.51 1.27 1.6025 1 6 3 4 57.65 2.58 1.5991 -5 1 2 4 57.85 1.90 1.5939 -3 8 2 4 57.93 1.01 1.5920 -2 9 2 4 58.50 1.56 1.5778 -5 2 2 4 58.58 4.39 1.5759 4 4 1 4 59.02 1.06 1.5651 2 4 3 4 59.84 1.08 1.5456 -2 10 1 4 60.02 2.41 1.5415 1 9 2 4 60.11 1.87 1.5393 -3 4 4 4 60.30 3.80 1.5349 5 0 0 2 61.02 1.40 1.5185 -4 7 2 4 61.08 4.27 1.5171 4 5 1 4 61.23 1.30 1.5138 -4 1 4 4 61.24 4.92 1.5135 -1 10 2 4 61.35 1.63 1.5111 -5 0 3 2 61.40 1.01 1.5099 5 2 0 4 61.44 7.19 1.5090 3 9 0 4 61.45 5.07 1.5090 1 1 4 4 61.51 1.29 1.5075 2 5 3 4 61.83 1.04 1.5006 -5 4 2 4 61.89 3.66 1.4993 4 7 0 4 61.92 3.24 1.4986 0 10 2 4 62.21 1.02 1.4922 3 6 2 4 62.34 1.09 1.4896 0 11 1 4 62.36 4.10 1.4891 -4 6 3 4 62.57 4.55 1.4846 -3 9 2 4 63.00 1.11 1.4754 -2 6 4 4 63.18 6.18 1.4717 -2 10 2 4 63.76 1.48 1.4596 -4 8 1 4 63.92 4.38 1.4564 -5 5 1 4 64.20 1.96 1.4507 3 0 3 2 64.49 5.25 1.4450 2 6 3 4 64.61 1.56 1.4425 4 2 2 4 65.17 1.80 1.4315 1 10 2 4 65.20 1.19 1.4310 1 8 3 4 65.37 2.14 1.4276 -3 10 1 4 65.65 1.06 1.4222 0 6 4 4 65.65 7.59 1.4221 -5 4 3 4 65.84 1.16 1.4186 -4 7 3 4 65.88 5.10 1.4177 2 9 2 4 66.59 2.96 1.4044 3 3 3 4 66.83 2.24 1.3998 -5 6 1 4 67.50 2.21 1.3877 4 7 1 4 67.51 2.57 1.3874 0 11 2 4 68.41 4.47 1.3713 3 4 3 4 68.85 5.63 1.3637 -5 1 4 4 68.87 2.07 1.3633 2 0 4 2 69.28 3.10 1.3563 5 3 1 4 69.51 3.33 1.3523 -4 9 2 4 69.60 1.57 1.3508 3 8 2 4 69.64 4.67 1.3502 -6 0 2 2 70.20 1.27 1.3408 -5 7 1 4 70.32 2.03 1.3387 4 9 0 4 70.33 2.00 1.3386 -1 3 5 4 70.39 3.45 1.3376 -1 8 4 4 70.72 4.24 1.3321 3 5 3 4 70.81 1.22 1.3307 2 10 2 4 70.84 1.24 1.3302 -5 6 3 4 70.84 1.36 1.3301 -3 3 5 4 70.90 1.26 1.3292 -5 3 4 4 71.15 1.64 1.3252 -2 4 5 4 71.95 2.88 1.3124 3 11 0 4 72.53 3.17 1.3032 -6 3 1 4 72.62 1.84 1.3019 -3 4 5 4 72.74 2.08 1.3000 -3 8 4 4 72.98 2.66 1.2963 -3 11 2 4 73.34 3.94 1.2908 5 5 1 4 73.42 3.11 1.2896 -2 5 5 4 73.70 1.20 1.2855 -6 4 2 4 73.91 1.76 1.2823 3 9 2 4 73.96 1.16 1.2816 1 7 4 4 74.12 1.20 1.2792 -5 7 3 4 74.13 2.18 1.2791 6 0 0 2 74.37 1.87 1.2755 -1 5 5 4 74.60 2.47 1.2722 -6 3 3 4 74.68 1.02 1.2710 -1 9 4 4 74.88 3.41 1.2682 -3 5 5 4 75.07 3.23 1.2654 -1 13 1 4 75.11 2.63 1.2647 4 10 0 4 75.47 2.96 1.2596 0 4 5 4 76.08 2.49 1.2510 2 11 2 4 76.51 3.00 1.2452 5 0 2 2 76.53 2.98 1.2448 -6 5 1 4 76.87 2.24 1.2401 1 13 1 4 76.91 1.81 1.2397 5 8 0 4 77.10 2.60 1.2370 0 9 4 4 77.11 2.13 1.2370 -1 6 5 4 78.52 2.00 1.2182 -5 9 2 4 78.56 1.04 1.2177 3 0 4 2 78.56 2.95 1.2177 -6 5 3 4 78.69 1.03 1.2160 -4 5 5 4 79.33 6.00 1.2077 -2 10 4 4 80.44 1.79 1.1939 5 4 2 4 80.69 1.04 1.1908 2 10 3 4 80.84 1.56 1.1890 -5 7 4 4 81.01 1.60 1.1869 1 14 0 4 81.13 1.55 1.1855 1 4 5 4 81.25 1.03 1.1840 -6 6 3 4 81.38 2.05 1.1825 -4 6 5 4 81.66 2.48 1.1792 -4 9 4 4 81.71 1.31 1.1786 -1 14 1 4 81.76 2.00 1.1780 0 10 4 4 81.78 2.56 1.1777 4 5 3 4 81.85 1.69 1.1769 1 9 4 4 82.60 4.13 1.1681 -5 4 5 4 82.85 1.08 1.1652 -5 10 1 4 83.05 1.57 1.1628 -2 0 6 2 83.16 3.56 1.1616 -5 10 2 4 83.30 1.80 1.1601 -2 1 6 4 83.58 1.11 1.1568 -3 0 6 2 85.47 1.91 1.1361 -6 8 2 4 85.68 1.94 1.1337 5 10 0 4 85.98 1.11 1.1306 1 6 5 4 86.42 2.00 1.1259 -4 0 6 2 86.82 2.91 1.1218 -2 13 3 4 86.84 1.18 1.1216 0 11 4 4 87.17 1.08 1.1182 6 5 1 4 87.33 1.82 1.1165 2 3 5 4 87.46 1.15 1.1153 0 13 3 4 87.83 2.14 1.1115 2 14 1 4 88.44 1.04 1.1054 0 15 1 4 88.55 4.22 1.1044 4 10 2 4 88.59 1.44 1.1040 -5 9 4 4 88.72 2.28 1.1027 -1 15 1 4 88.85 1.88 1.1014 2 9 4 4 89.21 2.83 1.0979 0 1 6 4 89.23 2.19 1.0976 -3 -14 1 4 89.61 1.61 1.0940 7 1 0 4 89.74 1.33 1.0927 6 8 0 4 89.82 1.35 1.0919 -7 0 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.