H4 N Ni O9 P3 Tordjman I, Tranqui D, Durif A, Averbuch M Bulletin de la Societe Francaise de Mineralogie et de Cristallographie 91 (1968) 242-246 Structure cristalline du metaphosphate de nickel-ammonium rhomboedrique Ni N H4 (P O3)3. Donnees cristallographique sur les metaphosphates rhomboedriques du type M^II^ N H4 (P O3)3 (M^II^ = Ni,Co,Mg) _cod_database_code 1007049 _database_code_amcsd 0012128 CELL PARAMETERS: 10.1300 10.1300 7.0980 90.000 90.000 120.000 SPACE GROUP: R32 X-RAY WAVELENGTH: 1.541838 Cell Volume: 630.791 Density (g/cm3): 2.445 MAX. ABS. INTENSITY / VOLUME**2: 27.55088757 RIR: 3.669 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.06 100.00 5.5181 1 0 1 6 17.51 73.14 5.0650 1 1 0 3 23.85 7.61 3.7314 0 2 1 6 29.74 28.59 3.0042 2 1 1 6 30.57 14.97 2.9243 3 0 0 6 32.45 47.43 2.7590 2 0 2 6 35.45 7.22 2.5325 2 2 0 3 37.11 9.09 2.4229 1 2 2 6 38.03 2.10 2.3660 0 0 3 2 39.14 5.89 2.3017 1 3 1 6 42.15 2.81 2.1437 1 1 3 6 43.17 2.52 2.0955 4 0 1 6 45.18 15.68 2.0068 3 1 2 6 46.92 3.55 1.9363 3 2 1 6 49.56 5.69 1.8394 0 3 3 6 49.56 4.30 1.8394 3 0 3 6 52.25 5.68 1.7507 2 3 2 6 54.34 5.98 1.6883 3 3 0 3 55.89 7.95 1.6450 0 2 4 6 57.05 2.48 1.6145 2 4 1 6 58.70 7.38 1.5729 5 0 2 6 59.04 1.63 1.5645 2 1 4 6 60.16 3.95 1.5382 5 1 1 6 61.76 1.62 1.5021 4 2 2 6 62.40 3.27 1.4882 1 4 3 6 62.40 2.90 1.4882 4 1 3 6 64.73 1.31 1.4401 1 5 2 6 65.06 3.89 1.4337 1 3 4 6 66.57 6.63 1.4048 5 2 0 6 66.75 1.67 1.4014 0 1 5 6 68.24 2.67 1.3743 3 3 3 6 70.79 2.01 1.3310 3 2 4 6 71.80 1.98 1.3147 1 6 1 6 72.42 1.37 1.3050 1 2 5 6 76.33 2.74 1.2477 0 5 4 6 76.60 1.33 1.2438 0 6 3 6 76.60 1.52 1.2438 6 0 3 6 77.31 1.98 1.2342 3 5 1 6 77.31 1.21 1.2342 7 0 1 6 80.02 1.62 1.1991 6 2 1 6 81.33 1.65 1.1830 0 0 6 2 81.44 3.47 1.1817 0 7 2 6 87.34 1.13 1.1164 4 4 3 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.