Ba H8 N4 O4 Pd de Rassenfosse A, Pierard J Bulletin de la Societe Royal des Sciences de Liege 4 (1935) 74-79 Etude cristallographique du palladocyanure de baryum. BaPd(CN)4(H2O)4 _cod_database_code 1010798 _database_code_amcsd 0017539 CELL PARAMETERS: 11.9500 13.8200 6.7100 90.000 103.630 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1076.942 Density (g/cm3): 1.503 MAX. ABS. INTENSITY / VOLUME**2: 27.51097835 RIR: 5.960 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.95 2.51 8.8910 1 1 0 4 12.81 30.91 6.9100 0 2 0 2 15.26 100.00 5.8067 2 0 0 2 15.33 29.03 5.7790 -1 1 1 4 18.27 19.26 4.8570 1 1 1 4 18.71 36.36 4.7426 0 2 1 4 19.97 22.48 4.4455 2 2 0 4 20.74 68.75 4.2821 1 3 0 4 22.07 24.26 4.0268 -2 2 1 4 23.85 9.98 3.7312 -1 3 1 4 24.67 9.15 3.6082 -3 1 1 4 25.86 8.09 3.4447 1 3 1 4 26.22 15.62 3.3989 2 2 1 4 27.38 33.89 3.2570 -1 1 2 4 30.15 26.07 2.9637 3 3 0 4 30.20 5.33 2.9598 3 1 1 4 30.31 7.68 2.9487 0 2 2 4 30.80 17.34 2.9034 4 0 0 2 30.81 5.05 2.9025 -3 3 1 4 30.87 24.43 2.8969 1 1 2 4 30.95 7.25 2.8895 -2 2 2 4 32.11 21.86 2.7876 -3 1 2 4 33.31 8.08 2.6900 -4 2 1 4 33.32 19.65 2.6889 1 5 0 4 33.48 5.80 2.6767 4 2 0 4 35.41 3.38 2.5351 -1 5 1 4 35.46 3.37 2.5315 3 3 1 4 36.85 3.00 2.4394 1 5 1 4 37.02 4.31 2.4285 2 2 2 4 37.94 18.85 2.3713 0 4 2 4 38.47 18.07 2.3402 -2 4 2 4 38.51 2.62 2.3376 -5 1 1 4 38.60 3.79 2.3322 -4 2 2 4 39.05 5.02 2.3064 4 2 1 4 39.11 1.82 2.3033 0 6 0 2 40.08 11.27 2.2495 3 5 0 4 40.59 2.23 2.2224 -3 5 1 4 40.69 10.75 2.2175 3 1 2 4 40.92 2.17 2.2053 -1 1 3 4 41.58 4.12 2.1718 0 6 1 4 42.21 2.86 2.1410 2 6 0 4 42.64 9.26 2.1203 -5 1 2 4 42.89 1.87 2.1087 -5 3 1 4 42.89 3.73 2.1086 -2 2 3 4 43.16 1.83 2.0961 -3 1 3 4 43.32 3.62 2.0887 -2 6 1 4 43.63 12.13 2.0744 2 4 2 4 43.64 8.59 2.0740 5 3 0 4 43.65 3.53 2.0735 0 2 3 4 44.36 1.67 2.0420 3 5 1 4 44.67 1.64 2.0287 1 1 3 4 44.89 1.61 2.0194 5 1 1 4 45.03 10.95 2.0134 -4 4 2 4 45.11 1.58 2.0100 -1 3 3 4 45.74 3.03 1.9838 2 6 1 4 46.94 4.77 1.9356 6 0 0 2 47.18 1.36 1.9263 -3 3 3 4 47.60 2.65 1.9103 -6 2 1 4 47.83 2.60 1.9016 -4 2 3 4 48.27 1.26 1.8856 -1 7 1 4 48.38 1.83 1.8813 0 6 2 4 48.46 1.82 1.8784 4 2 2 4 48.59 1.23 1.8737 1 3 3 4 48.80 1.22 1.8663 5 3 1 4 48.82 1.77 1.8656 -2 6 2 4 48.86 1.77 1.8638 6 2 0 4 49.39 1.17 1.8452 1 7 1 4 49.92 2.25 1.8270 2 2 3 4 50.46 2.17 1.8085 -4 6 1 4 50.58 1.57 1.8045 4 6 0 4 50.60 1.57 1.8041 -6 2 2 4 50.72 1.07 1.8000 -5 5 1 4 50.74 1.06 1.7993 -5 1 3 4 51.38 4.97 1.7782 5 5 0 4 53.01 3.14 1.7275 0 8 0 2 53.18 1.32 1.7223 2 6 2 4 53.90 4.21 1.7011 -1 7 2 4 53.95 5.91 1.6994 4 4 2 4 54.01 4.18 1.6979 5 1 2 4 54.16 1.70 1.6934 6 2 1 4 54.39 1.22 1.6869 -4 6 2 4 54.73 1.63 1.6771 4 6 1 4 54.78 2.80 1.6757 -2 0 4 2 55.50 5.35 1.6558 2 8 0 4 55.94 5.20 1.6438 -6 4 2 4 55.97 3.68 1.6429 1 7 2 4 56.38 3.59 1.6319 -7 1 2 4 56.44 2.52 1.6303 0 0 4 2 56.51 1.07 1.6285 -2 2 4 4 56.75 3.51 1.6222 -3 7 2 4 57.36 1.38 1.6065 -6 2 3 4 57.76 1.35 1.5963 -2 6 3 4 57.99 2.29 1.5905 -4 0 4 2 58.37 1.30 1.5809 0 6 3 4 58.83 3.08 1.5696 -1 3 4 4 59.19 3.02 1.5609 7 3 0 4 59.59 2.94 1.5515 -3 3 4 4 60.41 1.15 1.5323 4 2 3 4 61.63 1.07 1.5048 -6 6 1 4 61.83 1.06 1.5006 -4 6 3 4 62.57 3.48 1.4846 4 8 0 4 62.64 2.46 1.4830 3 7 2 4 62.72 2.45 1.4814 1 3 4 4 62.72 1.73 1.4814 2 0 4 2 64.09 2.27 1.4529 -5 7 2 4 64.15 1.59 1.4517 8 0 0 2 64.89 2.17 1.4370 -5 3 4 4 65.29 2.12 1.4290 -1 5 4 4 65.60 1.47 1.4230 -6 0 4 2 65.63 2.08 1.4225 7 5 0 4 66.01 2.04 1.4153 -3 5 4 4 67.04 1.93 1.3960 -1 9 2 4 67.51 2.65 1.3875 6 4 2 4 68.87 1.75 1.3633 1 9 2 4 68.97 1.74 1.3615 1 5 4 4 69.56 1.69 1.3514 -3 9 2 4 69.72 1.68 1.3487 7 1 2 4 69.94 2.34 1.3450 -8 4 2 4 70.81 1.59 1.3306 3 3 4 4 71.05 1.57 1.3268 -5 5 4 4 72.47 1.47 1.3043 -9 1 2 4 72.94 1.01 1.2970 4 0 4 2 73.21 1.42 1.2929 5 7 2 4 73.48 1.97 1.2888 6 8 0 4 74.21 1.35 1.2778 -7 3 4 4 74.91 1.31 1.2677 3 9 2 4 75.23 1.29 1.2631 -7 7 2 4 76.22 1.23 1.2491 1 11 0 4 76.25 1.23 1.2487 -5 9 2 4 76.69 1.21 1.2426 9 3 0 4 76.76 1.21 1.2417 3 5 4 4 79.72 1.50 1.2028 -2 8 4 4 80.07 1.05 1.1985 -7 5 4 4 80.35 1.04 1.1950 3 11 0 4 81.11 1.42 1.1857 0 8 4 4 82.43 1.35 1.1701 -4 8 4 4 83.90 1.28 1.1532 8 4 2 4 86.56 1.17 1.1245 2 8 4 4 86.83 1.16 1.1217 -10 4 2 4 87.84 1.12 1.1114 8 8 0 4 89.16 1.08 1.0984 -6 8 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.