Gerstleyite Nakai I, Appleman D E Chemistry Letters 1981 (1981) 1327-1330 The crystal structure of gerstleyite Na2(Sb,As)8S13*2H2O: the first sulfosalt mineral of sodium Locality: Baker mine, Kern County, Boron, California, USA _database_code_amcsd 0012197 CELL PARAMETERS: 9.9110 23.0500 7.0970 90.000 127.850 90.000 SPACE GROUP: Cm X-RAY WAVELENGTH: 1.541838 Cell Volume: 1280.210 Density (g/cm3): 3.735 MAX. ABS. INTENSITY / VOLUME**2: 39.67088323 RIR: 3.459 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.67 100.00 11.5250 0 2 0 2 11.94 7.72 7.4105 1 1 0 2 13.15 7.08 6.7312 -1 1 1 2 15.38 6.65 5.7625 0 4 0 2 15.81 30.15 5.6039 0 0 1 1 16.17 8.39 5.4827 1 3 0 2 17.09 6.70 5.1898 -1 3 1 2 18.00 2.98 4.9273 -2 0 1 1 22.13 40.23 4.0175 0 4 1 2 22.38 10.56 3.9721 1 5 0 2 22.73 29.80 3.9130 2 0 0 1 23.06 10.34 3.8564 -1 5 1 2 23.76 11.74 3.7449 -2 4 1 2 24.02 6.67 3.7052 2 2 0 2 24.87 9.34 3.5798 1 1 1 2 25.31 23.26 3.5190 -2 0 2 1 26.48 4.65 3.3656 -2 2 2 2 26.69 9.53 3.3404 -1 1 2 2 27.21 3.07 3.2775 1 3 1 2 27.75 8.92 3.2153 -3 1 1 2 28.16 16.60 3.1686 0 6 1 2 28.89 5.15 3.0909 -1 3 2 2 29.39 6.66 3.0385 -3 1 2 2 29.43 4.49 3.0351 1 7 0 2 29.48 67.13 3.0296 -2 6 1 2 29.75 1.86 3.0033 -2 4 2 2 29.87 19.81 2.9909 -3 3 1 2 29.96 5.81 2.9826 -1 7 1 2 31.40 3.81 2.8489 1 5 1 2 31.42 13.45 2.8471 -3 3 2 2 31.94 29.43 2.8020 0 0 2 1 32.67 9.67 2.7413 2 6 0 2 32.88 2.42 2.7238 -1 5 2 2 32.90 12.24 2.7227 0 2 2 2 33.76 6.14 2.6547 -3 5 1 2 34.60 1.99 2.5921 3 1 0 2 35.02 12.50 2.5624 0 8 1 2 35.12 4.24 2.5556 2 0 1 1 35.16 3.50 2.5525 -3 5 2 2 36.11 16.26 2.4872 -2 8 1 2 36.37 4.74 2.4702 3 3 0 2 36.47 9.77 2.4636 -4 0 2 1 36.88 1.50 2.4370 1 7 1 2 36.93 2.81 2.4341 1 9 0 2 37.32 1.72 2.4092 -4 2 2 2 37.36 3.03 2.4067 -1 9 1 2 38.18 1.15 2.3573 -1 7 2 2 38.31 3.65 2.3495 -4 0 1 1 38.54 10.82 2.3361 2 4 1 2 38.62 1.99 2.3312 -2 0 3 1 38.81 1.22 2.3201 2 8 0 2 38.96 2.11 2.3120 -3 7 1 2 39.70 8.63 2.2704 3 5 0 2 39.82 5.20 2.2638 0 6 2 2 40.19 4.57 2.2437 -3 3 3 2 40.50 1.22 2.2275 1 1 2 2 41.51 1.45 2.1756 -4 4 1 2 41.80 9.89 2.1611 -2 4 3 2 42.05 1.01 2.1487 1 3 2 2 42.48 1.36 2.1279 -1 1 3 2 42.48 6.93 2.1278 2 6 1 2 43.27 11.49 2.0908 -3 5 3 2 43.34 1.24 2.0878 -2 10 1 2 43.65 4.72 2.0738 -4 6 2 2 43.98 1.65 2.0589 -1 3 3 2 44.30 2.42 2.0448 3 7 0 2 44.59 1.44 2.0321 -4 4 3 2 45.09 1.99 2.0109 -3 9 1 2 45.24 4.56 2.0043 -4 6 1 2 45.51 5.30 1.9930 -2 6 3 2 45.68 3.28 1.9860 2 10 0 2 46.19 1.67 1.9654 -3 9 2 2 47.12 2.00 1.9289 4 2 0 2 47.13 2.64 1.9282 -2 10 2 2 47.32 11.83 1.9208 0 12 0 2 47.48 6.03 1.9150 -5 3 2 2 47.56 5.70 1.9119 2 8 1 2 47.59 4.04 1.9107 -3 7 3 2 48.12 3.31 1.8909 3 3 1 2 48.13 2.57 1.8905 -4 6 3 2 48.75 1.55 1.8680 0 0 3 1 49.24 2.41 1.8506 -5 3 3 2 49.43 1.27 1.8439 0 2 3 2 49.90 2.32 1.8276 3 9 0 2 50.13 1.43 1.8197 -5 1 1 2 50.20 3.66 1.8173 -5 5 2 2 50.30 1.63 1.8140 1 11 1 2 50.35 4.83 1.8123 -2 8 3 2 50.36 2.11 1.8119 2 0 2 1 50.82 5.76 1.7966 3 5 1 2 51.03 2.36 1.7899 2 2 2 2 51.32 2.03 1.7804 -1 11 2 2 51.33 3.51 1.7801 0 10 2 2 51.42 6.24 1.7769 0 4 3 2 51.46 2.19 1.7759 -5 3 1 2 51.89 1.89 1.7620 -5 5 3 2 51.93 3.41 1.7607 -3 11 1 2 52.49 1.13 1.7434 4 6 0 2 52.62 1.66 1.7393 -4 2 4 2 52.93 3.34 1.7299 -3 9 3 2 52.93 1.96 1.7299 -3 11 2 2 52.98 2.58 1.7284 2 4 2 2 53.11 5.87 1.7243 2 12 0 2 53.22 3.10 1.7211 -3 3 4 2 54.10 1.86 1.6952 -5 7 2 2 54.35 1.32 1.6880 -2 0 4 1 54.42 5.55 1.6860 -2 12 2 2 54.53 1.94 1.6828 -4 4 4 2 54.63 1.69 1.6799 0 6 3 2 54.68 2.31 1.6784 3 7 1 2 54.98 1.70 1.6702 -2 2 4 2 55.10 1.89 1.6669 -5 1 4 2 55.71 1.99 1.6501 -5 7 3 2 55.74 2.64 1.6491 -3 5 4 2 55.84 1.56 1.6464 0 14 0 2 55.99 4.70 1.6424 -6 0 3 1 56.34 3.75 1.6330 -5 3 4 2 56.70 2.55 1.6235 -6 0 2 1 56.83 1.03 1.6200 -2 4 4 2 57.75 1.21 1.5965 -5 7 1 2 58.23 5.84 1.5843 0 12 2 2 58.92 2.48 1.5674 0 8 3 2 59.02 3.50 1.5652 -5 9 2 2 59.16 1.22 1.5616 5 1 0 2 59.36 1.06 1.5569 4 2 1 2 59.57 2.04 1.5519 3 9 1 2 60.27 1.63 1.5355 2 12 1 2 60.35 3.42 1.5337 5 3 0 2 60.54 1.63 1.5294 -5 9 3 2 61.13 1.85 1.5160 4 4 1 2 61.18 1.49 1.5148 -4 12 2 2 62.98 1.08 1.4758 3 3 2 2 64.05 1.29 1.4539 -3 9 4 2 65.53 1.88 1.4245 2 10 2 2 65.79 1.03 1.4195 0 14 2 2 66.77 2.74 1.4010 0 0 4 1 66.90 1.05 1.3986 -1 15 2 2 67.08 1.14 1.3953 0 16 1 2 67.43 2.00 1.3890 -3 15 1 2 67.67 1.18 1.3846 -5 3 5 2 68.13 1.14 1.3764 -5 11 1 2 68.28 1.72 1.3737 -3 15 2 2 68.95 1.48 1.3619 -2 10 4 2 71.59 1.41 1.3180 2 12 2 2 72.32 1.14 1.3066 -5 11 4 2 72.45 1.73 1.3046 2 6 3 2 76.27 1.28 1.2484 0 18 1 2 76.81 1.22 1.2410 -2 6 5 2 76.93 1.01 1.2394 -2 18 1 2 85.86 1.83 1.1319 0 12 4 2 85.93 1.55 1.1312 -5 15 4 2 86.78 1.21 1.1222 -2 20 1 2 89.34 1.40 1.0965 5 15 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.