(C2N2H10)8Sc8(ScO2)4(PO4)4(HPO4)12*12H2O Bull I, Young V, Teat S J, Peng L, Grey C P, Parise J B Chemistry of Materials 15 (2003) 3818-3825 Hydrothermal synthesis and structural characterization of four scandium phosphate frameworks _database_code_amcsd 0012217 CELL PARAMETERS: 8.6030 15.4760 16.5040 90.000 96.877 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 2181.534 Density (g/cm3): 2.219 MAX. ABS. INTENSITY / VOLUME**2: 6.444663443 RIR: 0.946 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.86 37.49 11.2509 0 1 1 4 11.44 100.00 7.7380 0 2 0 2 11.83 23.87 7.4779 1 1 0 4 12.22 2.15 7.2407 0 1 2 4 12.25 14.07 7.2275 1 0 1 2 12.49 6.98 7.0894 -1 1 1 4 15.75 3.17 5.6255 0 2 2 4 16.87 2.20 5.2556 1 1 2 4 18.03 1.43 4.9206 0 3 1 4 18.20 5.84 4.8739 -1 0 3 2 19.60 10.48 4.5300 1 2 2 4 20.11 1.46 4.4157 1 3 0 4 20.32 2.32 4.3700 1 0 3 2 20.34 1.78 4.3654 0 3 2 4 21.13 7.39 4.2056 1 1 3 4 21.16 1.03 4.1988 1 3 1 4 21.55 21.09 4.1240 -1 2 3 4 21.59 12.94 4.1167 2 1 0 4 21.70 2.18 4.0963 0 0 4 2 22.27 1.41 3.9917 -1 3 2 4 22.29 3.04 3.9877 -2 0 2 2 22.45 2.35 3.9599 0 1 4 4 22.87 15.57 3.8880 2 1 1 4 22.99 3.74 3.8690 0 4 0 2 23.03 1.91 3.8616 -2 1 2 4 23.38 3.99 3.8051 1 2 3 4 23.47 5.28 3.7903 1 3 2 4 23.63 17.00 3.7655 0 4 1 4 23.65 2.17 3.7626 -1 1 4 4 23.80 9.64 3.7389 2 2 0 4 24.59 16.09 3.6203 0 2 4 4 24.64 1.69 3.6137 2 0 2 2 25.12 18.63 3.5447 -2 2 2 4 25.14 3.17 3.5428 -1 3 3 4 25.27 16.36 3.5243 1 4 0 4 25.31 4.43 3.5191 2 1 2 4 25.46 2.48 3.4985 0 4 2 4 25.55 7.30 3.4866 -2 1 3 4 26.12 13.03 3.4110 1 4 1 4 26.74 40.03 3.3344 1 3 3 4 27.11 18.66 3.2896 2 3 0 4 27.15 2.35 3.2842 -2 3 1 4 27.24 17.44 3.2743 2 2 2 4 27.76 1.31 3.2133 1 2 4 4 27.83 3.60 3.2060 0 1 5 4 28.16 9.89 3.1693 2 3 1 4 28.33 3.97 3.1507 -2 0 4 2 28.57 31.75 3.1243 -1 1 5 4 28.62 3.20 3.1190 2 1 3 4 28.80 1.02 3.1003 -1 3 4 4 28.92 38.12 3.0873 -2 1 4 4 29.37 6.74 3.0414 0 5 1 4 29.60 7.85 3.0176 0 2 5 4 30.20 4.21 2.9598 2 3 2 4 30.35 3.05 2.9447 2 2 3 4 30.36 4.50 2.9440 1 0 5 2 30.64 1.30 2.9181 -2 2 4 4 30.72 1.15 2.9100 1 5 0 4 30.92 10.39 2.8921 1 1 5 4 31.19 4.73 2.8673 2 4 0 4 31.24 3.83 2.8634 -3 0 1 2 31.81 1.28 2.8127 0 4 4 4 31.96 1.38 2.8000 3 1 0 4 32.24 2.71 2.7768 -2 4 2 4 32.55 1.36 2.7506 -3 1 2 4 32.79 3.01 2.7309 0 0 6 2 33.08 1.70 2.7076 3 1 1 4 33.37 1.80 2.6855 -3 2 1 4 33.94 1.21 2.6409 2 4 2 4 34.12 1.62 2.6278 2 2 4 4 34.22 3.44 2.6201 -3 1 3 4 34.32 1.06 2.6128 -1 5 3 4 35.22 8.69 2.5480 0 6 1 4 36.39 4.94 2.4692 1 6 0 4 36.52 1.93 2.4603 0 6 2 4 36.55 1.80 2.4587 2 4 3 4 36.65 1.99 2.4517 2 5 1 4 36.79 1.20 2.4431 -2 4 4 4 36.88 2.91 2.4369 -2 0 6 2 37.01 1.93 2.4293 1 6 1 4 37.05 1.34 2.4267 3 3 1 4 37.25 1.59 2.4136 0 3 6 4 37.33 1.43 2.4092 3 0 3 2 37.79 2.68 2.3805 3 1 3 4 38.42 3.41 2.3428 1 4 5 4 38.74 1.71 2.3244 -2 2 6 4 39.14 1.92 2.3016 -3 4 1 4 40.09 1.93 2.2494 -2 4 5 4 40.65 3.97 2.2195 2 5 3 4 41.61 2.02 2.1704 2 6 1 4 42.33 1.21 2.1353 4 0 0 2 42.75 1.01 2.1152 4 1 0 4 42.77 2.23 2.1142 1 7 1 4 43.17 2.90 2.0954 3 5 0 4 43.64 2.34 2.0739 2 5 4 4 43.80 1.31 2.0669 4 1 1 4 43.91 1.37 2.0619 -2 5 5 4 44.23 1.01 2.0478 0 5 6 4 44.56 1.13 2.0332 -1 5 6 4 44.63 1.45 2.0305 0 1 8 4 44.95 2.26 2.0167 -3 5 3 4 45.02 1.88 2.0138 4 2 1 4 45.14 1.24 2.0084 4 0 2 2 45.49 1.70 1.9939 -4 0 4 2 45.62 2.84 1.9884 3 5 2 4 45.83 1.12 1.9799 -1 2 8 4 46.91 1.21 1.9369 2 7 1 4 47.07 1.32 1.9308 -4 2 4 4 47.22 1.27 1.9247 -3 0 7 2 47.23 3.14 1.9245 -2 1 8 4 47.32 1.81 1.9212 0 8 1 4 47.33 1.50 1.9208 -1 7 4 4 47.61 3.60 1.9100 -3 1 7 4 48.25 1.04 1.8860 -2 6 5 4 48.38 1.74 1.8815 1 2 8 4 48.42 1.39 1.8800 -1 8 1 4 48.82 2.08 1.8655 -4 4 2 4 49.89 1.27 1.8280 1 8 2 4 49.95 1.24 1.8257 -1 0 9 2 50.02 1.01 1.8235 0 8 3 4 50.32 1.89 1.8131 -1 1 9 4 50.51 1.69 1.8069 4 0 4 2 50.75 1.11 1.7991 3 4 5 4 50.88 2.76 1.7947 4 1 4 4 51.31 1.12 1.7807 2 6 5 4 51.41 1.17 1.7774 -4 1 6 4 51.52 1.69 1.7740 -2 5 7 4 51.76 1.59 1.7661 2 0 8 2 51.94 2.87 1.7606 3 6 3 4 52.80 1.83 1.7337 2 7 4 4 52.81 1.29 1.7334 0 6 7 4 53.04 1.40 1.7266 -2 7 5 4 53.20 2.15 1.7219 2 2 8 4 53.22 2.85 1.7211 -1 3 9 4 53.60 1.43 1.7099 -5 1 1 4 53.61 1.50 1.7097 -1 7 6 4 53.75 1.23 1.7055 2 8 2 4 54.26 2.16 1.6905 -4 3 6 4 54.59 1.40 1.6812 3 6 4 4 54.65 2.33 1.6794 -5 2 1 4 54.88 1.11 1.6729 1 9 1 4 55.13 1.18 1.6659 0 8 5 4 55.90 1.20 1.6448 4 6 0 4 55.95 1.46 1.6435 1 9 2 4 55.98 1.88 1.6426 -4 2 7 4 56.57 2.88 1.6270 4 5 3 4 56.66 1.10 1.6246 -3 0 9 2 57.35 2.53 1.6067 2 4 8 4 58.01 1.82 1.5900 -3 2 9 4 58.38 2.16 1.5808 2 9 1 4 59.38 1.70 1.5565 1 7 7 4 60.89 1.59 1.5213 4 3 6 4 61.25 1.14 1.5133 1 10 1 4 62.26 1.57 1.4911 -1 1 11 4 63.45 1.24 1.4660 -5 0 7 2 63.52 1.38 1.4646 -3 9 2 4 63.74 1.25 1.4602 -2 9 5 4 64.07 1.53 1.4533 -1 5 10 4 65.06 1.15 1.4336 4 8 0 4 66.53 1.06 1.4054 0 7 9 4 68.27 1.39 1.3738 -5 5 6 4 71.20 1.21 1.3244 -6 1 6 4 71.45 1.01 1.3203 -1 7 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.