Sc4(HPO4)8*4(H3O) Bull I, Young V, Teat S J, Peng L, Grey C P, Parise J B Chemistry of Materials 15 (2003) 3818-3825 Hydrothermal synthesis and structural characterization of four scandium phosphate frameworks _database_code_amcsd 0012219 CELL PARAMETERS: 5.3048 8.8230 14.7790 90.000 95.685 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 688.318 Density (g/cm3): 2.469 MAX. ABS. INTENSITY / VOLUME**2: 10.56146342 RIR: 1.393 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.70 100.00 7.5658 0 1 1 4 12.04 4.28 7.3532 0 0 2 2 15.69 10.16 5.6486 0 1 2 4 19.60 1.09 4.5299 1 1 0 4 19.71 4.73 4.5048 -1 0 2 2 20.01 9.84 4.4366 -1 1 1 4 20.13 2.82 4.4115 0 2 0 2 20.73 6.26 4.2851 0 1 3 4 21.01 16.49 4.2292 1 1 1 4 22.16 22.34 4.0121 -1 1 2 4 23.93 34.16 3.7182 1 1 2 4 24.21 10.13 3.6766 0 0 4 2 25.62 2.20 3.4775 -1 1 3 4 26.26 41.79 3.3937 0 1 4 4 26.33 1.13 3.3850 1 2 0 4 26.64 11.64 3.3456 -1 2 1 4 27.19 8.34 3.2792 0 2 3 4 27.41 13.02 3.2539 1 2 1 4 27.93 1.40 3.1943 1 1 3 4 28.17 1.28 3.1677 -1 0 4 2 28.32 69.78 3.1519 -1 2 2 4 29.75 24.04 3.0033 1 2 2 4 29.97 1.52 2.9814 -1 1 4 4 31.01 1.17 2.8839 0 3 1 4 31.68 12.58 2.8243 0 2 4 4 32.80 1.83 2.7307 0 3 2 4 33.10 1.15 2.7062 1 2 3 4 33.97 31.53 2.6394 2 0 0 2 34.87 4.10 2.5731 -1 2 4 4 34.92 4.36 2.5692 1 3 0 4 34.93 4.90 2.5686 -1 1 5 4 34.96 2.31 2.5663 -2 0 2 2 35.17 1.90 2.5518 -1 3 1 4 35.60 6.03 2.5219 0 3 3 4 35.77 2.27 2.5104 1 3 1 4 36.66 2.69 2.4511 0 0 6 2 36.72 7.95 2.4472 0 2 5 4 37.86 1.51 2.3763 1 1 5 4 38.11 6.67 2.3616 0 1 6 4 38.74 3.15 2.3243 2 1 2 4 38.95 4.30 2.3123 -1 0 6 2 39.23 1.47 2.2966 0 3 4 4 40.32 1.67 2.2368 -1 1 6 4 40.67 1.11 2.2183 -2 2 2 4 41.92 8.61 2.1553 -1 3 4 4 42.16 3.56 2.1435 1 0 6 2 42.76 3.45 2.1146 2 2 2 4 42.80 1.13 2.1127 0 4 2 4 43.52 1.16 2.0797 0 3 5 4 44.18 2.71 2.0500 2 0 4 2 44.22 1.46 2.0480 -1 2 6 4 44.52 2.49 2.0352 1 4 0 4 45.07 1.25 2.0115 0 4 3 4 45.21 1.19 2.0056 1 4 1 4 45.52 2.54 1.9926 2 2 3 4 45.76 2.03 1.9829 -1 3 5 4 46.17 1.23 1.9661 -2 3 1 4 46.77 1.82 1.9425 1 4 2 4 47.13 1.14 1.9285 2 3 1 4 47.73 2.55 1.9056 -1 4 3 4 48.11 2.01 1.8915 0 4 4 4 48.34 1.79 1.8829 0 3 6 4 48.61 1.42 1.8731 -2 2 5 4 48.65 4.01 1.8716 -2 3 3 4 49.00 1.01 1.8591 2 2 4 4 49.12 4.54 1.8547 1 4 3 4 49.59 1.08 1.8383 0 0 8 2 50.19 2.69 1.8178 -1 3 6 4 50.96 4.27 1.7920 -1 0 8 2 51.37 3.77 1.7787 2 3 3 4 51.81 1.14 1.7647 0 4 5 4 52.81 1.39 1.7334 -3 1 1 4 53.09 2.50 1.7250 2 2 5 4 53.34 1.77 1.7175 -3 1 2 4 53.40 3.92 1.7159 0 5 2 4 53.48 1.03 1.7134 2 0 6 2 53.61 4.01 1.7095 0 3 7 4 54.04 1.28 1.6970 -2 1 7 4 54.04 4.52 1.6969 0 2 8 4 54.11 2.28 1.6949 3 1 1 4 54.15 2.43 1.6937 -2 4 1 4 54.19 1.88 1.6925 2 4 0 4 54.46 1.68 1.6850 1 0 8 2 55.90 1.67 1.6448 3 1 2 4 56.04 1.74 1.6410 -3 2 1 4 56.09 2.25 1.6396 0 4 6 4 56.37 1.02 1.6322 -2 4 3 4 56.55 7.36 1.6275 -3 2 2 4 56.57 1.22 1.6270 2 4 2 4 57.29 1.32 1.6082 3 2 1 4 57.35 1.55 1.6067 0 1 9 4 57.96 1.24 1.5911 -2 3 6 4 58.04 2.34 1.5892 1 3 7 4 58.39 2.18 1.5806 -1 1 9 4 58.57 2.05 1.5759 -2 4 4 4 59.01 3.34 1.5652 3 2 2 4 59.41 1.08 1.5558 -3 1 5 4 59.85 1.99 1.5454 2 1 7 4 61.40 1.34 1.5100 3 3 0 4 61.45 1.32 1.5090 -2 4 5 4 61.61 2.27 1.5055 1 5 4 4 62.28 1.57 1.4907 -2 2 8 4 62.29 1.14 1.4905 -1 4 7 4 64.04 4.67 1.4540 -2 5 2 4 64.64 1.23 1.4419 0 6 2 4 64.94 1.35 1.4360 -2 4 6 4 64.94 1.74 1.4359 -2 1 9 4 65.01 2.17 1.4347 1 4 7 4 65.57 1.16 1.4236 2 5 2 4 66.48 1.03 1.4065 1 6 1 4 68.41 1.84 1.3714 2 2 8 4 68.77 1.54 1.3651 1 1 10 4 69.57 2.29 1.3513 1 6 3 4 70.62 1.20 1.3338 -1 6 4 4 71.32 1.19 1.3224 -3 4 4 4 71.49 2.28 1.3197 4 0 0 2 71.68 1.43 1.3166 2 1 9 4 72.09 1.12 1.3102 1 6 4 4 72.41 1.13 1.3052 4 1 0 4 72.84 1.54 1.2985 3 4 3 4 73.85 1.26 1.2832 -4 0 4 2 75.78 1.32 1.2552 2 6 2 4 77.93 3.57 1.2260 1 7 0 4 83.02 1.17 1.1632 1 3 11 4 84.59 1.46 1.1455 4 3 3 4 89.90 1.22 1.0912 -4 2 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.