Agricolaite Han J C, Rong S B, Chen Q M, Wu X R Chinese Journal of Chemistry 4 (1990) 313-318 The determination of the crystal structure of tetrapotassium uranyl tricarbonate by powder X-ray diffraction method Locality: synthetic _database_code_amcsd 0012225 CELL PARAMETERS: 10.2400 9.1980 12.2220 90.000 95.120 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1146.567 Density (g/cm3): 3.513 MAX. ABS. INTENSITY / VOLUME**2: 33.64375008 RIR: 3.119 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.96 36.19 6.8306 1 1 0 4 14.49 100.00 6.1149 -1 1 1 4 14.55 46.61 6.0866 0 0 2 2 15.25 76.17 5.8105 1 1 1 4 17.39 56.39 5.0996 2 0 0 2 18.94 8.37 4.6855 -1 1 2 4 19.30 26.51 4.5990 0 2 0 2 20.65 19.51 4.3022 0 2 1 4 21.71 21.15 4.0929 -2 0 2 2 23.74 38.92 3.7478 2 0 2 2 24.26 21.70 3.6693 0 2 2 4 24.84 21.02 3.5839 -1 1 3 4 26.09 6.92 3.4153 2 2 0 4 26.21 56.61 3.4005 1 1 3 4 26.68 5.01 3.3407 -2 2 1 4 27.54 41.26 3.2384 2 2 1 4 28.33 42.72 3.1501 -3 1 1 4 29.21 11.19 3.0574 -2 2 2 4 29.35 6.44 3.0433 0 0 4 2 29.35 6.18 3.0427 0 2 3 4 29.55 15.90 3.0234 3 1 1 4 30.44 12.63 2.9362 1 3 0 4 30.78 2.61 2.9053 2 2 2 4 31.15 6.67 2.8712 -1 3 1 4 31.46 2.32 2.8438 -1 1 4 4 31.53 4.48 2.8378 1 3 1 4 32.78 3.16 2.7322 3 1 2 4 32.90 31.91 2.7224 -2 0 4 2 33.26 8.18 2.6935 -2 2 3 4 33.54 49.56 2.6716 -1 3 2 4 34.25 6.42 2.6184 1 3 2 4 34.28 8.24 2.6159 -3 1 3 4 35.20 2.36 2.5498 4 0 0 2 35.35 4.76 2.5392 2 2 3 4 35.37 6.65 2.5380 0 2 4 4 36.99 4.42 2.4303 -4 0 2 2 37.29 5.50 2.4111 3 1 3 4 37.34 6.65 2.4083 -1 3 3 4 38.30 2.73 2.3503 1 3 3 4 38.42 27.40 2.3427 -2 2 4 4 38.51 9.60 2.3379 -1 1 5 4 39.52 29.45 2.2804 4 0 2 2 39.58 5.05 2.2769 3 3 0 4 39.84 2.87 2.2626 -3 3 1 4 39.90 17.15 2.2595 0 4 1 4 40.05 4.51 2.2512 1 1 5 4 40.45 1.62 2.2300 4 2 0 4 40.55 2.60 2.2245 -4 2 1 4 40.75 1.14 2.2143 3 3 1 4 40.88 3.80 2.2075 2 2 4 4 41.51 2.51 2.1756 -3 3 2 4 41.74 1.47 2.1638 4 2 1 4 41.99 19.72 2.1517 0 2 5 4 42.05 4.27 2.1488 -4 2 2 4 42.22 5.17 2.1407 -1 3 4 4 43.25 1.41 2.0919 3 3 2 4 43.37 2.62 2.0864 1 3 4 4 43.54 4.58 2.0786 -2 4 1 4 44.11 28.66 2.0533 2 4 1 4 44.26 1.89 2.0464 -4 0 4 2 44.34 5.70 2.0430 4 2 2 4 44.39 6.98 2.0410 -2 2 5 4 44.45 1.34 2.0383 -3 3 3 4 44.66 1.97 2.0289 0 0 6 2 44.82 16.66 2.0221 -4 2 3 4 44.91 5.58 2.0183 -3 1 5 4 45.33 3.63 2.0006 0 4 3 4 45.51 2.81 1.9932 -5 1 1 4 45.55 1.38 1.9914 5 1 0 4 46.32 1.08 1.9600 2 4 2 4 46.68 2.50 1.9457 -2 0 6 2 46.87 4.97 1.9386 5 1 1 4 46.91 1.66 1.9368 3 3 3 4 47.12 1.51 1.9287 2 2 5 4 48.07 2.33 1.8929 4 2 3 4 48.12 5.35 1.8909 -2 4 3 4 48.48 6.32 1.8777 -3 3 4 4 48.59 4.24 1.8739 4 0 4 2 48.70 4.59 1.8697 -4 2 4 4 48.93 3.51 1.8614 3 1 5 4 49.08 4.96 1.8563 0 2 6 4 49.18 4.72 1.8527 -5 1 3 4 49.23 1.21 1.8509 1 3 5 4 49.68 3.19 1.8352 2 4 3 4 49.83 7.67 1.8299 2 0 6 2 50.41 5.83 1.8104 1 5 0 4 50.96 2.67 1.7920 -2 2 6 4 51.31 2.51 1.7806 -3 1 6 4 51.55 11.13 1.7730 3 3 4 4 52.51 7.94 1.7428 -1 5 2 4 52.75 3.17 1.7354 4 2 4 4 52.95 2.94 1.7292 5 1 3 4 53.00 3.39 1.7278 1 5 2 4 53.43 2.06 1.7149 -3 3 5 4 53.51 1.09 1.7124 -4 2 5 4 53.60 6.76 1.7099 -1 1 7 4 53.76 3.36 1.7052 -4 4 1 4 53.93 6.25 1.7003 2 2 6 4 53.94 3.67 1.6999 6 0 0 2 53.96 1.17 1.6994 -5 3 1 4 53.99 7.70 1.6983 5 3 0 4 54.29 2.06 1.6896 -1 3 6 4 54.72 3.38 1.6773 4 4 1 4 54.76 4.91 1.6764 -6 0 2 2 54.92 7.14 1.6717 0 4 5 4 55.05 1.52 1.6682 -5 3 2 4 55.16 1.26 1.6652 5 3 1 4 55.28 2.00 1.6617 1 1 7 4 55.29 1.85 1.6615 -4 0 6 2 55.73 1.76 1.6495 1 3 6 4 56.58 1.52 1.6266 0 2 7 4 56.90 2.33 1.6182 -2 4 5 4 56.91 2.34 1.6179 3 5 0 4 57.01 1.52 1.6155 3 3 5 4 57.15 4.72 1.6118 -5 1 5 4 57.27 5.47 1.6087 -4 4 3 4 57.40 3.84 1.6052 5 3 2 4 57.58 1.72 1.6006 6 0 2 2 57.68 1.96 1.5982 -6 2 1 4 57.83 1.76 1.5944 6 2 0 4 58.27 1.90 1.5835 -3 1 7 4 58.39 2.25 1.5804 -3 5 2 4 58.61 5.80 1.5750 -6 2 2 4 58.95 2.39 1.5668 -1 5 4 4 59.12 1.37 1.5626 -4 2 6 4 59.16 5.83 1.5618 -3 3 6 4 59.21 1.34 1.5605 2 4 5 4 59.76 2.22 1.5474 3 5 2 4 59.86 1.79 1.5452 1 5 4 4 60.02 5.06 1.5414 4 4 3 4 60.38 2.40 1.5330 0 6 0 2 60.41 1.09 1.5323 -5 3 4 4 60.59 1.39 1.5282 -6 2 3 4 60.91 2.42 1.5210 0 6 1 4 61.24 2.25 1.5136 2 2 7 4 61.25 1.26 1.5134 -1 3 7 4 61.32 1.13 1.5117 6 2 2 4 62.80 4.76 1.4796 5 1 5 4 62.99 1.75 1.4757 3 1 7 4 63.18 2.01 1.4717 3 3 6 4 64.02 1.87 1.4544 -3 5 4 4 64.08 1.27 1.4531 2 6 1 4 64.46 1.53 1.4456 4 2 6 4 64.53 1.10 1.4442 -5 3 5 4 64.53 1.51 1.4440 -7 1 1 4 64.56 3.01 1.4434 6 2 3 4 64.78 1.08 1.4391 -4 4 5 4 65.04 1.02 1.4341 0 6 3 4 65.21 2.35 1.4307 6 0 4 2 65.57 1.27 1.4237 2 0 8 2 65.57 1.08 1.4237 -3 3 7 4 66.04 3.58 1.4147 7 1 1 4 66.60 2.87 1.4041 3 5 4 4 67.06 1.52 1.3956 -7 1 3 4 67.26 2.38 1.3920 -2 6 3 4 68.53 1.87 1.3693 -6 4 1 4 68.71 2.92 1.3661 5 5 0 4 68.88 1.60 1.3632 -2 4 7 4 68.97 1.42 1.3616 -1 5 6 4 68.99 3.55 1.3612 -4 0 8 2 69.06 1.51 1.3600 2 2 8 4 69.78 1.34 1.3477 6 4 1 4 70.42 3.10 1.3370 1 3 8 4 70.50 2.81 1.3358 -2 6 4 4 71.33 2.74 1.3222 4 2 7 4 71.46 1.79 1.3201 7 1 3 4 71.70 1.95 1.3162 5 5 2 4 71.79 1.29 1.3149 2 4 7 4 72.21 2.17 1.3082 -7 3 2 4 72.40 1.83 1.3052 -4 2 8 4 72.92 2.08 1.2973 0 6 5 4 73.27 2.86 1.2920 -3 5 6 4 73.77 1.32 1.2845 -3 1 9 4 73.79 1.88 1.2841 -2 2 9 4 74.40 1.15 1.2751 -5 5 4 4 74.60 1.88 1.2722 4 6 2 4 74.63 2.58 1.2717 -2 6 5 4 74.88 4.12 1.2682 6 4 3 4 74.95 2.18 1.2671 -4 6 3 4 75.65 1.01 1.2571 5 3 6 4 75.67 1.15 1.2568 5 1 7 4 75.69 1.32 1.2566 -4 4 7 4 76.52 2.11 1.2450 -7 3 4 4 76.65 1.03 1.2432 2 6 5 4 76.91 1.26 1.2396 3 5 6 4 77.12 1.72 1.2367 1 7 3 4 77.37 1.16 1.2334 4 6 3 4 77.40 2.22 1.2330 -8 2 1 4 77.73 1.01 1.2286 8 2 0 4 77.81 1.52 1.2275 -6 2 7 4 78.12 1.37 1.2234 -3 7 1 4 78.43 1.28 1.2194 5 5 4 4 78.59 1.85 1.2173 0 0 10 2 78.88 1.08 1.2136 4 2 8 4 79.21 2.34 1.2093 3 1 9 4 81.29 2.31 1.1836 4 4 7 4 81.85 1.10 1.1768 0 2 10 4 82.00 1.54 1.1751 2 6 6 4 83.57 1.20 1.1570 6 4 5 4 83.65 2.43 1.1560 -2 4 9 4 83.67 1.67 1.1559 1 5 8 4 84.21 1.26 1.1497 0 8 0 2 85.09 1.27 1.1402 8 0 4 2 85.12 1.42 1.1398 -6 6 1 4 85.37 1.07 1.1371 -7 5 2 4 85.91 1.24 1.1313 -6 6 2 4 86.12 1.12 1.1292 -9 1 1 4 86.45 1.64 1.1257 -8 0 6 2 87.16 1.61 1.1183 -8 4 1 4 87.56 2.14 1.1142 -6 4 7 4 88.03 1.33 1.1095 -9 1 3 4 88.19 1.59 1.1079 2 6 7 4 88.73 1.20 1.1026 8 4 1 4 89.07 1.00 1.0992 2 8 2 4 89.52 1.27 1.0948 -7 5 4 4 89.76 1.34 1.0925 -4 4 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.