Dickite Bish D L, Johnston C T Clays and Clay Minerals 41 (1993) 297-304 Rietveld refinement and Fourier-transform infrared spectroscopic study of the dickite structure at low temperature Locality: St. Claire, Pennsylvania, USA Note: Sample at T = 12 K _database_code_amcsd 0012236 CELL PARAMETERS: 5.1474 8.9386 14.3900 90.000 96.483 90.000 SPACE GROUP: Cc X-RAY WAVELENGTH: 1.541838 Cell Volume: 657.858 Density (g/cm3): 2.606 MAX. ABS. INTENSITY / VOLUME**2: 8.337170372 RIR: 1.042 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.38 100.00 7.1490 0 0 2 1 19.87 4.14 4.4693 0 2 0 2 20.00 31.53 4.4392 1 1 0 2 20.36 33.87 4.3623 -1 1 1 2 20.82 24.17 4.2658 0 2 1 2 21.53 55.04 4.1266 1 1 1 2 22.52 10.24 3.9487 -1 1 2 2 23.47 43.49 3.7897 0 2 2 2 24.62 8.92 3.6158 1 1 2 2 24.91 58.87 3.5745 0 0 4 1 26.06 17.27 3.4198 -1 1 3 2 27.36 3.71 3.2601 0 2 3 2 28.80 5.63 3.1004 1 1 3 2 30.53 5.07 2.9278 -1 1 4 2 32.06 8.23 2.7915 0 2 4 2 33.70 1.32 2.6597 1 1 4 2 35.06 13.37 2.5593 -1 3 1 2 35.09 8.78 2.5572 2 0 0 1 35.64 7.03 2.5190 -1 1 5 2 35.79 23.67 2.5090 1 3 1 2 35.94 12.27 2.4990 -2 0 2 1 37.33 1.29 2.4087 0 2 5 2 37.75 9.43 2.3830 0 0 6 1 38.71 24.09 2.3260 2 0 2 1 38.80 53.81 2.3210 -1 3 3 2 39.11 4.22 2.3034 1 1 5 2 40.77 4.78 2.2132 1 3 3 2 41.01 2.45 2.2007 -2 0 4 1 41.40 1.21 2.1812 -2 2 2 2 43.01 2.28 2.1028 0 2 6 2 44.79 1.23 2.0233 0 4 3 2 45.91 9.03 1.9769 2 0 4 1 45.97 2.96 1.9743 -2 2 4 2 46.08 16.26 1.9698 -1 3 5 2 46.81 1.89 1.9406 2 2 3 2 48.01 4.20 1.8948 0 4 4 2 48.93 6.03 1.8614 1 3 5 2 49.23 3.49 1.8507 -2 0 6 1 49.45 2.21 1.8431 -2 2 5 2 50.48 4.17 1.8079 2 2 4 2 51.11 3.42 1.7872 0 0 8 1 51.93 2.14 1.7608 0 4 5 2 53.60 1.36 1.7099 -2 2 6 2 54.43 1.83 1.6858 -2 4 1 2 54.53 1.96 1.6827 2 4 0 2 54.78 1.46 1.6756 2 2 5 2 54.82 1.93 1.6746 3 1 0 2 55.03 2.05 1.6687 1 5 1 2 55.14 3.16 1.6658 -2 4 2 2 55.36 1.29 1.6595 0 2 8 2 55.48 3.71 1.6563 -1 5 2 2 55.61 8.78 1.6528 2 0 6 1 55.84 17.38 1.6463 -1 3 7 2 55.99 3.69 1.6424 3 1 1 2 56.16 2.23 1.6378 -3 1 3 2 56.64 2.32 1.6251 -2 4 3 2 57.16 2.06 1.6115 2 4 2 2 57.23 1.44 1.6098 -1 5 3 2 57.94 2.28 1.5918 3 1 2 2 58.32 1.65 1.5823 -2 2 7 2 58.71 1.21 1.5725 1 5 3 2 59.33 9.12 1.5576 1 3 7 2 59.64 1.55 1.5502 2 2 6 2 59.68 3.11 1.5494 -2 0 8 1 60.93 1.39 1.5205 -3 1 5 2 61.51 1.97 1.5077 0 4 7 2 61.86 1.22 1.4998 -2 4 5 2 62.33 7.91 1.4898 0 6 0 2 62.46 17.36 1.4869 -3 3 1 2 62.75 1.32 1.4806 2 4 4 2 62.89 1.17 1.4777 -1 5 5 2 63.55 4.05 1.4639 -2 2 8 2 63.82 2.83 1.4584 0 6 2 2 63.88 2.01 1.4573 3 3 1 2 64.03 3.97 1.4541 -3 3 3 2 65.01 2.25 1.4346 2 2 7 2 65.26 1.59 1.4298 0 0 10 1 65.48 1.10 1.4254 -2 4 6 2 66.71 1.34 1.4021 -1 5 6 2 67.05 2.81 1.3957 0 4 8 2 67.21 1.10 1.3929 2 0 8 1 67.50 2.87 1.3877 -1 3 9 2 68.17 2.54 1.3755 3 3 3 2 68.20 1.61 1.3751 0 6 4 2 68.48 1.49 1.3702 -3 3 5 2 69.28 1.38 1.3563 -2 2 9 2 70.86 1.44 1.3298 2 2 8 2 71.54 14.93 1.3189 1 3 9 2 71.93 7.64 1.3127 -2 0 10 1 73.08 1.41 1.2948 0 4 9 2 73.58 4.52 1.2873 2 6 0 2 73.80 2.07 1.2840 -4 0 2 1 74.09 1.57 1.2796 -2 6 2 2 74.16 1.26 1.2786 4 0 0 1 74.36 1.03 1.2756 2 6 1 2 75.12 1.37 1.2646 3 3 5 2 75.56 1.47 1.2583 -3 3 7 2 75.83 5.36 1.2545 2 6 2 2 76.19 4.12 1.2495 -4 0 4 1 76.96 2.61 1.2389 1 7 0 2 77.27 1.44 1.2347 4 0 2 1 77.34 1.34 1.2338 3 5 0 2 77.35 2.29 1.2337 -2 6 4 2 77.52 1.11 1.2314 1 7 1 2 77.68 1.33 1.2293 4 2 0 2 78.16 1.92 1.2229 -4 2 3 2 78.33 1.96 1.2207 3 5 1 2 80.63 1.74 1.1915 0 0 12 1 80.75 1.03 1.1901 4 2 2 2 80.78 1.41 1.1898 2 6 4 2 80.94 1.82 1.1878 -1 3 11 2 81.41 1.01 1.1821 2 4 8 2 84.04 1.10 1.1517 2 2 10 2 88.32 3.97 1.1066 2 6 6 2 88.95 2.18 1.1004 -4 0 8 1 89.45 1.18 1.0955 -2 2 12 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.