H3 O7.5 P2 Rb2 Averbuch-Pouchot M, Durif A Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences 316 (1993) 469-476 Synthese et structure cristalline du dihydrogenodiphosphate de rubidium hemihydrate: Rb2H2P2O7 . 1/2H2O _cod_database_code 1007212 _database_code_amcsd 0012310 CELL PARAMETERS: 19.5680 10.5450 7.7730 90.000 90.000 90.000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 Cell Volume: 1603.916 Density (g/cm3): 2.939 MAX. ABS. INTENSITY / VOLUME**2: 11.89178767 RIR: 1.317 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.04 4.11 9.7840 2 0 0 2 12.34 6.16 7.1723 2 1 0 4 14.16 2.51 6.2568 0 1 1 4 14.55 20.35 6.0861 2 0 1 4 15.98 2.25 5.5472 3 1 0 4 16.82 4.38 5.2725 0 2 0 2 17.42 2.61 5.0909 1 2 0 4 19.12 1.09 4.6415 2 2 0 4 20.86 26.29 4.2588 1 2 1 8 21.67 29.05 4.1004 3 2 0 4 22.31 2.82 3.9851 2 2 1 8 22.88 6.19 3.8865 0 0 2 2 23.08 1.71 3.8539 4 1 1 8 24.26 4.87 3.6691 5 1 0 4 24.55 88.02 3.6267 3 2 1 8 24.65 4.84 3.6120 2 0 2 4 24.83 25.62 3.5861 4 2 0 4 24.84 3.56 3.5850 1 1 2 8 25.75 16.50 3.4596 1 3 0 4 26.08 40.24 3.4171 2 1 2 8 26.87 13.02 3.3180 5 1 1 8 27.39 8.17 3.2563 4 2 1 8 28.03 7.10 3.1830 3 1 2 8 28.23 7.26 3.1607 1 3 1 8 28.40 39.48 3.1425 5 2 0 4 28.53 24.56 3.1284 0 2 2 4 28.65 35.63 3.1157 6 1 0 4 28.85 36.64 3.0943 3 3 0 4 28.90 91.68 3.0892 1 2 2 8 29.34 5.13 3.0438 2 3 1 8 29.35 100.00 3.0431 4 0 2 4 29.71 3.71 3.0074 6 0 1 4 30.69 15.99 2.9134 5 2 1 8 30.92 16.88 2.8920 6 1 1 8 31.11 5.72 2.8749 3 3 1 8 31.72 4.33 2.8208 3 2 2 8 33.15 4.40 2.7021 7 1 0 4 33.59 4.83 2.6680 5 1 2 8 34.01 4.50 2.6363 0 4 0 2 34.02 5.23 2.6356 4 2 2 8 34.29 6.59 2.6151 5 3 0 4 34.32 1.88 2.6126 1 4 0 4 35.85 4.26 2.5047 2 0 3 4 35.95 2.64 2.4983 6 0 2 4 36.24 12.43 2.4786 5 3 1 8 36.27 14.99 2.4765 1 4 1 8 36.38 1.27 2.4698 7 2 0 4 36.74 4.48 2.4460 8 0 0 2 36.77 5.06 2.4442 3 4 0 4 36.78 2.06 2.4436 5 2 2 8 36.98 57.28 2.4310 6 1 2 8 37.14 3.49 2.4208 3 3 2 8 37.75 1.31 2.3827 8 1 0 4 38.34 1.96 2.3475 3 1 3 8 38.61 19.22 2.3316 3 4 1 8 38.80 10.00 2.3207 4 4 0 4 39.01 22.09 2.3091 1 2 3 8 39.35 5.10 2.2897 4 0 3 4 39.85 1.03 2.2624 2 2 3 8 39.93 2.07 2.2577 6 2 2 8 40.67 10.35 2.2186 7 1 2 8 41.21 4.08 2.1904 3 2 3 8 41.26 13.30 2.1879 7 3 0 4 41.39 17.09 2.1817 0 4 2 4 41.65 14.61 2.1683 1 4 2 8 42.72 2.15 2.1165 5 1 3 8 43.75 1.31 2.0690 3 4 2 8 44.09 5.56 2.0538 9 1 1 8 44.17 1.48 2.0502 6 4 0 4 44.41 1.39 2.0398 2 3 3 8 44.67 1.73 2.0287 6 0 3 4 44.77 1.22 2.0245 1 5 1 8 45.11 2.68 2.0100 9 2 0 4 45.52 10.00 1.9925 4 4 2 8 45.53 2.63 1.9922 6 1 3 8 45.67 2.88 1.9865 3 3 3 8 46.68 2.15 1.9460 9 2 1 8 46.75 24.16 1.9432 0 0 4 2 46.75 1.58 1.9430 3 5 1 8 47.24 7.84 1.9240 10 1 0 4 47.70 6.04 1.9065 7 3 2 8 47.73 3.28 1.9056 5 4 2 8 47.94 3.49 1.8976 10 0 1 4 48.44 1.85 1.8792 4 5 1 8 48.54 1.51 1.8756 2 1 4 8 48.69 1.10 1.8702 7 1 3 8 48.76 7.01 1.8676 10 1 1 8 48.91 1.50 1.8621 7 4 1 8 49.52 12.34 1.8406 5 3 3 8 49.55 2.33 1.8397 1 4 3 8 50.02 2.92 1.8234 0 2 4 4 50.08 4.90 1.8213 2 5 2 8 50.26 2.98 1.8155 1 2 4 8 50.54 3.90 1.8060 4 0 4 4 50.75 21.34 1.7989 9 3 1 8 51.09 5.82 1.7877 7 2 3 8 51.39 10.00 1.7779 3 4 3 8 51.61 11.85 1.7710 6 5 0 4 52.03 12.39 1.7575 0 6 0 2 52.08 2.26 1.7560 3 2 4 8 52.14 1.52 1.7541 11 1 0 4 52.81 2.34 1.7334 4 5 2 8 53.03 4.19 1.7267 6 5 1 8 53.12 6.97 1.7242 10 1 2 8 53.64 2.07 1.7085 4 2 4 8 55.56 1.94 1.6540 4 6 0 4 55.61 3.55 1.6528 5 2 4 8 55.75 7.65 1.6488 6 1 4 8 55.87 3.91 1.6456 3 3 4 8 55.89 4.06 1.6451 9 1 3 8 56.24 1.53 1.6356 0 5 3 4 56.43 3.24 1.6307 12 0 0 2 56.92 1.29 1.6178 4 6 1 8 57.16 6.07 1.6115 6 5 2 8 57.56 4.15 1.6014 0 6 2 4 57.66 2.10 1.5988 11 1 2 8 57.77 2.25 1.5959 12 0 1 4 58.08 2.07 1.5882 9 2 3 8 58.12 3.81 1.5872 11 3 0 4 58.50 1.82 1.5776 7 1 4 8 59.06 2.16 1.5642 0 4 4 4 59.24 2.71 1.5598 5 3 4 8 59.60 1.05 1.5512 4 5 3 8 59.81 1.12 1.5464 11 2 2 8 59.88 4.79 1.5447 10 1 3 8 60.08 1.41 1.5400 9 4 2 8 60.28 1.65 1.5353 2 0 5 4 60.87 7.39 1.5219 4 6 2 8 60.90 1.30 1.5211 3 4 4 8 61.62 3.95 1.5051 9 3 3 8 62.32 4.01 1.4899 4 4 4 8 62.37 1.52 1.4889 2 7 0 4 62.51 1.13 1.4859 9 5 1 8 63.29 2.43 1.4694 11 3 2 8 63.37 1.56 1.4678 3 7 0 4 63.58 1.39 1.4635 13 1 1 8 63.64 1.53 1.4621 6 5 3 8 64.06 7.00 1.4536 3 2 5 8 64.09 7.06 1.4529 7 3 4 8 66.14 2.88 1.4129 11 2 3 8 66.25 2.54 1.4106 10 5 1 8 66.65 1.17 1.4033 6 0 5 4 67.14 1.02 1.3942 4 6 3 8 67.18 2.28 1.3934 5 2 5 8 67.31 1.70 1.3911 6 1 5 8 67.73 1.15 1.3834 5 7 1 8 68.00 1.37 1.3787 11 4 2 8 68.65 4.35 1.3672 10 1 4 8 68.76 1.32 1.3652 12 4 1 8 68.83 1.08 1.3641 14 1 1 8 68.93 1.31 1.3623 13 3 1 8 69.27 4.47 1.3564 13 2 2 8 69.90 8.09 1.3457 10 5 2 8 70.49 1.99 1.3360 1 4 5 8 71.99 1.78 1.3117 3 4 5 8 72.17 3.68 1.3089 6 5 4 8 72.29 1.16 1.3071 9 5 3 8 72.51 1.52 1.3035 13 3 2 8 72.52 5.44 1.3035 0 6 4 4 73.04 2.87 1.2955 0 0 6 2 73.39 6.03 1.2900 6 7 2 8 74.44 2.74 1.2745 3 8 1 8 75.48 2.08 1.2595 4 6 4 8 75.76 1.22 1.2555 1 2 6 8 75.79 3.82 1.2551 7 7 2 8 75.80 3.55 1.2550 10 5 3 8 76.17 3.15 1.2499 15 2 1 8 76.22 1.35 1.2492 5 8 0 4 76.46 2.10 1.2458 1 8 2 8 77.20 2.85 1.2357 5 7 3 8 77.61 1.45 1.2301 14 0 3 4 77.68 1.41 1.2293 11 3 4 8 78.16 1.89 1.2228 9 7 1 8 78.34 3.94 1.2206 13 3 3 8 78.50 1.16 1.2184 4 2 6 8 78.59 2.04 1.2172 10 0 5 4 78.97 1.45 1.2123 4 5 5 8 79.30 1.37 1.2081 16 0 1 4 80.13 1.50 1.1977 5 2 6 8 80.25 4.30 1.1962 6 1 6 8 80.32 1.40 1.1954 12 6 0 4 80.35 1.48 1.1950 3 3 6 8 80.46 1.21 1.1937 10 7 0 4 80.76 5.88 1.1899 9 3 5 8 81.60 1.37 1.1798 10 7 1 8 82.20 2.59 1.1727 1 8 3 8 82.58 1.01 1.1683 6 5 5 8 82.72 1.52 1.1666 15 3 2 8 82.86 1.20 1.1651 14 5 0 4 83.07 1.10 1.1627 0 4 6 4 83.24 1.34 1.1606 1 4 6 8 83.64 1.28 1.1562 15 4 1 8 83.82 1.74 1.1541 10 5 4 8 84.23 1.24 1.1496 11 7 0 4 86.49 1.16 1.1252 12 0 5 4 86.55 1.36 1.1246 17 2 0 4 88.38 2.46 1.1060 16 0 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.