Cl H28 N12 O6 P Averbuch-Pouchot M, Durif A Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences 317 (1993) 1179-1184 Synthese et structure cristalline d'un compose d'addition entre le monophosphate et le chlorure de guanidinium: (C(NH2)3)3PO4.(C(NH2)3)Cl.2H2O _cod_database_code 1007221 _database_code_amcsd 0015903 CELL PARAMETERS: 14.0380 13.9060 9.9610 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1944.511 Density (g/cm3): 1.389 MAX. ABS. INTENSITY / VOLUME**2: 1.302287716 RIR: 0.305 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.95 72.74 9.8794 1 1 0 4 10.89 15.54 8.1237 1 0 1 4 10.93 32.24 8.0978 0 1 1 4 12.61 8.93 7.0190 2 0 0 2 12.62 18.73 7.0145 1 1 1 4 14.13 32.17 6.2660 2 1 0 4 14.21 50.71 6.2306 1 2 0 4 15.44 18.41 5.7376 2 0 1 4 15.54 12.22 5.7014 0 2 1 4 16.72 60.97 5.3039 2 1 1 4 16.78 6.98 5.2824 1 2 1 4 17.81 31.04 4.9805 0 0 2 2 18.91 2.40 4.6938 1 0 2 4 18.93 48.22 4.6888 0 1 2 4 19.96 11.83 4.4473 1 1 2 4 20.02 27.03 4.4350 3 1 0 4 20.06 15.91 4.4254 2 2 1 4 20.17 3.06 4.4016 1 3 0 4 20.98 8.79 4.2353 3 0 1 4 21.14 7.41 4.2026 0 3 1 4 21.88 49.77 4.0618 2 0 2 4 21.94 60.31 4.0515 3 1 1 4 21.95 9.46 4.0489 0 2 2 4 22.08 100.00 4.0260 1 3 1 4 22.81 18.51 3.8989 2 1 2 4 22.86 56.00 3.8903 1 2 2 4 22.91 35.29 3.8821 3 2 0 4 22.99 8.02 3.8680 2 3 0 4 24.61 32.12 3.6171 3 2 1 4 24.69 43.94 3.6057 2 3 1 4 25.38 20.28 3.5095 4 0 0 2 25.40 17.85 3.5072 2 2 2 4 26.13 44.79 3.4103 3 0 2 4 26.19 8.24 3.4028 4 1 0 4 26.26 16.24 3.3931 0 3 2 4 26.41 20.43 3.3746 1 4 0 4 26.92 30.89 3.3121 3 1 2 4 26.94 19.45 3.3101 4 0 1 4 27.03 32.07 3.2982 1 3 2 4 27.17 1.71 3.2823 0 4 1 4 27.61 8.56 3.2312 1 0 3 4 27.62 8.67 3.2295 0 1 3 4 27.70 6.38 3.2201 4 1 1 4 27.92 32.11 3.1961 1 4 1 4 28.36 32.71 3.1473 1 1 3 4 28.55 52.14 3.1267 3 3 1 4 29.17 27.23 3.0618 3 2 2 4 29.23 8.65 3.0549 2 3 2 4 29.77 8.05 3.0014 2 0 3 4 29.90 8.42 2.9887 4 2 1 4 30.05 59.08 2.9733 2 4 1 4 30.47 12.92 2.9339 2 1 3 4 30.51 28.12 2.9302 1 2 3 4 31.18 20.53 2.8688 4 0 2 4 31.85 36.33 2.8096 4 1 2 4 31.99 8.03 2.7980 4 3 0 4 32.04 11.41 2.7937 1 4 2 4 32.07 1.55 2.7906 3 4 0 4 32.49 7.32 2.7557 2 2 3 4 32.54 2.98 2.7521 5 1 0 4 32.60 10.43 2.7470 3 3 2 4 32.83 3.24 2.7282 1 5 0 4 33.15 1.32 2.7023 5 0 1 4 33.19 4.95 2.6993 0 3 3 4 33.26 5.67 2.6938 4 3 1 4 33.34 3.08 2.6872 3 4 1 4 33.72 15.55 2.6580 3 1 3 4 33.79 5.78 2.6527 5 1 1 4 33.80 18.41 2.6519 4 2 2 4 33.82 3.29 2.6507 1 3 3 4 33.94 23.26 2.6412 2 4 2 4 34.07 1.28 2.6313 1 5 1 4 34.69 8.06 2.5856 2 5 0 4 35.58 1.12 2.5233 3 2 3 4 35.64 12.66 2.5194 2 3 3 4 35.65 2.91 2.5188 5 2 1 4 35.88 2.46 2.5027 2 5 1 4 36.07 1.90 2.4903 0 0 4 2 36.38 2.28 2.4698 4 4 0 4 36.65 3.32 2.4520 1 0 4 4 36.85 2.10 2.4394 4 3 2 4 36.92 8.12 2.4345 3 4 2 4 37.02 11.28 2.4282 0 5 2 4 37.24 3.90 2.4147 1 1 4 4 37.28 1.52 2.4119 4 0 3 4 37.45 3.78 2.4011 0 4 3 4 37.52 5.63 2.3972 4 4 1 4 37.62 8.87 2.3908 3 5 0 4 37.86 2.13 2.3765 4 1 3 4 38.02 2.32 2.3668 1 4 3 4 38.50 1.96 2.3382 3 3 3 4 38.56 5.89 2.3346 5 3 1 4 38.95 3.23 2.3124 1 2 4 4 39.04 2.29 2.3072 6 1 0 4 39.04 2.29 2.3072 5 2 2 4 39.94 1.21 2.2574 0 6 1 4 40.12 2.94 2.2477 6 1 1 4 40.47 1.26 2.2287 1 6 1 4 40.57 13.73 2.2237 2 2 4 4 40.69 8.91 2.2175 6 2 0 4 40.78 3.35 2.2127 4 4 2 4 41.15 1.69 2.1937 0 3 4 4 41.33 1.14 2.1843 5 4 0 4 41.42 4.87 2.1797 4 5 0 4 41.59 3.42 2.1714 3 1 4 4 41.67 2.38 2.1674 1 3 4 4 41.73 6.86 2.1645 6 2 1 4 41.76 1.66 2.1631 5 3 2 4 41.92 1.76 2.1553 3 5 2 4 42.05 6.44 2.1490 2 6 1 4 42.31 1.67 2.1363 3 4 3 4 42.36 3.07 2.1336 5 4 1 4 42.45 1.03 2.1293 4 5 1 4 42.67 2.67 2.1189 5 1 3 4 43.05 2.09 2.1013 0 6 2 4 43.16 3.35 2.0961 3 2 4 4 43.21 2.06 2.0938 2 3 4 4 43.21 2.58 2.0935 6 1 2 4 43.55 6.29 2.0781 1 6 2 4 44.21 1.86 2.0487 5 2 3 4 44.31 2.21 2.0442 6 3 1 4 44.57 6.55 2.0332 3 6 1 4 44.74 2.46 2.0258 6 2 2 4 45.04 2.58 2.0130 2 6 2 4 45.12 2.35 2.0096 4 1 4 4 45.34 1.87 2.0003 5 4 2 4 45.68 5.69 1.9863 3 3 4 4 45.79 1.22 1.9817 4 4 3 4 45.93 1.30 1.9759 5 5 0 4 46.15 3.56 1.9670 1 7 0 4 46.17 4.83 1.9660 7 0 1 4 46.50 1.43 1.9529 1 1 5 4 46.59 2.40 1.9495 4 2 4 4 46.68 1.50 1.9458 5 3 3 4 46.70 3.50 1.9452 2 4 4 4 47.09 1.65 1.9297 1 7 1 4 47.44 1.23 1.9165 2 0 5 4 47.47 2.05 1.9151 0 2 5 4 47.54 1.18 1.9125 6 0 3 4 47.74 2.97 1.9052 6 4 1 4 47.91 2.23 1.8986 2 1 5 4 47.94 4.16 1.8976 1 2 5 4 48.02 1.03 1.8947 6 1 3 4 48.10 2.21 1.8918 7 2 1 4 48.33 1.32 1.8833 1 6 3 4 48.49 2.12 1.8772 2 7 1 4 48.97 3.03 1.8602 4 3 4 4 49.35 1.83 1.8465 5 1 4 4 49.42 1.06 1.8441 6 2 3 4 49.43 2.52 1.8439 7 1 2 4 49.64 2.48 1.8366 5 5 2 4 49.70 1.55 1.8344 2 6 3 4 49.87 1.92 1.8286 3 7 0 4 49.98 3.55 1.8248 5 4 3 4 50.06 1.92 1.8222 4 5 3 4 50.27 3.38 1.8150 1 3 5 4 50.46 1.21 1.8085 6 4 2 4 50.91 7.53 1.7936 2 5 4 4 51.01 1.41 1.7904 6 5 0 4 51.56 2.72 1.7724 3 2 5 4 51.70 3.07 1.7680 6 3 3 4 51.89 1.67 1.7622 6 5 1 4 51.93 1.30 1.7608 3 6 3 4 52.16 3.71 1.7536 4 4 4 4 53.09 1.02 1.7251 1 8 0 4 53.37 3.72 1.7166 7 0 3 4 53.43 1.28 1.7149 8 1 1 4 53.78 1.40 1.7046 3 3 5 4 54.20 2.37 1.6923 1 7 3 4 54.48 2.21 1.6843 1 6 4 4 54.55 1.91 1.6823 5 6 2 4 54.78 1.10 1.6757 6 4 3 4 55.49 2.78 1.6561 6 2 4 4 55.95 1.12 1.6434 8 1 2 4 56.04 1.33 1.6411 8 3 0 4 56.07 1.82 1.6402 4 5 4 4 56.77 1.76 1.6217 5 7 0 4 57.07 4.39 1.6138 5 1 5 4 57.29 1.93 1.6081 3 8 1 4 57.60 1.57 1.6003 6 3 4 4 57.81 1.06 1.5950 3 6 4 4 59.51 1.19 1.5533 1 3 6 4 59.71 2.73 1.5487 3 8 2 4 59.81 1.92 1.5463 7 5 2 4 59.93 1.19 1.5435 1 7 4 4 59.99 1.33 1.5420 5 7 2 4 60.12 1.50 1.5390 4 8 1 4 60.44 1.17 1.5316 9 1 1 4 60.48 1.30 1.5308 1 8 3 4 60.71 2.22 1.5256 2 3 6 4 61.09 1.04 1.5168 6 0 5 4 61.12 1.12 1.5163 2 7 4 4 62.22 1.44 1.4921 4 1 6 4 64.29 2.66 1.4488 6 7 2 4 65.52 1.85 1.4247 7 4 4 4 66.28 1.25 1.4102 4 8 3 4 69.77 1.45 1.3479 9 5 1 4 70.76 1.30 1.3315 10 3 1 4 71.74 1.12 1.3156 2 10 2 4 73.36 1.27 1.2905 2 9 4 4 75.61 1.27 1.2577 5 7 5 4 78.06 1.05 1.2242 5 3 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.