K3.73 Nb8.41 O34 P4.47 W0.12 Leclaire A, Borel M, Mezaoui D, Rebbah H, Raveau B Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences 323 (1996) 679-685 Introduction of tungsten in the niobium phosphate bronzes: the monophosphate K3.75 Nb8-x Wx O14 (P O4)4 (P0.5 Nb0.5 O4) _cod_database_code 1001732 _database_code_amcsd 0012319 CELL PARAMETERS: 10.6265 10.6265 6.4092 90.000 90.000 90.000 SPACE GROUP: P-4m2 X-RAY WAVELENGTH: 1.541838 Cell Volume: 723.743 Density (g/cm3): 3.744 MAX. ABS. INTENSITY / VOLUME**2: 38.67651216 RIR: 3.364 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.82 34.52 6.4092 0 0 1 2 16.15 37.98 5.4882 1 0 1 4 16.69 10.87 5.3133 2 0 0 4 18.19 2.88 4.8763 1 1 1 8 21.73 40.02 4.0904 2 0 1 4 23.30 16.87 3.8174 2 1 1 8 23.68 10.40 3.7570 2 2 0 4 25.14 100.00 3.5422 3 0 0 4 27.52 2.64 3.2412 2 2 1 8 27.84 7.47 3.2046 0 0 2 2 28.80 38.77 3.1002 3 0 1 4 29.11 11.11 3.0681 1 0 2 4 30.03 14.40 2.9761 3 1 1 8 30.32 18.36 2.9477 1 1 2 8 30.33 1.80 2.9473 3 2 0 8 32.63 20.00 2.7441 2 0 2 4 33.46 20.95 2.6777 3 2 1 8 33.73 11.38 2.6570 2 1 2 8 33.74 4.68 2.6566 4 0 0 4 35.85 14.27 2.5047 3 3 0 4 36.62 5.82 2.4542 4 0 1 4 36.87 13.85 2.4381 2 2 2 8 37.86 1.33 2.3764 3 0 2 4 38.59 6.27 2.3329 3 3 1 8 38.83 2.83 2.3191 3 1 2 8 41.63 1.83 2.1693 3 2 2 8 42.54 7.03 2.1253 5 0 0 4 43.19 4.76 2.0945 1 0 3 4 44.29 3.29 2.0452 4 0 2 4 44.93 6.62 2.0173 5 0 1 4 44.93 2.88 2.0173 4 3 1 8 45.15 3.80 2.0084 4 1 2 8 45.78 2.54 1.9822 2 0 3 4 45.78 1.83 1.9819 5 1 1 8 46.61 8.65 1.9486 2 1 3 8 47.64 1.83 1.9087 4 2 2 8 49.05 2.51 1.8571 2 2 3 8 49.85 1.71 1.8294 3 0 3 4 50.05 3.47 1.8224 5 3 0 8 50.63 6.66 1.8029 3 1 3 8 51.60 6.39 1.7712 5 0 2 4 51.60 2.18 1.7712 4 3 2 8 51.61 13.25 1.7711 6 0 0 4 52.18 9.09 1.7529 5 3 1 8 52.37 13.02 1.7471 5 1 2 8 52.93 5.08 1.7298 3 2 3 8 53.69 10.47 1.7071 6 0 1 4 54.44 1.40 1.6855 6 1 1 8 54.62 11.56 1.6803 5 2 2 8 55.17 3.10 1.6648 4 0 3 4 55.90 1.56 1.6448 4 1 3 8 56.63 7.09 1.6253 6 2 1 8 57.52 4.05 1.6023 0 0 4 2 58.06 5.16 1.5887 4 2 3 8 58.23 1.98 1.5844 1 0 4 4 58.24 1.38 1.5842 5 3 2 8 58.24 9.31 1.5841 6 3 0 8 60.17 7.00 1.5378 6 3 1 8 60.34 2.49 1.5341 2 0 4 4 60.34 1.54 1.5339 6 1 2 8 61.04 1.30 1.5181 7 0 0 4 61.55 1.74 1.5067 5 0 3 4 61.55 1.17 1.5067 4 3 3 8 62.23 2.77 1.4918 5 1 3 8 63.08 1.41 1.4739 2 2 4 8 63.08 2.62 1.4737 5 4 2 8 63.75 4.25 1.4599 3 0 4 4 64.26 5.30 1.4496 5 2 3 8 64.42 1.00 1.4463 3 1 4 8 66.41 1.02 1.4077 3 2 4 8 67.56 4.07 1.3865 5 3 3 8 68.86 1.66 1.3635 6 0 3 4 69.03 1.32 1.3606 7 1 2 8 69.03 6.01 1.3606 5 5 2 8 69.66 2.08 1.3497 3 3 4 8 70.31 1.71 1.3389 6 4 2 8 70.79 3.31 1.3309 6 5 1 8 71.43 2.80 1.3207 6 2 3 8 72.06 2.89 1.3106 5 4 3 8 72.70 2.71 1.3007 8 0 1 4 74.11 1.97 1.2794 5 0 4 4 75.99 3.86 1.2523 6 6 0 4 77.69 1.46 1.2292 5 5 3 8 78.31 2.23 1.2210 8 3 1 8 78.46 1.41 1.2190 8 1 2 8 79.52 3.13 1.2053 3 0 5 4 79.68 1.02 1.2033 5 3 4 8 80.90 1.96 1.1882 6 0 4 4 81.52 1.49 1.1807 9 0 0 4 83.20 1.99 1.1612 9 0 1 4 84.41 1.37 1.1476 6 5 3 8 85.00 2.15 1.1411 3 3 5 8 85.62 1.15 1.1344 9 2 1 8 86.22 1.33 1.1280 8 0 3 4 86.37 2.44 1.1265 6 3 4 8 86.83 1.47 1.1217 8 1 3 8 86.98 1.97 1.1201 9 3 0 8 87.58 1.62 1.1140 8 4 2 8 88.64 3.16 1.1035 8 2 3 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.