Rakovanite Duraisamy T, Ramanan A, Vittal J J Crystal Engineering 3 (2000) 237-250 Novel self-assembled decavanadate clusters forming 1D molecular chains and 2D molecular arrays: [HMTA-H...H2O][HMTA-CH2OH][H3V10O28{Na(H2O)4}]*4H2O and [Na2(H2O)10] [H3V10O28 {Na(H2O)2}]*3H2O Locality: Synthetic _database_code_amcsd 0018393 CELL PARAMETERS: 12.0627 17.1745 18.2094 90.000 106.340 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 3620.084 Density (g/cm3): 2.379 MAX. ABS. INTENSITY / VOLUME**2: 13.85782937 RIR: 1.897 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.89 100.00 11.2109 -1 0 1 2 9.21 9.35 9.5988 1 1 0 4 9.42 6.06 9.3878 -1 1 1 4 10.12 28.51 8.7370 0 0 2 2 10.29 60.30 8.6003 1 0 1 2 11.48 96.33 7.7069 0 2 1 4 11.51 1.69 7.6900 1 1 1 4 12.84 67.71 6.8967 1 2 0 4 14.97 3.36 5.9172 -1 2 2 4 14.98 2.64 5.9138 -1 0 3 2 15.31 6.43 5.7877 2 0 0 2 15.81 3.64 5.6055 -2 0 2 2 18.41 2.01 4.8204 0 2 3 4 18.88 1.87 4.6992 1 0 3 2 20.30 2.81 4.3747 2 2 1 4 20.33 3.30 4.3685 0 0 4 2 21.06 1.99 4.2183 -2 2 3 4 21.84 1.11 4.0701 2 3 0 4 22.15 2.08 4.0129 -3 0 1 2 22.19 2.69 4.0065 -1 2 4 4 22.76 1.17 3.9077 -3 1 1 4 23.15 15.57 3.8415 1 4 1 4 23.40 1.85 3.8013 2 3 1 4 24.45 1.01 3.6410 -1 0 5 2 25.64 2.66 3.4745 -1 4 3 4 25.84 12.94 3.4483 2 4 0 4 26.68 3.19 3.3412 -3 1 4 4 26.68 2.74 3.3411 2 2 3 4 27.56 2.89 3.2370 0 2 5 4 28.18 1.10 3.1663 -3 2 4 4 28.27 2.65 3.1568 3 1 2 4 29.26 1.62 3.0526 -3 0 5 2 29.40 14.77 3.0383 2 4 2 4 29.53 1.96 3.0247 3 3 1 4 29.70 1.53 3.0080 3 2 2 4 29.73 1.61 3.0055 -3 1 5 4 29.95 1.27 2.9838 -2 5 1 4 30.21 15.25 2.9586 -2 4 4 4 30.26 2.81 2.9539 2 5 0 4 30.49 1.10 2.9318 -3 4 1 4 30.70 13.84 2.9123 0 0 6 2 30.83 1.80 2.9001 -4 1 3 4 31.27 3.65 2.8602 -1 2 6 4 31.43 1.54 2.8462 2 5 1 4 31.64 1.07 2.8276 3 1 3 4 31.74 2.60 2.8188 -3 4 3 4 31.93 4.61 2.8027 -4 0 4 2 31.94 1.19 2.8017 -2 5 3 4 31.95 2.46 2.8009 3 3 2 4 32.21 2.39 2.7787 1 6 0 4 32.24 1.48 2.7770 -1 4 5 4 32.37 2.74 2.7661 -4 1 4 4 32.66 2.05 2.7417 3 4 1 4 33.16 1.59 2.7012 -1 6 2 4 33.18 1.39 2.6997 4 1 1 4 34.53 3.04 2.5978 1 6 2 4 34.63 1.36 2.5903 -4 1 5 4 35.31 6.13 2.5419 4 0 2 2 35.67 1.29 2.5172 -4 3 4 4 35.71 3.80 2.5145 4 1 2 4 36.91 15.75 2.4353 -2 4 6 4 36.92 1.18 2.4349 -2 5 5 4 37.52 1.17 2.3970 0 2 7 4 37.76 1.18 2.3826 -4 3 5 4 38.80 4.32 2.3208 4 1 3 4 39.49 1.58 2.2817 -3 5 5 4 40.24 3.28 2.2410 -2 5 6 4 40.75 1.17 2.2144 0 6 5 4 40.96 6.02 2.2035 -2 6 5 4 41.08 1.25 2.1971 5 1 1 4 41.19 1.05 2.1914 -3 6 4 4 42.02 2.36 2.1501 4 0 4 2 42.09 1.42 2.1468 0 8 0 2 42.37 1.39 2.1332 -3 5 6 4 42.75 2.77 2.1154 -3 4 7 4 43.47 7.84 2.0819 -1 6 6 4 43.48 6.23 2.0811 5 1 2 4 44.00 2.12 2.0578 -2 5 7 4 46.02 11.25 1.9724 -3 6 6 4 46.40 6.69 1.9568 5 1 3 4 47.55 5.30 1.9124 -2 6 7 4 47.55 1.34 1.9124 -3 7 5 4 47.87 1.07 1.9001 -2 8 4 4 48.20 1.26 1.8882 -2 7 6 4 49.78 1.92 1.8318 5 1 4 4 50.05 2.44 1.8223 -3 7 6 4 52.69 2.65 1.7372 -2 8 6 4 52.82 1.91 1.7334 -6 5 3 4 53.27 3.27 1.7195 2 4 8 4 53.35 1.21 1.7173 -6 5 4 4 53.62 1.87 1.7092 0 10 1 4 53.97 1.28 1.6989 1 10 0 4 54.40 1.24 1.6864 6 1 3 4 55.22 1.64 1.6635 1 6 8 4 60.07 1.43 1.5403 -7 5 3 4 60.34 1.02 1.5340 -7 5 4 4 60.96 1.11 1.5197 6 5 3 4 63.47 1.57 1.4655 3 6 8 4 63.60 1.31 1.4629 2 6 9 4 65.18 2.60 1.4312 0 12 0 2 65.24 1.03 1.4301 -2 4 12 4 65.67 1.07 1.4218 -5 1 12 4 66.03 1.59 1.4149 0 10 7 4 66.28 1.47 1.4102 -7 7 3 4 66.54 1.06 1.4053 -7 7 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.