Sulfur Debaerdemaeker T, Kutoglu A Crystal Structure Communications 3 (1974) 611-613 Cyclooctadecasulfur, S18 (beta) Locality: synthetic Note: beta phase _database_code_amcsd 0012330 CELL PARAMETERS: 10.7500 7.2500 12.2500 90.000 92.300 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 953.965 Density (g/cm3): 2.009 MAX. ABS. INTENSITY / VOLUME**2: 4.894468852 RIR: 0.793 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.20 5.67 6.2379 0 1 1 4 14.74 1.27 6.0093 1 1 0 4 16.29 25.77 5.4428 -1 1 1 4 16.51 7.45 5.3707 2 0 0 2 18.98 11.83 4.6766 0 1 2 4 20.48 21.66 4.3368 -1 1 2 4 20.58 4.90 4.3156 2 1 0 4 20.95 60.98 4.2405 1 1 2 4 21.57 33.07 4.1195 -2 0 2 2 21.61 5.51 4.1118 -2 1 1 4 22.06 24.33 4.0295 2 1 1 4 22.46 46.62 3.9587 2 0 2 2 23.00 100.00 3.8660 -1 0 3 2 23.64 11.29 3.7643 1 0 3 2 24.56 52.32 3.6250 0 2 0 2 24.86 2.75 3.5817 -2 1 2 4 25.04 5.43 3.5557 0 1 3 4 25.64 15.82 3.4745 2 1 2 4 25.64 11.68 3.4742 -3 0 1 2 26.12 13.27 3.4113 -1 1 3 4 26.21 37.29 3.3999 3 0 1 2 26.68 37.40 3.3409 1 1 3 4 26.87 17.96 3.3180 -1 2 1 4 27.05 10.26 3.2960 1 2 1 4 27.79 7.47 3.2103 3 1 0 4 28.49 51.29 3.1331 -3 1 1 4 28.62 3.01 3.1189 0 2 2 4 29.01 11.79 3.0782 3 1 1 4 29.18 3.29 3.0600 0 0 4 2 29.64 1.47 3.0137 -2 1 3 4 29.66 22.98 3.0118 -1 2 2 4 29.73 26.66 3.0046 2 2 0 4 30.00 1.76 2.9790 1 2 2 4 30.47 2.16 2.9333 -2 2 1 4 30.64 2.67 2.9182 2 1 3 4 30.80 9.59 2.9029 2 2 1 4 31.74 18.67 2.8192 0 1 4 4 32.91 11.31 2.7214 -2 2 2 4 33.06 4.27 2.7099 0 2 3 4 33.15 21.46 2.7024 1 1 4 4 33.37 19.17 2.6853 4 0 0 2 33.90 25.35 2.6444 -1 2 3 4 34.31 1.30 2.6140 2 0 4 2 34.34 8.83 2.6111 1 2 3 4 35.80 15.69 2.5083 -3 2 1 4 36.15 2.15 2.4850 -4 1 1 4 36.22 1.71 2.4798 3 2 1 4 36.54 1.47 2.4591 2 1 4 4 36.71 2.97 2.4484 4 1 1 4 36.75 14.55 2.4457 -2 2 3 4 37.10 5.94 2.4235 4 0 2 2 37.57 1.56 2.3939 2 2 3 4 37.87 1.18 2.3760 -3 2 2 4 38.03 4.01 2.3663 1 0 5 2 38.13 1.20 2.3602 -4 1 2 4 38.50 9.38 2.3383 0 2 4 4 38.83 1.91 2.3194 0 1 5 4 38.83 3.09 2.3190 -1 3 1 4 39.43 1.43 2.2851 -1 1 5 4 39.97 1.81 2.2559 -3 1 4 4 40.95 1.53 2.2038 2 3 0 4 41.24 1.94 2.1891 -3 2 3 4 41.49 8.45 2.1762 3 1 4 4 41.51 1.15 2.1752 -2 3 1 4 41.65 12.44 2.1684 -2 2 4 4 41.87 11.58 2.1578 4 2 0 4 42.30 5.05 2.1368 -4 2 1 4 42.36 3.63 2.1336 3 2 3 4 42.64 2.77 2.1202 2 2 4 4 42.79 2.54 2.1134 4 2 1 4 42.91 1.26 2.1077 4 1 3 4 43.07 6.01 2.1004 2 1 5 4 43.41 1.28 2.0845 -2 3 2 4 43.96 2.04 2.0597 -3 0 5 2 44.05 2.19 2.0559 -4 2 2 4 44.20 4.94 2.0492 -1 3 3 4 44.99 3.78 2.0147 4 2 2 4 45.69 1.02 1.9859 -3 2 4 4 45.94 1.29 1.9753 -5 1 2 4 46.08 7.61 1.9698 3 3 1 4 47.00 1.30 1.9334 -4 2 3 4 47.01 6.84 1.9331 -5 0 3 2 47.01 2.78 1.9330 -2 0 6 2 47.38 1.38 1.9187 1 1 6 4 47.51 2.85 1.9137 3 1 5 4 47.62 1.07 1.9095 4 1 4 4 48.35 1.77 1.8825 4 2 3 4 48.36 1.91 1.8822 2 0 6 2 48.54 1.56 1.8757 -1 3 4 4 48.69 6.78 1.8702 5 0 3 2 50.18 2.46 1.8182 5 2 1 4 50.34 4.37 1.8125 0 4 0 2 50.64 7.54 1.8024 -2 3 4 4 51.00 4.59 1.7909 -4 2 4 4 51.00 1.94 1.7908 -3 2 5 4 51.01 3.65 1.7902 6 0 0 2 51.13 1.32 1.7864 -5 2 2 4 51.26 4.85 1.7823 3 3 3 4 51.40 8.41 1.7778 0 2 6 4 51.50 3.71 1.7745 2 3 4 4 51.63 1.35 1.7702 -1 4 1 4 52.19 1.19 1.7525 5 2 2 4 52.26 1.20 1.7505 -3 1 6 4 52.58 1.22 1.7404 3 2 5 4 52.60 2.38 1.7400 -5 1 4 4 52.66 1.21 1.7380 6 1 0 4 52.69 2.15 1.7371 -6 0 2 2 52.70 1.57 1.7370 -1 0 7 2 52.72 5.29 1.7363 -4 3 2 4 52.92 1.75 1.7302 -6 1 1 4 53.30 3.63 1.7187 -1 4 2 4 53.35 1.69 1.7173 2 4 0 4 53.43 3.97 1.7150 1 0 7 2 53.74 12.23 1.7057 -5 2 3 4 53.74 2.25 1.7057 -1 3 5 4 53.74 4.47 1.7057 -2 2 6 4 53.94 1.37 1.6999 6 0 2 2 53.94 6.77 1.6998 0 1 7 4 54.01 3.82 1.6977 2 4 1 4 54.13 1.59 1.6944 3 1 6 4 54.25 5.58 1.6908 1 3 5 4 54.31 1.49 1.6892 -1 1 7 4 54.66 4.03 1.6790 5 1 4 4 54.97 1.45 1.6704 2 2 6 4 55.27 4.84 1.6620 5 2 3 4 55.32 1.09 1.6606 -4 3 3 4 55.38 1.41 1.6590 3 3 4 4 55.47 2.33 1.6564 0 4 3 4 55.78 5.42 1.6480 2 4 2 4 56.04 4.27 1.6411 -1 4 3 4 56.11 6.85 1.6391 -2 1 7 4 57.34 1.19 1.6070 -3 4 1 4 57.41 2.12 1.6052 6 2 0 4 57.50 1.07 1.6027 2 1 7 4 57.68 1.40 1.5982 -5 3 1 4 57.85 2.68 1.5939 4 0 6 2 58.00 1.68 1.5902 -2 4 3 4 58.17 5.37 1.5858 5 3 1 4 58.61 1.34 1.5749 0 2 7 4 58.92 3.72 1.5676 -3 3 5 4 59.78 1.06 1.5470 5 1 5 4 60.51 1.74 1.5302 -7 0 1 2 61.17 1.15 1.5151 7 0 1 2 62.08 3.11 1.4952 -4 4 1 4 62.34 1.70 1.4895 2 4 4 4 62.64 2.25 1.4830 7 1 1 4 62.87 1.47 1.4782 -5 1 6 4 63.19 1.60 1.4714 -7 1 2 4 63.63 1.59 1.4623 -4 1 7 4 63.79 3.88 1.4591 4 2 6 4 64.18 1.04 1.4511 5 2 5 4 64.49 1.18 1.4449 7 1 2 4 65.64 1.18 1.4223 5 1 6 4 66.30 1.69 1.4097 -7 2 1 4 66.78 3.09 1.4009 6 2 4 4 66.79 1.62 1.4006 -1 5 2 4 68.31 1.29 1.3732 -6 0 6 2 68.53 1.23 1.3692 -7 1 4 4 68.97 1.01 1.3615 2 5 2 4 69.29 1.22 1.3560 -1 0 9 2 69.47 1.57 1.3531 1 5 3 4 70.36 1.54 1.3381 -3 5 1 4 70.62 1.47 1.3338 3 5 1 4 72.08 1.10 1.3103 0 5 4 4 72.19 1.23 1.3086 3 5 2 4 73.04 1.11 1.2954 3 2 8 4 73.79 1.80 1.2841 -6 2 6 4 74.74 1.35 1.2701 -1 2 9 4 76.24 1.09 1.2488 5 2 7 4 76.36 1.21 1.2472 2 3 8 4 79.63 1.05 1.2039 -2 0 10 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.