Zdenekite Zubkova N V, Pushcharovsky D Y, Sarp H, Teat S J, MacLean E J Crystallography Reports 48 (2003) 939-943 Crystal structure of zdenekite NaPbCu5(AsO4)4Cl*5H2O Locality: Cap Garrone copper-lead mine, France _database_code_amcsd 0012387 CELL PARAMETERS: 10.0230 19.5500 10.0230 90.000 90.020 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1964.003 Density (g/cm3): 4.193 MAX. ABS. INTENSITY / VOLUME**2: 28.18180377 RIR: 2.189 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.05 100.00 9.7750 0 2 0 2 9.92 10.30 8.9191 1 1 0 4 9.92 5.16 8.9191 0 1 1 4 12.49 1.18 7.0861 1 0 1 2 12.65 4.01 6.9980 1 2 0 4 12.65 59.83 6.9980 0 2 1 4 15.44 2.64 5.7385 -1 2 1 4 15.44 15.45 5.7372 1 2 1 4 18.15 19.21 4.8875 0 4 0 2 18.27 3.34 4.8545 2 1 0 4 18.49 10.68 4.7974 -1 3 1 4 18.50 4.65 4.7967 1 3 1 4 19.91 2.81 4.4596 2 2 0 4 19.91 31.44 4.4596 0 2 2 4 20.21 38.60 4.3930 0 4 1 4 20.32 17.09 4.3696 -2 1 1 4 20.32 5.08 4.3696 -1 1 2 4 20.33 14.51 4.3685 2 1 1 4 21.81 2.27 4.0749 -1 2 2 4 21.82 5.58 4.0740 1 2 2 4 21.82 1.75 4.0740 2 2 1 4 22.09 5.62 4.0233 1 4 1 4 22.38 29.18 3.9726 2 3 0 4 22.38 6.57 3.9726 0 3 2 4 24.44 2.75 3.6426 0 5 1 4 25.13 4.05 3.5430 2 0 2 2 25.54 2.83 3.4874 -2 1 2 4 25.55 2.32 3.4863 2 1 2 4 26.03 1.09 3.4237 -1 5 1 4 26.76 3.90 3.3310 2 2 2 4 26.99 2.02 3.3037 -1 4 2 4 26.99 5.72 3.3032 1 4 2 4 27.08 10.25 3.2933 3 1 0 4 28.15 1.19 3.1699 -3 0 1 2 28.16 2.02 3.1692 1 0 3 2 28.23 8.01 3.1614 3 2 0 4 28.23 2.47 3.1614 0 2 3 4 28.53 4.87 3.1290 -1 1 3 4 28.53 2.97 3.1290 -3 1 1 4 28.53 3.94 3.1284 3 1 1 4 28.67 48.95 3.1136 -2 3 2 4 28.68 35.07 3.1127 2 3 2 4 28.81 3.44 3.0987 1 6 0 4 28.81 4.96 3.0987 0 6 1 4 28.96 24.41 3.0827 2 5 0 4 28.96 3.75 3.0827 0 5 2 4 30.06 25.85 2.9730 3 3 0 4 30.06 13.49 2.9730 0 3 3 4 30.33 2.80 2.9467 -2 5 1 4 30.33 5.61 2.9467 -1 5 2 4 30.34 1.86 2.9463 2 5 1 4 31.17 4.03 2.8693 -2 4 2 4 31.18 16.71 2.8686 2 4 2 4 31.38 1.26 2.8505 -1 3 3 4 31.39 1.14 2.8501 3 3 1 4 32.46 17.37 2.7582 0 4 3 4 32.53 13.10 2.7526 -2 1 3 4 32.54 7.07 2.7518 2 1 3 4 32.54 1.41 2.7518 3 1 2 4 32.78 1.77 2.7317 2 6 0 4 32.78 26.50 2.7317 0 6 2 4 33.30 1.64 2.6904 1 7 0 4 33.51 3.16 2.6743 -2 2 3 4 33.51 1.98 2.6743 -3 2 2 4 33.52 15.08 2.6735 2 2 3 4 34.02 3.70 2.6355 1 6 2 4 34.14 10.89 2.6260 -2 5 2 4 34.15 8.65 2.6255 2 5 2 4 35.09 6.96 2.5573 -2 3 3 4 35.09 4.43 2.5573 -3 3 2 4 35.10 3.12 2.5566 2 3 3 4 35.10 3.79 2.5566 3 3 2 4 35.34 1.99 2.5400 0 5 3 4 35.84 13.52 2.5057 4 0 0 2 35.84 4.50 2.5057 0 0 4 2 36.14 1.56 2.4854 4 1 0 4 36.14 9.98 2.4854 0 1 4 4 36.49 1.66 2.4623 -3 5 1 4 36.49 1.64 2.4623 -1 5 3 4 36.50 3.19 2.4620 3 5 1 4 36.84 15.81 2.4396 2 7 0 4 36.84 3.82 2.4396 0 7 2 4 37.21 7.43 2.4167 -3 4 2 4 37.27 2.73 2.4126 -1 1 4 4 37.90 2.41 2.3742 1 8 0 4 37.90 1.32 2.3742 0 8 1 4 37.96 9.24 2.3705 -2 7 1 4 37.96 8.74 2.3703 2 7 1 4 38.14 1.00 2.3593 -4 2 1 4 38.15 4.45 2.3589 1 2 4 4 38.99 1.29 2.3103 -1 8 1 4 39.67 1.65 2.2721 -3 6 1 4 39.67 3.95 2.2718 1 6 3 4 39.78 2.19 2.2659 -3 5 2 4 39.79 14.39 2.2654 3 5 2 4 40.23 2.91 2.2415 -4 0 2 2 40.24 1.34 2.2409 2 0 4 2 40.45 1.10 2.2298 0 4 4 4 41.15 1.40 2.1936 -2 7 2 4 41.16 1.05 2.1934 2 7 2 4 41.32 1.38 2.1848 -4 2 2 4 41.34 1.80 2.1842 2 2 4 4 41.48 4.18 2.1767 -4 4 1 4 41.49 3.68 2.1764 4 4 1 4 42.12 2.13 2.1455 2 8 1 4 42.59 1.06 2.1229 1 9 0 4 42.66 2.12 2.1196 -2 3 4 4 42.67 1.43 2.1191 4 3 2 4 42.75 1.66 2.1150 -3 6 2 4 43.17 2.24 2.0955 -1 7 3 4 43.86 2.15 2.0643 4 5 1 4 44.47 2.29 2.0375 -4 4 2 4 44.48 1.03 2.0370 2 4 4 4 44.48 1.29 2.0370 4 4 2 4 45.49 4.95 1.9941 0 1 5 4 45.49 1.27 1.9938 4 1 3 4 45.51 4.44 1.9931 2 9 0 4 46.01 3.27 1.9724 0 8 3 4 46.06 2.58 1.9704 -2 7 3 4 46.07 1.59 1.9701 2 7 3 4 46.22 1.04 1.9640 -4 2 3 4 46.22 1.40 1.9640 -3 2 4 4 46.23 1.74 1.9637 0 2 5 4 46.45 2.30 1.9548 -2 9 1 4 46.45 1.22 1.9548 -1 9 2 4 46.46 1.33 1.9547 2 9 1 4 46.61 1.26 1.9485 -4 6 1 4 46.62 1.22 1.9483 4 6 1 4 46.62 1.89 1.9483 1 6 4 4 47.16 1.60 1.9272 -5 2 1 4 47.16 1.32 1.9270 1 2 5 4 47.16 1.50 1.9270 5 2 1 4 47.38 4.69 1.9188 0 10 1 4 47.45 1.16 1.9160 0 3 5 4 47.53 1.79 1.9128 -3 6 3 4 48.36 1.58 1.8820 -1 3 5 4 49.11 3.97 1.8549 -4 4 3 4 49.12 1.45 1.8547 5 4 0 4 49.35 1.59 1.8467 -2 6 4 4 49.35 4.53 1.8467 -4 6 2 4 49.36 4.42 1.8464 2 6 4 4 49.36 2.33 1.8464 4 6 2 4 49.68 1.58 1.8353 2 8 3 4 49.72 2.35 1.8337 -1 7 4 4 49.87 2.41 1.8286 -5 2 2 4 49.88 4.59 1.8282 5 2 2 4 50.08 6.29 1.8213 0 10 2 4 50.97 1.86 1.7917 3 9 1 4 51.03 1.49 1.7899 -2 3 5 4 51.03 1.07 1.7899 -5 3 2 4 51.21 1.48 1.7838 0 5 5 4 51.22 1.71 1.7836 4 5 3 4 51.57 6.64 1.7721 -4 0 4 2 51.80 2.05 1.7649 -4 1 4 4 51.82 10.81 1.7643 4 1 4 4 52.34 1.91 1.7481 -2 7 4 4 52.34 1.88 1.7478 4 7 2 4 52.61 2.23 1.7396 -2 4 5 4 52.62 4.18 1.7392 2 4 5 4 53.15 1.41 1.7234 1 8 4 4 53.28 1.70 1.7192 -3 0 5 2 53.68 2.25 1.7074 5 6 0 4 53.68 1.05 1.7074 0 6 5 4 54.52 1.33 1.6832 -5 6 1 4 54.52 1.06 1.6830 5 6 1 4 54.52 1.12 1.6830 1 6 5 4 54.80 2.80 1.6751 2 11 0 4 55.18 2.29 1.6644 6 1 0 4 55.18 2.43 1.6644 0 1 6 4 55.63 1.10 1.6522 -1 11 2 4 56.00 1.08 1.6420 -6 1 1 4 56.03 1.50 1.6413 0 9 4 4 56.48 1.49 1.6292 0 12 0 2 56.51 2.80 1.6285 0 7 5 4 56.52 1.07 1.6283 4 7 3 4 56.76 1.19 1.6218 -3 4 5 4 56.84 1.37 1.6198 -1 9 4 4 56.90 1.14 1.6182 6 3 0 4 56.90 1.36 1.6182 0 3 6 4 57.65 1.10 1.5989 3 9 3 4 58.06 4.52 1.5887 -2 11 2 4 58.06 3.00 1.5886 2 11 2 4 59.04 2.07 1.5645 -2 2 6 4 59.06 2.72 1.5642 2 2 6 4 59.06 1.68 1.5642 6 2 2 4 59.23 1.14 1.5601 4 1 5 4 59.37 1.09 1.5568 -4 6 4 4 59.65 2.36 1.5500 -4 8 3 4 59.66 8.84 1.5499 5 8 0 4 60.02 1.10 1.5414 4 10 0 4 60.08 3.84 1.5400 -6 3 2 4 60.09 1.10 1.5397 6 3 2 4 60.80 2.46 1.5235 -4 10 1 4 61.51 1.33 1.5076 -2 4 6 4 61.52 1.38 1.5074 2 4 6 4 62.75 2.24 1.4808 -2 8 5 4 62.75 1.03 1.4808 -5 8 2 4 62.76 4.86 1.4806 2 8 5 4 62.76 1.07 1.4806 5 8 2 4 62.78 2.25 1.4802 2 12 2 4 63.10 1.23 1.4733 -4 10 2 4 63.11 3.18 1.4732 0 9 5 4 64.09 1.46 1.4530 4 5 5 4 66.08 2.37 1.4140 -5 1 5 4 66.10 1.84 1.4135 5 1 5 4 66.85 1.64 1.3996 5 10 0 4 66.91 1.50 1.3985 7 3 0 4 67.68 3.21 1.3844 -2 13 2 4 67.68 1.73 1.3843 2 13 2 4 67.75 2.04 1.3831 0 14 1 4 68.32 1.26 1.3729 4 9 4 4 68.41 1.19 1.3713 3 13 0 4 68.86 2.73 1.3634 -2 2 7 4 68.88 2.71 1.3632 2 2 7 4 69.82 1.47 1.3471 -7 3 2 4 69.83 1.83 1.3469 7 3 2 4 69.97 1.45 1.3445 0 5 7 4 70.68 1.29 1.3328 -5 5 5 4 70.86 1.24 1.3299 0 11 5 4 71.62 1.01 1.3176 -6 7 3 4 72.83 1.17 1.2987 -7 5 2 4 72.84 1.05 1.2985 7 5 2 4 74.46 2.10 1.2742 0 7 7 4 78.24 2.13 1.2219 0 16 0 2 78.37 1.23 1.2202 3 6 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.