Rb(VO2)(HPO4) Amoros P, Beltran-Porter D, Le Bail A, Ferey G, Villeneuve G European Journal of Solid State and Inorganic Chemistry 25 (1988) 599-607 Crystal structure of A(VO2)(HPO4)(A=NH4,K,Rb) solved from X-ray powder diffraction _cod_database_code 1000081 _database_code_amcsd 0012525 CELL PARAMETERS: 6.8182 9.2910 17.6310 90.000 90.000 90.000 SPACE GROUP: Pbca X-RAY WAVELENGTH: 1.541838 Cell Volume: 1116.887 Density (g/cm3): 3.132 MAX. ABS. INTENSITY / VOLUME**2: 14.49488713 RIR: 1.507 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.03 32.37 8.8155 0 0 2 2 16.44 11.63 5.3933 1 0 2 4 16.90 4.45 5.2477 1 1 1 8 19.10 1.55 4.6455 0 2 0 2 19.76 15.62 4.4922 0 2 1 4 20.15 6.11 4.4078 0 0 4 2 21.62 50.73 4.1098 0 2 2 4 23.72 100.00 3.7512 1 2 1 8 24.42 15.50 3.6444 0 2 3 4 25.30 57.77 3.5198 1 2 2 8 25.91 1.32 3.4387 1 1 4 8 26.14 10.11 3.4091 2 0 0 2 27.76 12.19 3.2141 1 2 3 8 27.88 11.35 3.2005 2 1 0 4 27.90 42.23 3.1975 0 2 4 4 28.06 70.49 3.1796 2 0 2 4 29.70 4.85 3.0083 2 1 2 8 30.11 8.19 2.9680 1 1 5 8 30.42 51.95 2.9385 0 0 6 2 30.89 13.63 2.8950 1 2 4 8 32.58 30.21 2.7484 2 2 0 4 32.98 6.48 2.7156 2 2 1 8 33.20 6.00 2.6985 1 0 6 4 33.22 43.81 2.6966 2 0 4 4 34.17 8.75 2.6239 2 2 2 8 34.54 62.50 2.5970 1 2 5 8 34.64 1.76 2.5898 2 1 4 8 36.08 7.71 2.4896 2 2 3 8 36.17 1.52 2.4834 0 2 6 4 38.58 6.14 2.3334 1 2 6 8 38.60 2.55 2.3322 2 2 4 8 39.12 34.86 2.3029 0 4 1 4 39.35 2.67 2.2898 1 1 7 8 40.15 1.38 2.2461 0 4 2 4 40.53 4.81 2.2258 2 0 6 4 40.95 6.99 2.2039 0 0 8 2 41.01 10.73 2.2008 3 0 2 4 41.21 1.43 2.1905 3 1 1 8 41.38 13.97 2.1818 1 4 1 8 41.73 7.09 2.1645 2 1 6 8 41.82 2.71 2.1602 0 4 3 4 42.32 1.74 2.1356 2 3 3 8 43.14 12.31 2.0970 1 0 8 4 44.07 1.81 2.0549 0 4 4 4 44.53 1.59 2.0345 1 3 6 8 44.69 5.05 2.0280 3 2 1 8 45.17 14.13 2.0073 2 2 6 8 45.56 1.79 1.9912 0 2 8 4 45.61 8.57 1.9889 3 2 2 8 47.57 4.17 1.9113 1 2 8 8 48.46 1.27 1.8784 1 3 7 8 48.66 1.27 1.8712 3 1 5 8 48.81 8.45 1.8657 1 4 5 8 49.06 2.26 1.8569 2 2 7 8 49.18 6.95 1.8525 3 2 4 8 49.23 1.43 1.8508 2 0 8 4 49.39 1.59 1.8453 1 1 9 8 49.98 25.25 1.8247 2 4 3 8 50.05 2.69 1.8225 3 3 1 8 50.57 2.15 1.8051 0 2 9 4 50.79 2.07 1.7978 3 0 6 4 51.74 10.29 1.7668 3 2 5 8 51.94 4.22 1.7604 1 4 6 8 52.44 4.62 1.7450 1 2 9 8 53.28 4.97 1.7194 2 2 8 8 53.68 14.28 1.7075 0 4 7 4 53.78 8.13 1.7046 4 0 0 2 54.42 1.00 1.6859 2 4 5 8 54.75 4.90 1.6766 4 1 0 4 54.86 1.07 1.6736 4 0 2 4 55.02 1.14 1.6690 4 1 1 8 55.34 2.41 1.6602 3 1 7 8 55.48 1.45 1.6564 1 4 7 8 55.77 6.79 1.6484 0 2 10 4 56.61 3.15 1.6259 3 3 5 8 56.92 5.20 1.6176 3 4 1 8 58.32 2.33 1.5822 3 0 8 4 58.63 1.59 1.5745 4 2 2 8 58.94 1.79 1.5670 4 1 4 8 58.98 13.73 1.5661 2 0 10 4 58.99 1.02 1.5657 3 4 3 8 59.90 1.12 1.5443 2 1 10 8 59.91 3.77 1.5440 4 2 3 8 60.13 2.15 1.5387 1 1 11 8 60.66 3.30 1.5267 2 4 7 8 61.17 1.27 1.5152 0 2 11 4 61.66 5.95 1.5042 4 2 4 8 61.96 1.43 1.4977 3 2 8 8 61.97 8.49 1.4974 0 6 3 4 62.39 5.13 1.4884 1 6 2 8 62.83 5.34 1.4791 1 2 11 8 63.00 3.00 1.4754 3 4 5 8 63.05 5.32 1.4744 4 0 6 4 63.30 1.25 1.4693 0 0 12 2 63.49 2.30 1.4653 3 1 9 8 63.62 3.16 1.4626 1 4 9 8 63.93 3.20 1.4562 4 1 6 8 64.92 1.30 1.4363 1 0 12 4 65.32 1.93 1.4285 1 6 4 8 66.10 2.04 1.4135 3 2 9 8 66.30 1.21 1.4099 2 6 0 4 66.34 1.87 1.4089 3 3 8 8 66.53 9.66 1.4054 2 6 1 8 68.36 3.49 1.3722 1 2 12 8 68.43 6.93 1.3711 2 4 9 8 68.48 5.54 1.3701 4 4 1 8 68.52 1.32 1.3694 2 5 7 8 69.75 1.95 1.3483 4 0 8 4 69.93 1.28 1.3453 5 1 1 8 70.06 2.05 1.3431 1 6 6 8 72.16 1.80 1.3091 2 6 5 8 73.02 2.06 1.2957 2 2 12 8 73.06 1.07 1.2952 1 4 11 8 73.12 1.88 1.2943 5 2 2 8 75.40 3.00 1.2607 3 2 11 8 75.44 2.08 1.2601 5 1 5 8 75.49 1.36 1.2594 0 0 14 2 75.95 1.35 1.2529 4 5 1 8 76.12 1.53 1.2505 3 4 9 8 76.47 2.15 1.2457 1 6 8 8 76.52 1.19 1.2449 5 3 1 8 77.20 1.55 1.2357 5 3 2 8 77.60 4.01 1.2303 2 4 11 8 77.60 5.83 1.2302 2 6 7 8 77.75 1.55 1.2284 4 5 3 8 78.77 1.01 1.2150 4 1 10 8 78.78 1.77 1.2148 0 6 9 4 79.44 4.49 1.2063 4 4 7 8 80.55 1.54 1.1925 3 2 12 8 81.17 3.79 1.1849 4 2 10 8 81.88 1.46 1.1765 5 3 5 8 82.33 2.52 1.1712 0 4 13 4 85.42 1.10 1.1366 3 7 2 8 85.53 3.73 1.1354 1 8 2 8 86.52 3.26 1.1250 4 6 3 8 86.60 1.62 1.1241 4 5 7 8 86.62 1.76 1.1239 1 2 15 8 87.43 1.18 1.1156 5 4 5 8 87.61 1.48 1.1137 0 6 11 4 88.05 1.04 1.1093 3 7 4 8 88.17 1.62 1.1081 1 8 4 8 88.31 1.39 1.1067 3 6 8 8 89.28 1.05 1.0972 2 8 1 8 89.74 1.34 1.0927 6 1 4 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.