CsSb2PO8 Crosnier M, Guyomard D, Verbaere A, Piffard Y European Journal of Solid State and Inorganic Chemistry 26 (1989) 529-538 Preparation and crystal structure of CsSb2PO8 _cod_database_code 1000281 _database_code_amcsd 0012529 CELL PARAMETERS: 18.1650 7.1540 13.6770 90.000 120.420 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1532.682 Density (g/cm3): 4.640 MAX. ABS. INTENSITY / VOLUME**2: 28.70456707 RIR: 2.014 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.50 8.57 11.7942 0 0 1 2 9.90 1.73 8.9343 -2 0 1 2 11.30 34.69 7.8322 2 0 0 2 13.47 4.35 6.5749 -2 0 2 2 13.61 49.29 6.5075 1 1 0 4 14.09 2.08 6.2842 -1 1 1 4 15.02 95.28 5.8971 0 0 2 2 16.45 7.67 5.3875 2 0 1 2 16.89 10.64 5.2497 1 1 1 4 18.05 13.11 4.9143 -1 1 2 4 19.23 1.04 4.6145 -3 1 1 4 19.88 52.67 4.4671 -4 0 2 2 19.95 2.42 4.4512 -4 0 1 2 20.27 17.94 4.3817 -3 1 2 4 21.06 5.83 4.2176 3 1 0 4 22.37 90.95 3.9736 1 1 2 4 22.52 18.77 3.9488 -4 0 3 2 22.62 3.43 3.9314 0 0 3 2 22.71 27.42 3.9161 4 0 0 2 23.02 26.67 3.8638 2 0 2 2 23.85 2.62 3.7301 -1 1 3 4 24.89 22.86 3.5770 0 2 0 2 25.17 1.59 3.5388 3 1 1 4 26.36 8.99 3.3811 -2 0 4 2 26.85 18.84 3.3207 -2 2 1 4 27.12 5.02 3.2875 -4 0 4 2 27.41 40.25 3.2537 2 2 0 4 28.39 3.87 3.1434 -5 1 1 4 28.41 100.00 3.1421 -2 2 2 4 28.78 32.82 3.1023 -5 1 3 4 29.00 5.73 3.0793 -3 1 4 4 29.20 20.79 3.0584 0 2 2 4 29.59 9.17 3.0193 -6 0 2 2 29.99 12.67 2.9800 2 2 1 4 30.01 37.77 2.9781 -6 0 3 2 30.16 9.18 2.9632 2 0 3 2 30.31 23.18 2.9485 0 0 4 2 30.54 85.47 2.9271 -1 1 4 4 30.69 2.09 2.9128 3 1 2 4 31.11 33.34 2.8746 -6 0 1 2 31.17 1.28 2.8698 5 1 0 4 31.87 28.19 2.8080 -5 1 4 4 32.10 32.07 2.7883 -4 2 1 4 33.26 2.35 2.6937 4 0 2 2 33.81 2.04 2.6510 -4 2 3 4 33.94 51.26 2.6411 4 2 0 4 35.19 9.08 2.5505 -3 1 5 4 35.46 13.59 2.5317 5 1 1 4 36.15 4.63 2.4845 -6 0 5 2 36.40 2.75 2.4685 -5 1 5 4 36.57 1.18 2.4571 -2 2 4 4 36.93 2.95 2.4338 -7 1 3 4 37.14 2.31 2.4205 -4 2 4 4 37.21 5.73 2.4165 -7 1 2 4 37.35 20.67 2.4079 4 2 1 4 38.15 2.93 2.3588 0 0 5 2 38.92 4.32 2.3138 6 0 1 2 39.04 4.67 2.3072 -6 2 2 4 39.06 1.34 2.3060 -7 1 1 4 39.49 4.32 2.2819 2 2 3 4 39.61 1.42 2.2752 0 2 4 4 39.88 2.96 2.2606 4 0 3 2 40.09 1.73 2.2489 -1 3 2 4 40.25 5.27 2.2407 -6 2 1 4 40.53 2.58 2.2256 -8 0 2 2 40.86 9.54 2.2087 5 1 2 4 41.08 9.95 2.1973 -7 1 5 4 41.19 2.31 2.1916 -6 0 6 2 41.21 5.28 2.1908 -6 2 4 4 41.21 3.47 2.1906 -3 3 2 4 41.64 3.16 2.1692 3 3 0 4 41.73 2.89 2.1644 -4 2 5 4 41.97 2.50 2.1527 -5 1 6 4 42.03 4.40 2.1499 -3 1 6 4 42.36 8.71 2.1337 1 3 2 4 42.53 7.32 2.1257 -8 0 5 2 42.82 1.15 2.1121 -8 0 1 2 44.00 1.38 2.0578 3 3 1 4 44.09 9.33 2.0540 3 1 4 4 44.50 2.80 2.0360 6 0 2 2 45.30 2.26 2.0019 -1 1 6 4 45.42 4.74 1.9967 2 0 5 2 45.66 11.86 1.9868 2 2 4 4 45.97 1.20 1.9744 -8 0 6 2 46.06 5.00 1.9706 -5 3 1 4 46.09 1.27 1.9692 0 2 5 4 46.18 23.64 1.9657 0 0 6 2 46.31 6.80 1.9603 -5 3 3 4 46.74 3.65 1.9433 7 1 1 4 46.89 2.06 1.9376 -9 1 3 4 46.98 2.39 1.9340 -9 1 4 4 47.08 4.80 1.9304 5 1 3 4 47.11 12.65 1.9289 -6 0 7 2 47.29 9.02 1.9223 -4 2 6 4 47.43 31.90 1.9169 -8 2 3 4 47.51 12.36 1.9138 -1 3 4 4 47.58 10.85 1.9110 4 2 3 4 48.44 5.23 1.8793 -5 3 4 4 48.83 15.09 1.8651 -2 2 6 4 49.22 2.64 1.8512 -2 0 7 2 49.90 6.77 1.8274 -8 2 5 4 50.16 4.15 1.8187 -8 2 1 4 50.21 1.57 1.8170 -7 1 7 4 50.62 1.78 1.8033 -9 1 1 4 50.84 2.13 1.7960 -3 3 5 4 50.84 4.45 1.7958 6 0 3 2 51.00 1.95 1.7907 8 0 1 2 51.04 6.10 1.7893 5 3 1 4 51.07 25.22 1.7885 0 4 0 2 51.12 5.85 1.7869 -10 0 5 2 51.55 1.29 1.7729 3 1 5 4 52.15 2.67 1.7537 -7 3 3 4 52.29 1.08 1.7496 -10 0 2 2 52.36 1.96 1.7472 -7 3 2 4 52.49 5.89 1.7434 2 2 5 4 52.97 1.19 1.7286 -8 2 6 4 53.17 2.85 1.7227 0 2 6 4 53.34 8.56 1.7176 8 2 0 4 53.54 5.82 1.7115 0 4 2 4 53.74 6.05 1.7057 -6 0 8 2 54.01 3.04 1.6978 -6 2 7 4 54.26 5.65 1.6906 -4 0 8 2 54.82 3.76 1.6746 -9 1 7 4 55.21 4.43 1.6637 5 3 2 4 55.33 3.66 1.6604 -4 4 2 4 55.39 10.52 1.6588 -7 3 5 4 56.15 3.05 1.6381 -3 3 6 4 56.48 1.80 1.6292 -4 4 3 4 56.53 2.12 1.6280 8 0 2 2 56.57 3.20 1.6269 4 4 0 4 56.72 5.50 1.6231 2 4 2 4 56.87 7.66 1.6191 -10 2 4 4 57.10 7.77 1.6131 -8 2 7 4 57.23 3.60 1.6096 -10 2 3 4 57.28 1.26 1.6085 -11 1 4 4 57.32 1.07 1.6074 1 3 5 4 57.63 2.75 1.5994 -11 1 5 4 57.83 4.71 1.5945 3 3 4 4 58.37 3.98 1.5809 -2 4 4 4 58.75 1.67 1.5717 -10 2 2 4 58.77 1.79 1.5711 -4 4 4 4 60.01 4.62 1.5415 -11 1 2 4 60.04 4.30 1.5410 7 3 1 4 60.13 2.00 1.5388 -6 4 2 4 60.24 1.34 1.5364 -9 3 4 4 60.31 2.72 1.5345 5 3 3 4 60.37 8.70 1.5333 -6 4 3 4 60.46 2.60 1.5312 2 4 3 4 60.55 5.72 1.5292 0 4 4 4 60.76 2.06 1.5243 0 2 7 4 60.94 14.30 1.5202 4 2 5 4 60.97 1.72 1.5196 -6 0 9 2 61.02 12.68 1.5186 -6 4 1 4 61.36 4.40 1.5109 -10 2 1 4 61.37 2.33 1.5107 5 1 5 4 61.42 4.51 1.5096 -12 0 4 2 61.50 1.93 1.5078 -1 1 8 4 61.92 1.18 1.4986 2 0 7 2 62.30 1.24 1.4904 -4 0 9 2 62.36 4.38 1.4890 -12 0 6 2 62.61 1.57 1.4837 -12 0 3 2 62.61 7.13 1.4837 -10 2 7 4 62.71 2.59 1.4816 4 0 6 2 62.76 1.61 1.4805 -7 1 9 4 62.99 1.10 1.4757 -7 3 7 4 63.57 10.75 1.4636 -2 2 8 4 63.92 4.20 1.4564 6 2 4 4 64.16 3.51 1.4515 -6 4 5 4 64.87 2.62 1.4373 -12 0 2 2 65.00 4.39 1.4349 10 2 0 4 65.15 1.44 1.4319 7 1 4 4 65.38 2.35 1.4273 6 0 5 2 65.81 1.83 1.4192 -10 0 9 2 66.02 4.54 1.4150 6 4 1 4 66.51 1.03 1.4059 9 3 0 4 67.02 2.10 1.3963 -9 3 7 4 67.24 1.16 1.3923 -12 2 5 4 67.60 1.72 1.3858 -12 0 8 2 67.61 1.27 1.3857 -6 4 6 4 67.80 2.03 1.3822 2 2 7 4 68.04 13.86 1.3780 -8 2 9 4 68.10 1.80 1.3768 1 1 8 4 68.16 1.17 1.3758 -4 2 9 4 68.45 3.55 1.3707 1 5 2 4 68.46 1.13 1.3705 -12 2 3 4 68.56 1.95 1.3688 4 2 6 4 68.57 1.51 1.3686 -8 4 5 4 68.67 2.43 1.3669 8 2 3 4 68.89 3.03 1.3630 -13 1 4 4 69.22 1.21 1.3573 -11 3 4 4 69.54 1.77 1.3518 -11 3 5 4 70.02 1.08 1.3437 6 4 2 4 70.41 1.21 1.3372 -13 1 3 4 70.72 1.10 1.3322 2 4 5 4 70.82 1.18 1.3306 -4 0 10 2 71.29 8.28 1.3229 0 4 6 4 71.39 2.06 1.3212 -5 5 3 4 71.70 2.04 1.3163 -11 3 2 4 71.70 1.96 1.3163 -12 0 9 2 71.92 1.64 1.3129 11 1 1 4 72.00 7.21 1.3115 -6 4 7 4 72.31 6.45 1.3067 -1 5 4 4 72.40 4.44 1.3054 12 0 0 2 72.94 3.14 1.2970 5 3 5 4 73.03 2.03 1.2956 -5 5 4 4 73.06 1.22 1.2951 -1 3 8 4 73.21 1.49 1.2928 -13 1 8 4 73.65 1.02 1.2862 -2 4 7 4 74.09 1.10 1.2797 -3 1 10 4 74.22 1.13 1.2777 -7 3 9 4 74.39 2.86 1.2753 -6 2 10 4 74.94 2.55 1.2672 6 4 3 4 75.04 7.87 1.2658 10 2 2 4 75.10 1.15 1.2650 5 5 1 4 75.16 2.23 1.2641 -10 4 5 4 76.79 3.11 1.2412 4 2 7 4 77.30 2.94 1.2344 -6 4 8 4 77.73 2.59 1.2286 -4 4 8 4 78.62 1.31 1.2169 -14 -2 6 4 78.67 1.01 1.2162 -7 5 5 4 79.48 2.44 1.2059 -1 1 10 4 79.63 1.09 1.2039 8 4 2 4 80.57 1.27 1.1923 0 6 0 2 80.74 1.24 1.1902 3 5 4 4 81.69 1.36 1.1788 2 6 0 4 81.92 1.57 1.1760 -14 -2 8 4 82.16 3.87 1.1732 -2 6 2 4 83.47 1.14 1.1581 -6 4 9 4 83.58 1.40 1.1569 12 0 2 2 83.87 1.61 1.1536 -12 -4 4 4 84.04 1.34 1.1517 -4 6 1 4 84.70 1.26 1.1443 -12 -4 6 4 85.01 2.17 1.1410 4 4 6 4 85.04 2.63 1.1406 4 6 0 4 86.56 1.12 1.1245 -2 6 4 4 86.96 1.18 1.1204 -12 -4 2 4 87.03 2.46 1.1196 4 6 1 4 87.24 1.01 1.1175 5 1 8 4 87.42 2.56 1.1156 6 4 5 4 87.81 1.79 1.1117 -10 4 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.