Cr F6 Na Sr Hemon A, Courbion G European Journal of Solid State and Inorganic Chemistry 29 (1992) 519-531 Synthesis and crystal structures of beta-NaSrCrF6 and NaSrFeF6. Structural correlations with A2MF6 compounds _cod_database_code 1000305 _database_code_amcsd 0012556 CELL PARAMETERS: 5.5676 9.2937 9.5858 90.000 93.201 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 495.230 Density (g/cm3): 3.709 MAX. ABS. INTENSITY / VOLUME**2: 16.41730827 RIR: 1.441 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.28 8.68 6.6675 0 1 1 4 15.94 2.73 5.5589 1 0 0 2 18.54 3.18 4.7854 0 0 2 2 18.60 20.38 4.7706 1 1 0 4 20.40 36.12 4.3537 -1 1 1 4 21.20 21.04 4.1902 1 1 1 4 21.25 39.95 4.1802 0 2 1 4 25.73 100.00 3.4625 -1 1 2 4 26.36 44.13 3.3808 -1 2 1 4 26.74 49.76 3.3337 0 2 2 4 27.00 27.56 3.3025 1 2 1 4 27.02 74.73 3.3004 1 1 2 4 29.60 15.48 3.0174 0 1 3 4 30.33 14.67 2.9473 0 3 1 4 32.21 23.92 2.7795 2 0 0 2 33.02 14.47 2.7127 -1 1 3 4 33.10 11.64 2.7061 1 3 0 4 34.09 2.61 2.6301 0 2 3 4 34.56 9.17 2.5951 1 1 3 4 37.14 13.10 2.4209 -1 2 3 4 37.71 2.17 2.3853 2 2 0 4 37.74 1.38 2.3835 -1 3 2 4 37.77 2.45 2.3817 -2 1 2 4 38.35 5.37 2.3472 2 0 2 2 38.54 8.33 2.3362 1 2 3 4 38.67 19.75 2.3286 1 3 2 4 39.36 1.32 2.2889 2 2 1 4 39.60 13.06 2.2758 2 1 2 4 40.59 33.79 2.2225 0 3 3 4 41.40 7.27 2.1811 -1 1 4 4 41.48 3.24 2.1769 -2 2 2 4 42.50 5.61 2.1273 0 2 4 4 43.04 9.78 2.1016 -1 4 1 4 43.07 22.69 2.1004 -2 1 3 4 43.10 9.32 2.0989 1 1 4 4 43.18 17.20 2.0951 2 2 2 4 43.46 11.63 2.0823 1 4 1 4 44.41 31.61 2.0397 -2 3 1 4 44.86 2.02 2.0205 -1 2 4 4 45.23 28.13 2.0050 2 3 1 4 45.52 7.48 1.9926 2 1 3 4 46.02 1.52 1.9723 -1 4 2 4 46.43 8.57 1.9559 -2 2 3 4 46.81 2.66 1.9409 1 4 2 4 48.47 12.42 1.8781 0 4 3 4 48.56 3.69 1.8748 0 1 5 4 48.75 4.10 1.8679 2 2 3 4 48.82 16.21 1.8656 -2 0 4 2 49.99 10.26 1.8246 0 5 1 4 50.20 4.70 1.8172 3 1 0 4 50.21 4.63 1.8172 -1 3 4 4 50.52 1.25 1.8067 -1 1 5 4 50.61 3.08 1.8035 -3 1 1 4 50.80 10.69 1.7973 -1 4 3 4 51.25 2.89 1.7826 2 4 0 4 51.64 3.77 1.7699 0 2 5 4 51.65 1.35 1.7697 -2 3 3 4 51.68 7.73 1.7688 1 3 4 4 51.79 11.67 1.7653 2 0 4 2 51.83 1.11 1.7639 -2 4 1 4 51.87 13.39 1.7628 1 5 0 4 51.90 9.51 1.7618 1 4 3 4 52.56 1.05 1.7413 2 4 1 4 52.79 1.65 1.7343 2 1 4 4 52.84 2.48 1.7326 0 5 2 4 52.88 1.76 1.7313 -2 2 4 4 52.91 10.53 1.7306 -3 1 2 4 52.99 4.51 1.7282 1 5 1 4 53.22 1.81 1.7212 3 2 0 4 53.52 8.94 1.7122 -1 2 5 4 53.61 11.57 1.7095 -3 2 1 4 54.67 1.36 1.6789 3 2 1 4 55.03 6.59 1.6688 3 1 2 4 55.10 3.63 1.6669 0 4 4 4 55.21 1.65 1.6637 -1 5 2 4 55.28 4.56 1.6619 1 2 5 4 56.51 7.16 1.6284 0 3 5 4 56.93 2.79 1.6176 -3 1 3 4 57.68 1.12 1.5982 -2 3 4 4 57.80 1.50 1.5951 0 0 6 2 58.00 4.11 1.5902 3 3 0 4 58.39 1.02 1.5805 -2 4 3 4 59.38 1.45 1.5565 -1 0 6 2 59.71 1.76 1.5487 -3 2 3 4 59.95 2.19 1.5431 3 1 3 4 59.95 1.18 1.5431 1 3 5 4 60.29 4.44 1.5351 -1 1 6 4 60.38 5.81 1.5330 2 4 3 4 60.39 2.87 1.5328 -2 5 1 4 60.55 2.98 1.5291 -2 2 5 4 61.04 1.92 1.5179 2 5 1 4 61.12 1.42 1.5163 2 1 5 4 61.35 1.57 1.5111 1 0 6 2 61.46 2.52 1.5087 0 2 6 4 62.25 4.33 1.4915 1 1 6 4 62.41 1.08 1.4879 3 3 2 4 62.46 1.19 1.4869 -3 1 4 4 62.64 1.74 1.4830 3 2 3 4 62.91 1.57 1.4774 0 4 5 4 63.08 8.88 1.4737 0 6 2 4 63.21 2.55 1.4709 1 6 1 4 63.79 4.98 1.4592 2 2 5 4 64.57 1.72 1.4433 -1 4 5 4 64.99 1.70 1.4351 -2 3 5 4 65.10 1.33 1.4329 -3 2 4 4 65.17 1.26 1.4314 -1 5 4 4 65.60 4.24 1.4232 3 4 1 4 66.14 2.38 1.4128 1 4 5 4 66.43 2.30 1.4074 1 5 4 4 66.52 1.05 1.4056 2 4 4 4 67.32 1.97 1.3908 -1 3 6 4 67.38 6.71 1.3897 4 0 0 2 68.26 2.19 1.3740 2 5 3 4 69.27 4.63 1.3563 -2 2 6 4 69.49 1.53 1.3527 0 1 7 4 69.64 1.47 1.3500 4 1 1 4 70.17 4.66 1.3413 -3 4 3 4 70.19 1.25 1.3408 -4 1 2 4 70.64 1.66 1.3335 0 5 5 4 71.83 1.97 1.3142 -3 2 5 4 71.95 2.57 1.3123 3 5 0 4 72.01 7.84 1.3114 -2 6 2 4 72.15 2.09 1.3092 4 2 1 4 72.21 1.06 1.3083 -1 5 5 4 72.29 1.13 1.3071 -3 5 1 4 72.69 2.55 1.3008 -4 2 2 4 72.87 1.18 1.2980 1 1 7 4 72.88 3.20 1.2979 3 4 3 4 72.90 1.79 1.2976 2 2 6 4 73.18 1.05 1.2933 3 5 1 4 73.21 4.30 1.2928 2 6 2 4 73.31 2.69 1.2914 1 7 0 4 73.44 1.44 1.2894 -2 3 6 4 73.85 1.12 1.2833 3 1 5 4 73.93 1.44 1.2820 -1 7 1 4 75.07 1.32 1.2654 -4 3 1 4 75.07 1.59 1.2654 4 2 2 4 76.29 1.84 1.2481 3 2 5 4 76.68 1.52 1.2427 1 7 2 4 77.42 2.63 1.2327 -3 1 6 4 77.48 1.01 1.2320 -4 0 4 2 78.31 2.22 1.2209 -2 5 5 4 79.12 1.68 1.2105 0 5 6 4 79.99 3.22 1.1995 -4 3 3 4 80.24 4.18 1.1964 0 0 8 2 80.62 1.37 1.1917 -2 6 4 4 80.69 1.00 1.1908 -4 2 4 4 81.20 1.45 1.1846 -3 6 1 4 81.57 1.44 1.1802 -3 4 5 4 82.41 1.98 1.1703 -3 5 4 4 82.65 2.12 1.1675 3 1 6 4 82.93 1.17 1.1643 2 6 4 4 82.94 3.09 1.1642 -1 4 7 4 83.03 2.98 1.1631 -2 3 7 4 83.15 1.12 1.1617 0 8 0 2 83.46 2.31 1.1582 4 3 3 4 84.86 3.83 1.1426 -1 7 4 4 84.95 1.42 1.1417 1 4 7 4 86.01 2.32 1.1303 1 7 4 4 86.25 1.53 1.1277 1 8 1 4 87.05 2.62 1.1195 2 3 7 4 87.85 1.00 1.1113 -4 5 1 4 87.85 2.96 1.1112 0 6 6 4 88.99 1.42 1.1000 4 4 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.