H24 N2 O26 P6 Zn2 Averbuch-Pouchot M, Durif A European Journal of Solid State and Inorganic Chemistry 30 (1993) 573-581 Elaboration and crystal structure of zinc-ammonium cyclohexaphosphate octahydrate: Zn2(NH4)2P6O18 . 8H2O _cod_database_code 1007214 _database_code_amcsd 0015899 CELL PARAMETERS: 8.7170 10.2970 7.4090 104.820 111.030 70.960 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 579.472 Density (g/cm3): 2.249 MAX. ABS. INTENSITY / VOLUME**2: 6.064480677 RIR: 0.878 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.20 47.93 9.6126 0 1 0 2 12.56 63.84 7.0462 1 1 0 2 12.96 35.07 6.8295 0 0 1 2 14.16 100.00 6.2551 -1 -1 1 2 14.68 60.85 6.0332 0 -1 1 2 16.32 70.71 5.4312 -1 1 0 2 17.07 35.98 5.1951 0 1 1 2 18.98 8.22 4.6764 1 2 0 2 19.11 8.59 4.6446 -1 -2 1 2 19.63 37.42 4.5235 1 0 1 2 19.63 3.15 4.5223 -1 1 1 2 20.86 13.21 4.2582 0 -2 1 2 21.03 18.67 4.2242 -2 -1 1 2 21.33 2.02 4.1665 1 1 1 2 22.10 2.25 4.0231 1 -1 1 2 22.11 23.59 4.0207 2 1 0 2 22.63 7.00 3.9285 2 0 0 2 23.53 2.42 3.7807 -2 -2 1 2 24.26 25.41 3.6685 0 2 1 2 25.11 6.11 3.5468 -1 0 2 2 26.10 2.01 3.4148 0 0 2 2 26.29 4.57 3.3903 0 -1 2 2 26.44 7.39 3.3714 1 2 1 2 26.56 3.95 3.3558 -1 -3 1 2 27.19 47.09 3.2799 1 3 0 2 27.20 17.48 3.2785 -1 2 1 2 27.21 20.47 3.2773 -2 -1 2 2 27.22 12.94 3.2766 -2 1 1 2 27.69 30.17 3.2218 1 -2 1 2 28.54 26.89 3.1275 -2 -2 2 2 28.86 13.47 3.0939 0 -3 1 2 29.02 1.14 3.0769 -2 0 2 2 29.10 3.23 3.0692 0 1 2 2 29.18 55.25 3.0603 -1 1 2 2 29.45 29.75 3.0331 2 0 1 2 29.70 20.69 3.0076 2 1 1 2 31.10 2.07 2.8758 2 3 0 2 31.56 1.77 2.8350 1 0 2 2 31.76 25.54 2.8176 -3 -2 1 2 31.96 16.84 2.8004 -1 -3 2 2 32.08 5.56 2.7897 2 -1 1 2 32.60 1.46 2.7467 1 -1 2 2 32.66 1.66 2.7420 -2 -3 2 2 32.72 2.07 2.7366 -3 0 1 2 32.79 5.46 2.7313 2 2 1 2 32.81 4.41 2.7294 -1 3 0 2 32.98 4.95 2.7156 -2 2 0 2 33.28 5.28 2.6924 1 1 2 2 33.50 3.31 2.6747 -2 1 2 2 34.11 2.17 2.6283 -3 -1 2 2 34.24 15.09 2.6190 3 0 0 2 34.38 1.45 2.6082 -3 -2 2 2 35.05 2.05 2.5604 1 -3 1 2 35.09 12.84 2.5575 -1 -4 1 2 36.24 1.56 2.4790 -2 -4 1 2 37.41 1.38 2.4039 -2 -1 3 2 37.42 5.57 2.4032 0 4 0 2 37.68 4.08 2.3875 0 -4 1 2 37.68 8.60 2.3873 -1 0 3 2 37.88 4.21 2.3752 -3 1 0 2 37.89 1.63 2.3743 -2 -2 3 2 38.32 3.98 2.3487 3 3 0 2 38.50 1.44 2.3382 2 4 0 2 38.78 7.94 2.3223 -2 -4 2 2 38.93 1.68 2.3137 -1 -4 2 2 39.21 4.09 2.2977 0 -1 3 2 39.59 1.21 2.2765 0 0 3 2 39.86 8.29 2.2617 2 0 2 2 39.87 8.86 2.2611 -2 2 2 2 40.43 4.28 2.2309 3 0 1 2 40.56 3.58 2.2243 2 1 2 2 40.88 1.72 2.2076 -3 1 2 2 41.12 1.13 2.1951 -1 1 3 2 41.57 6.80 2.1724 0 3 2 2 41.63 4.28 2.1692 3 2 1 2 41.76 3.05 2.1631 1 -3 2 2 41.81 8.88 2.1607 -4 -1 1 2 42.08 1.10 2.1473 -1 4 0 2 42.21 2.70 2.1410 0 1 3 2 42.46 11.01 2.1291 0 -4 2 2 43.33 1.40 2.0883 -2 1 3 2 44.00 1.41 2.0578 -4 -3 1 2 44.15 5.65 2.0513 -3 0 3 2 44.49 6.22 2.0362 -4 -3 2 2 44.98 2.02 2.0152 -1 4 1 2 45.08 2.26 2.0111 0 -3 3 2 45.10 4.09 2.0103 4 2 0 2 45.57 1.18 1.9906 1 5 0 2 45.83 3.48 1.9800 -4 0 2 2 46.22 6.53 1.9642 4 0 0 2 46.41 7.14 1.9565 -1 2 3 2 46.63 3.47 1.9477 -1 -4 3 2 46.91 1.35 1.9369 2 5 0 2 47.03 1.01 1.9321 -3 2 2 2 47.05 11.60 1.9315 0 -5 1 2 47.34 1.09 1.9204 1 -2 3 2 47.78 1.75 1.9037 3 -2 1 2 48.04 1.50 1.8938 -4 1 1 2 48.14 1.09 1.8904 -4 -4 2 2 48.48 5.25 1.8777 -3 -5 2 2 48.72 4.08 1.8690 -4 -1 3 2 49.33 1.71 1.8474 -2 4 0 2 49.54 1.57 1.8398 -2 -2 4 2 49.71 4.86 1.8342 0 4 2 2 49.84 3.48 1.8297 3 1 2 2 49.86 2.59 1.8289 3 0 2 2 49.87 1.23 1.8285 -1 -1 4 2 50.05 3.69 1.8223 1 2 3 2 50.22 1.45 1.8167 -4 1 2 2 50.90 1.98 1.7941 3 4 1 2 51.36 4.16 1.7791 0 5 1 2 51.73 1.55 1.7670 -2 -5 3 2 51.78 5.30 1.7655 3 -1 2 2 51.81 1.39 1.7646 -1 5 0 2 51.91 1.67 1.7616 4 4 0 2 52.15 1.68 1.7540 -3 -1 4 2 52.87 3.70 1.7317 0 3 3 2 52.88 1.86 1.7314 -1 -3 4 2 52.89 1.68 1.7310 -5 -2 2 2 52.95 1.10 1.7293 2 5 1 2 53.01 3.20 1.7273 -5 -2 1 2 53.41 1.95 1.7156 -1 -5 3 2 53.82 2.10 1.7033 -4 -5 1 2 53.87 1.05 1.7019 -5 -1 2 2 53.92 1.06 1.7003 3 -3 1 2 53.93 3.62 1.7001 -1 -6 1 2 54.10 4.20 1.6951 0 -2 4 2 54.35 1.25 1.6880 -3 2 3 2 54.43 2.08 1.6857 2 4 2 2 54.45 1.47 1.6850 -3 3 2 2 54.61 2.34 1.6807 -3 0 4 2 54.67 2.86 1.6789 4 3 1 2 54.90 1.77 1.6725 -4 2 0 2 55.25 1.13 1.6627 -2 1 4 2 55.37 2.36 1.6594 3 3 2 2 56.11 1.64 1.6393 -2 3 3 2 56.13 2.20 1.6386 -4 -2 4 2 56.14 1.49 1.6383 -4 2 2 2 56.62 2.08 1.6255 -4 -5 3 2 56.70 1.93 1.6234 5 2 0 2 56.86 2.45 1.6192 5 1 0 2 56.87 2.01 1.6191 1 -5 2 2 56.94 1.11 1.6173 0 -6 1 2 57.18 6.60 1.6109 2 -4 2 2 57.24 1.44 1.6094 1 -4 3 2 57.69 1.05 1.5979 0 -5 3 2 58.30 1.66 1.5828 5 3 0 2 58.96 2.30 1.5665 -5 -4 3 2 59.07 1.82 1.5638 -4 -4 4 2 59.50 1.64 1.5536 4 -2 1 2 59.73 2.81 1.5482 -3 -6 3 2 60.11 1.79 1.5392 -4 -6 2 2 60.14 2.81 1.5385 -4 0 4 2 60.31 2.83 1.5346 0 2 4 2 60.51 1.06 1.5302 -2 2 4 2 60.52 3.04 1.5299 1 1 4 2 60.69 3.16 1.5260 -5 0 3 2 60.92 2.26 1.5208 -1 5 2 2 61.50 1.45 1.5078 3 0 3 2 62.30 1.33 1.4904 -5 1 0 2 63.05 1.47 1.4743 -5 -3 4 2 63.41 2.42 1.4669 1 -3 4 2 63.56 1.30 1.4639 5 2 1 2 63.96 1.17 1.4555 1 2 4 2 64.75 1.04 1.4397 4 5 1 2 64.79 1.49 1.4390 -3 -7 2 2 65.02 5.26 1.4344 -1 6 1 2 65.40 1.17 1.4269 4 -3 1 2 65.62 1.17 1.4226 -6 -1 2 2 65.72 1.07 1.4207 3 6 1 2 65.77 1.65 1.4199 -1 0 5 2 66.67 1.55 1.4029 -3 -4 5 2 67.05 1.19 1.3958 -3 0 5 2 67.07 1.03 1.3955 -4 -3 5 2 67.43 1.27 1.3888 3 3 3 2 67.51 1.87 1.3874 -3 5 0 2 67.82 1.19 1.3818 -2 -7 3 2 67.89 1.92 1.3805 -5 -6 1 2 68.49 1.25 1.3699 0 6 2 2 68.59 1.42 1.3683 -6 0 2 2 68.74 2.01 1.3656 4 4 2 2 69.19 1.15 1.3578 -4 4 0 2 69.44 1.11 1.3535 -1 -4 5 2 69.80 1.44 1.3474 1 5 3 2 71.72 1.32 1.3160 -6 -5 1 2 72.17 1.40 1.3089 -4 -5 5 2 72.23 1.09 1.3079 4 1 3 2 72.27 1.45 1.3073 5 -2 1 2 72.46 1.49 1.3044 -5 1 4 2 72.81 1.09 1.2990 2 -5 3 2 73.24 1.18 1.2923 2 5 3 2 73.33 2.40 1.2911 -5 -4 5 2 74.11 1.45 1.2794 4 -1 3 2 74.59 1.34 1.2724 0 -6 4 2 74.63 1.14 1.2717 -5 -7 3 2 76.61 1.50 1.2438 -7 -3 2 2 76.67 1.06 1.2429 2 8 0 2 78.76 1.24 1.2150 1 6 3 2 79.34 1.29 1.2077 3 -6 1 2 80.69 1.51 1.1908 0 3 5 2 81.00 1.08 1.1870 4 -5 1 2 86.67 1.14 1.1233 -1 4 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.