PbRb(PO3)3 Prisset J, Averbuch-Pouchot M, Durif A European Journal of Solid State and Inorganic Chemistry 31 (1994) 37-46 The Pb(PO3)2-Rb(PO3) phase-equilibrium crystal structure of PbRb(PO3)3 _cod_database_code 1007228 _database_code_amcsd 0015910 CELL PARAMETERS: 14.0500 17.0900 7.2280 90.000 103.850 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1685.088 Density (g/cm3): 4.174 MAX. ABS. INTENSITY / VOLUME**2: 23.49431658 RIR: 1.833 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.29 3.03 10.6615 1 1 0 4 10.35 47.67 8.5450 0 2 0 2 12.73 1.02 6.9543 -1 0 1 2 13.64 89.99 6.4918 0 1 1 4 13.75 1.50 6.4414 -1 1 1 4 13.98 34.72 6.3349 2 1 0 4 15.52 1.03 5.7092 1 0 1 2 16.34 20.36 5.4233 0 2 1 4 16.37 5.31 5.4151 1 1 1 4 16.64 10.79 5.3284 -2 1 1 4 18.93 18.60 4.6884 -2 2 1 4 20.31 48.22 4.3723 2 3 0 4 20.79 5.16 4.2725 0 4 0 2 20.88 1.67 4.2553 2 1 1 4 21.23 2.66 4.1853 -3 1 1 4 22.14 1.93 4.0142 3 2 0 4 22.24 2.26 3.9964 -2 3 1 4 22.76 99.48 3.9074 2 2 1 4 24.39 23.24 3.6494 0 4 1 4 24.45 3.10 3.6404 -1 4 1 4 24.59 10.87 3.6208 2 4 0 4 25.06 1.95 3.5538 3 3 0 4 25.19 6.72 3.5352 -1 1 2 4 25.38 5.78 3.5089 0 0 2 2 25.60 4.69 3.4791 2 3 1 4 25.62 7.98 3.4772 -2 0 2 2 25.77 8.79 3.4571 3 0 1 2 25.90 1.22 3.4405 -3 3 1 4 25.92 27.86 3.4372 0 1 2 4 26.13 46.72 3.4104 4 0 0 2 26.15 37.36 3.4073 -2 1 2 4 26.22 100.00 3.3985 -2 4 1 4 26.65 7.11 3.3444 4 1 0 4 26.70 54.00 3.3388 -4 1 1 4 27.48 34.55 3.2459 0 2 2 4 27.70 37.14 3.2207 -2 2 2 4 28.17 54.72 3.1674 4 2 0 4 28.22 19.89 3.1627 -4 2 1 4 28.67 3.67 3.1137 3 4 0 4 29.06 53.92 3.0729 0 5 1 4 29.15 22.84 3.0631 2 4 1 4 29.23 51.86 3.0558 2 5 0 4 29.27 2.99 3.0513 -1 3 2 4 29.67 1.81 3.0112 1 2 2 4 29.91 39.23 2.9876 0 3 2 4 30.11 14.39 2.9680 -2 3 2 4 30.24 1.24 2.9555 3 3 1 4 30.48 1.34 2.9326 1 5 1 4 30.55 3.22 2.9261 4 3 0 4 30.59 6.56 2.9223 -4 3 1 4 31.34 1.19 2.8546 2 0 2 2 31.41 2.20 2.8483 0 6 0 2 31.92 9.00 2.8040 -4 0 2 2 31.94 1.17 2.8016 1 3 2 4 32.10 1.79 2.7882 1 6 0 4 32.24 8.70 2.7766 4 1 1 4 32.67 2.42 2.7414 -5 1 1 4 32.78 2.40 2.7322 3 5 0 4 33.09 10.10 2.7075 2 2 2 4 33.25 1.02 2.6942 5 1 0 4 33.34 1.19 2.6875 3 4 1 4 33.53 21.16 2.6728 4 2 1 4 33.62 1.15 2.6654 4 4 0 4 33.64 4.86 2.6642 -4 2 2 4 34.11 10.26 2.6284 2 6 0 4 34.91 5.46 2.5702 1 4 2 4 35.16 19.27 2.5521 2 3 2 4 35.34 3.58 2.5395 -2 6 1 4 35.69 14.63 2.5157 -4 3 2 4 36.95 1.68 2.4327 -5 1 2 4 37.28 8.76 2.4121 -4 5 1 4 37.42 1.48 2.4035 -1 0 3 2 37.63 5.58 2.3900 2 6 1 4 37.92 4.43 2.3725 -2 1 3 4 38.86 6.39 2.3177 0 1 3 4 38.97 1.23 2.3114 -6 1 1 4 39.05 3.62 2.3068 -2 2 3 4 39.06 27.03 2.3059 0 7 1 4 39.18 2.68 2.2995 5 4 0 4 39.22 2.51 2.2971 -3 1 3 4 39.31 2.13 2.2917 3 3 2 4 39.63 1.85 2.2742 5 2 1 4 39.64 2.30 2.2736 6 0 0 2 39.95 1.97 2.2567 -5 3 2 4 39.96 10.50 2.2563 0 2 3 4 40.01 5.54 2.2537 6 1 0 4 40.07 11.92 2.2505 -6 2 1 4 40.29 2.27 2.2385 -2 7 1 4 40.75 2.13 2.2144 -1 3 3 4 40.80 10.08 2.2115 0 6 2 4 40.86 7.38 2.2084 -2 3 3 4 40.96 8.48 2.2034 -2 6 2 4 41.02 1.69 2.2004 1 1 3 4 41.08 1.32 2.1971 6 2 0 4 41.09 5.71 2.1968 4 0 2 2 41.20 8.47 2.1910 2 5 2 4 41.30 19.23 2.1861 4 6 0 4 41.42 1.10 2.1798 5 3 1 4 41.57 9.94 2.1725 4 5 1 4 41.60 1.86 2.1712 -4 1 3 4 41.66 8.61 2.1678 -4 5 2 4 41.74 2.12 2.1639 0 3 3 4 41.82 1.15 2.1598 3 4 2 4 41.85 9.19 2.1584 -6 0 2 2 41.91 2.35 2.1555 -5 5 1 4 42.08 1.14 2.1471 -3 3 3 4 42.31 6.95 2.1363 0 8 0 2 42.35 1.91 2.1341 2 7 1 4 42.49 4.42 2.1277 4 2 2 4 42.64 16.45 2.1205 -4 2 3 4 42.83 19.09 2.1116 6 3 0 4 43.23 4.85 2.0926 -6 2 2 4 43.30 1.27 2.0896 -2 4 3 4 43.78 5.37 2.0675 1 3 3 4 44.14 17.51 2.0519 0 4 3 4 44.15 10.91 2.0512 2 1 3 4 44.19 6.93 2.0497 4 3 2 4 44.24 12.88 2.0475 -6 4 1 4 44.32 5.63 2.0437 0 8 1 4 44.33 4.36 2.0433 -4 3 3 4 44.91 7.98 2.0183 -6 3 2 4 44.96 15.71 2.0163 2 6 2 4 45.07 1.20 2.0113 6 1 1 4 45.15 1.09 2.0083 2 2 3 4 45.25 1.50 2.0041 0 7 2 4 45.33 1.60 2.0008 1 8 1 4 45.39 11.68 1.9982 -4 6 2 4 45.43 4.44 1.9963 -2 8 1 4 45.54 1.39 1.9919 -7 1 1 4 45.73 11.93 1.9840 -4 7 1 4 46.05 7.50 1.9708 6 2 1 4 46.28 8.26 1.9618 -2 5 3 4 46.62 7.16 1.9481 -4 4 3 4 46.93 1.58 1.9362 7 1 0 4 47.88 1.22 1.9000 7 2 0 4 48.06 2.66 1.8930 6 5 0 4 48.08 4.28 1.8923 5 2 2 4 48.94 1.23 1.8611 1 5 3 4 48.97 2.03 1.8601 2 4 3 4 49.02 6.91 1.8582 -6 1 3 4 49.04 1.72 1.8576 3 2 3 4 49.10 1.91 1.8554 2 7 2 4 49.31 5.32 1.8480 4 5 2 4 49.42 11.37 1.8441 4 7 1 4 49.43 1.11 1.8439 7 3 0 4 49.44 1.47 1.8433 -4 5 3 4 49.63 2.80 1.8369 -1 6 3 4 49.74 2.98 1.8330 0 9 1 4 49.82 13.91 1.8302 6 4 1 4 49.85 11.88 1.8293 2 9 0 4 49.94 5.15 1.8261 -6 2 3 4 49.98 6.98 1.8250 -6 5 2 4 49.98 3.00 1.8247 0 8 2 4 50.12 6.56 1.8202 -2 8 2 4 50.21 1.96 1.8169 5 6 1 4 50.41 2.47 1.8104 4 8 0 4 50.52 10.28 1.8067 -2 0 4 2 50.57 2.82 1.8048 -6 6 1 4 50.76 3.81 1.7986 -2 9 1 4 50.78 1.12 1.7979 -3 6 3 4 51.16 1.70 1.7855 -1 1 4 4 51.42 1.66 1.7771 -3 1 4 4 51.70 1.08 1.7682 2 5 3 4 51.89 1.00 1.7621 7 1 1 4 52.35 1.77 1.7478 3 7 2 4 52.37 4.66 1.7470 -8 1 1 4 52.74 1.51 1.7356 -4 6 3 4 52.77 1.05 1.7347 7 2 1 4 52.97 4.08 1.7286 6 0 2 2 53.25 1.53 1.7203 -8 2 1 4 53.25 3.02 1.7203 -6 6 2 4 53.58 2.30 1.7104 2 8 2 4 53.59 11.17 1.7100 -2 7 3 4 53.63 1.51 1.7089 4 2 3 4 53.76 4.23 1.7052 8 0 0 2 53.86 3.12 1.7022 -8 0 2 2 53.96 3.05 1.6993 -4 8 2 4 54.15 2.16 1.6938 -8 1 2 4 54.40 2.71 1.6866 -6 7 1 4 54.74 4.70 1.6767 0 3 4 4 54.91 6.45 1.6722 8 2 0 4 54.98 1.20 1.6700 0 9 2 4 55.11 3.29 1.6666 -2 9 2 4 55.20 1.02 1.6640 -2 4 4 4 55.24 5.08 1.6629 -4 3 4 4 55.40 5.38 1.6584 -4 9 1 4 55.54 1.69 1.6545 -5 6 3 4 55.56 3.86 1.6541 6 3 2 4 55.77 1.61 1.6484 -3 4 4 4 56.08 3.10 1.6401 -6 5 3 4 56.27 4.44 1.6348 -2 10 1 4 56.42 2.71 1.6310 -8 3 2 4 56.46 2.81 1.6298 -4 7 3 4 56.67 1.12 1.6244 -8 4 1 4 56.95 1.14 1.6171 -6 7 2 4 57.03 6.39 1.6148 4 4 3 4 57.27 3.12 1.6088 2 0 4 2 57.74 1.16 1.5967 -1 8 3 4 57.90 7.39 1.5928 2 10 1 4 58.23 2.44 1.5845 -6 0 4 2 58.31 1.55 1.5824 3 6 3 4 58.37 2.43 1.5810 2 9 2 4 58.37 2.28 1.5810 2 2 4 4 58.51 1.08 1.5775 0 8 3 4 58.52 2.38 1.5772 2 7 3 4 58.59 1.78 1.5755 -6 8 1 4 58.65 2.08 1.5740 4 9 1 4 58.72 1.47 1.5723 -4 9 2 4 58.76 1.37 1.5713 1 4 4 4 58.97 1.47 1.5662 8 1 1 4 59.14 3.89 1.5621 -8 5 1 4 59.16 1.07 1.5616 -8 1 3 4 59.20 5.10 1.5608 0 5 4 4 59.28 1.82 1.5588 6 7 1 4 59.29 1.26 1.5586 5 9 0 4 59.32 4.30 1.5579 -6 2 4 4 59.67 2.16 1.5496 -4 5 4 4 59.79 1.33 1.5468 7 1 2 4 59.97 2.26 1.5424 -8 2 3 4 60.18 2.67 1.5377 5 3 3 4 60.45 1.63 1.5315 4 8 2 4 60.63 1.33 1.5274 -4 10 1 4 60.79 1.39 1.5237 -8 5 2 4 61.03 2.59 1.5183 -6 8 2 4 61.18 5.65 1.5148 2 11 0 4 61.25 2.34 1.5133 3 1 4 4 61.66 2.80 1.5043 7 6 1 4 62.59 5.55 1.4842 -6 7 3 4 62.89 1.98 1.4777 6 6 2 4 63.05 1.57 1.4743 0 9 3 4 63.16 4.75 1.4722 -8 4 3 4 63.19 1.23 1.4715 -7 2 4 4 63.27 1.86 1.4698 6 8 1 4 63.51 1.11 1.4648 9 3 0 4 63.60 1.99 1.4631 8 6 0 4 63.69 1.54 1.4612 -8 6 2 4 63.71 1.19 1.4607 4 10 1 4 63.78 2.52 1.4592 6 1 3 4 63.87 4.91 1.4574 6 9 0 4 64.39 1.85 1.4469 5 5 3 4 64.56 1.16 1.4435 6 2 3 4 64.76 2.04 1.4396 -2 1 5 4 65.31 1.89 1.4288 8 5 1 4 65.47 3.37 1.4257 -8 7 1 4 65.55 2.79 1.4242 0 12 0 2 65.64 1.20 1.4224 4 1 4 4 65.73 4.07 1.4206 0 11 2 4 65.80 1.17 1.4192 4 7 3 4 65.84 3.12 1.4185 -2 11 2 4 66.78 2.13 1.4008 2 6 4 4 66.93 2.33 1.3981 2 9 3 4 67.44 1.43 1.3887 -10 0 2 2 67.46 1.39 1.3884 -1 3 5 4 67.46 1.09 1.3883 8 2 2 4 67.64 2.40 1.3850 0 2 5 4 67.65 1.46 1.3849 -10 2 1 4 67.66 3.42 1.3847 -6 6 4 4 67.67 1.26 1.3845 4 3 4 4 67.93 2.39 1.3800 0 10 3 4 67.95 1.57 1.3795 -2 8 4 4 68.00 4.90 1.3786 -6 10 1 4 68.57 1.64 1.3686 -2 4 5 4 68.87 1.44 1.3634 1 0 5 2 68.98 3.02 1.3614 -8 3 4 4 69.58 1.97 1.3512 -5 3 5 4 69.59 1.08 1.3510 4 8 3 4 69.62 4.50 1.3504 -4 4 5 4 69.70 2.01 1.3492 -10 3 2 4 69.82 1.08 1.3471 7 0 3 2 69.82 2.23 1.3471 -4 10 3 4 69.87 1.40 1.3462 6 5 3 4 70.02 1.66 1.3438 6 8 2 4 70.07 2.87 1.3430 -6 1 5 4 70.64 3.23 1.3334 -10 4 1 4 70.66 1.29 1.3331 5 1 4 4 70.69 2.08 1.3327 8 8 0 4 70.72 2.13 1.3321 -6 9 3 4 70.80 1.54 1.3307 -2 5 5 4 70.81 1.30 1.3307 -6 2 5 4 71.06 2.95 1.3266 10 3 0 4 71.33 3.12 1.3222 8 7 1 4 71.44 1.19 1.3205 -10 1 3 4 71.60 1.12 1.3179 -2 12 2 4 73.26 1.57 1.2921 0 13 1 4 73.49 2.02 1.2886 0 9 4 4 73.63 1.36 1.2865 -10 5 2 4 73.88 5.29 1.2827 6 11 0 4 73.90 1.28 1.2825 5 10 2 4 73.91 2.51 1.2823 -4 9 4 4 74.85 1.17 1.2686 10 2 1 4 74.85 1.31 1.2685 4 11 2 4 74.96 1.50 1.2670 10 5 0 4 75.34 1.30 1.2615 8 6 2 4 76.04 1.15 1.2516 6 0 4 2 76.28 1.28 1.2482 -10 6 2 4 76.64 1.31 1.2433 -2 7 5 4 77.25 1.57 1.2350 -10 5 3 4 77.64 1.06 1.2298 1 6 5 4 77.64 1.76 1.2297 9 4 2 4 77.71 1.62 1.2289 -10 0 4 2 77.73 1.66 1.2286 10 4 1 4 77.88 1.39 1.2265 2 5 5 4 77.90 1.50 1.2264 -4 13 1 4 78.33 1.12 1.2207 0 14 0 2 78.33 1.58 1.2207 4 10 3 4 78.65 1.19 1.2165 0 12 3 4 78.66 1.16 1.2163 -10 2 4 4 79.83 1.14 1.2015 -3 1 6 4 80.35 1.80 1.1950 4 12 2 4 80.45 1.06 1.1937 -4 12 3 4 80.73 1.60 1.1903 -4 13 2 4 80.76 1.05 1.1899 -8 4 5 4 80.86 1.38 1.1887 -6 12 2 4 81.21 1.02 1.1845 -4 8 5 4 81.47 1.15 1.1813 3 5 5 4 81.63 1.24 1.1795 -6 7 5 4 81.65 1.19 1.1792 -7 6 5 4 82.91 1.90 1.1644 -12 1 1 4 82.94 2.18 1.1642 -10 7 3 4 83.03 1.12 1.1631 0 11 4 4 83.44 2.79 1.1585 -4 11 4 4 83.56 1.15 1.1571 2 7 5 4 83.66 1.08 1.1559 4 4 5 4 83.70 1.06 1.1555 6 11 2 4 83.93 1.47 1.1529 0 14 2 4 84.25 2.98 1.1493 4 14 0 4 84.53 1.14 1.1462 -1 4 6 4 84.85 1.31 1.1427 -12 3 2 4 85.02 1.48 1.1409 4 9 4 4 85.12 1.42 1.1398 1 1 6 4 85.15 1.56 1.1395 7 8 3 4 85.40 1.36 1.1368 12 0 0 2 86.24 1.31 1.1279 -8 9 4 4 86.52 1.32 1.1249 -12 2 3 4 86.55 1.65 1.1246 0 15 1 4 86.91 1.10 1.1209 -10 9 2 4 87.07 1.18 1.1192 -10 1 5 4 87.14 1.64 1.1185 -2 12 4 4 88.06 1.15 1.1091 2 13 3 4 88.19 1.39 1.1079 10 9 0 4 89.32 1.87 1.0968 -12 4 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.