Cs2 O15 Si6 Zr Jolicart G, Leblanc M, Morel B, Dehaudt P, Dubois S European Journal of Solid State and Inorganic Chemistry 33 (1996) 647-657 Hydrothermal synthesis and structure determination of Cs2 Zr Si6 O15 _cod_database_code 1000423 _database_code_amcsd 0012605 CELL PARAMETERS: 26.6100 7.5060 11.6020 90.000 107.430 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 2210.918 Density (g/cm3): 3.449 MAX. ABS. INTENSITY / VOLUME**2: 23.64439819 RIR: 2.232 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.99 3.49 11.0693 0 0 1 2 8.89 2.78 9.9486 -2 0 1 2 12.08 32.50 7.3263 2 0 1 2 13.85 4.43 6.3943 -4 0 1 2 15.43 6.72 5.7426 -2 0 2 2 15.78 2.55 5.6155 3 1 0 4 16.01 1.64 5.5346 0 0 2 2 16.22 1.06 5.4653 -3 1 1 4 19.38 1.44 4.5795 -1 1 2 4 20.65 6.02 4.3018 -5 1 1 4 21.06 15.44 4.2179 1 1 2 4 22.30 1.74 3.9867 -6 0 2 2 23.00 2.79 3.8672 -2 0 3 2 23.17 5.65 3.8387 -5 1 2 4 23.71 27.01 3.7530 0 2 0 2 23.99 1.30 3.7089 -4 0 3 2 24.12 71.40 3.6898 0 0 3 2 24.30 7.50 3.6632 4 0 2 2 24.44 28.43 3.6429 5 1 1 4 24.67 2.82 3.6083 6 0 1 2 25.36 1.51 3.5115 -2 2 1 4 26.19 3.14 3.4029 -1 1 3 4 26.29 100.00 3.3901 -7 1 1 4 26.69 34.27 3.3402 2 2 1 4 26.89 6.62 3.3162 -6 0 3 2 27.11 4.79 3.2889 2 0 3 2 27.31 8.36 3.2656 7 1 0 4 27.56 11.53 3.2367 -4 2 1 4 27.72 6.43 3.2179 -7 1 2 4 27.91 2.72 3.1972 -8 0 2 2 28.10 1.14 3.1758 1 1 3 4 28.41 75.28 3.1416 -2 2 2 4 28.74 5.91 3.1062 0 2 2 4 30.19 3.02 2.9607 6 0 2 2 30.56 2.42 2.9254 7 1 1 4 30.76 1.66 2.9065 2 2 2 4 30.94 3.89 2.8900 -2 0 4 2 31.15 1.67 2.8713 -4 0 4 2 31.19 1.04 2.8679 -8 0 3 2 31.27 1.60 2.8604 -6 2 1 4 31.30 19.01 2.8577 -7 1 3 4 31.48 2.06 2.8415 4 0 3 2 31.55 1.87 2.8358 3 1 3 4 31.57 5.69 2.8340 8 0 1 2 31.87 12.74 2.8077 6 2 0 4 32.35 1.78 2.7673 0 0 4 2 32.58 3.51 2.7483 -9 1 1 4 33.24 4.39 2.6949 -9 1 2 4 33.27 3.69 2.6932 -2 2 3 4 33.77 1.42 2.6538 -10 0 1 2 33.95 11.92 2.6406 9 1 0 4 34.08 34.10 2.6311 0 2 3 4 34.08 5.37 2.6308 -5 1 4 4 35.20 3.43 2.5496 2 0 4 2 35.49 25.31 2.5297 7 1 2 4 35.84 4.67 2.5054 -9 1 3 4 36.08 1.83 2.4892 -8 2 1 4 36.11 1.66 2.4871 -8 0 4 2 36.32 1.19 2.4735 2 2 3 4 36.46 13.71 2.4643 -7 1 4 4 36.76 3.21 2.4447 -1 3 1 4 36.80 3.17 2.4421 6 0 3 2 36.93 1.72 2.4338 -8 2 2 4 39.15 1.32 2.3007 -2 0 5 2 39.35 5.87 2.2898 -2 2 4 4 39.86 1.49 2.2616 8 2 1 4 39.91 4.35 2.2592 -6 0 5 2 40.05 1.72 2.2516 -9 1 4 4 40.50 1.38 2.2273 0 2 4 4 40.76 1.21 2.2139 0 0 5 2 40.85 5.42 2.2092 -12 0 2 2 41.36 3.41 2.1829 -5 3 2 4 42.13 12.48 2.1450 5 3 1 4 42.72 1.11 2.1167 -7 1 5 4 42.74 4.07 2.1157 12 0 0 2 42.88 4.12 2.1089 2 2 4 4 43.20 1.67 2.0944 -3 3 3 4 43.30 4.79 2.0897 -7 3 1 4 43.37 7.06 2.0863 5 1 4 4 43.66 1.79 2.0732 -8 2 4 4 44.14 1.47 2.0515 6 0 4 2 44.25 1.57 2.0469 6 2 3 4 44.38 1.47 2.0412 -5 3 3 4 45.49 5.64 1.9939 -9 1 5 4 46.03 1.19 1.9720 12 0 1 2 46.29 8.43 1.9615 -2 2 5 4 46.71 6.59 1.9446 -7 3 3 4 47.63 1.05 1.9091 -9 3 1 4 47.64 4.84 1.9089 9 1 3 4 47.69 6.62 1.9068 0 2 5 4 47.77 2.85 1.9038 -12 2 2 4 47.88 3.79 1.8999 -14 0 2 2 48.12 2.73 1.8909 -9 3 2 4 48.37 3.79 1.8818 -14 0 1 2 48.51 13.20 1.8765 0 4 0 2 48.64 3.11 1.8718 9 3 0 4 48.74 1.32 1.8683 -5 3 4 4 49.16 1.36 1.8534 -12 2 3 4 49.40 1.41 1.8449 0 0 6 2 49.45 4.43 1.8430 12 2 0 4 49.78 5.58 1.8317 -7 1 6 4 49.80 11.53 1.8311 7 3 2 4 49.91 1.59 1.8272 -12 0 5 2 49.98 1.84 1.8248 -1 1 6 4 50.07 8.63 1.8218 -9 3 3 4 50.08 1.08 1.8214 10 2 2 4 50.18 1.45 1.8180 2 2 5 4 50.19 2.47 1.8178 2 4 1 4 50.54 1.78 1.8058 -7 3 4 4 51.22 3.85 1.7837 -2 4 2 4 51.30 4.68 1.7809 -14 0 4 2 52.04 2.47 1.7573 6 0 5 2 53.36 1.75 1.7169 -9 3 4 4 53.60 2.07 1.7097 14 0 1 2 53.88 1.26 1.7015 -2 2 6 4 54.10 1.94 1.6951 -14 2 2 4 54.55 2.66 1.6822 -14 2 1 4 54.89 9.23 1.6726 0 4 3 4 55.50 4.18 1.6557 0 2 6 4 55.77 1.24 1.6484 13 1 2 4 55.79 1.76 1.6478 -16 0 3 2 55.97 2.68 1.6428 -12 2 5 4 56.07 4.37 1.6401 5 3 4 4 56.13 3.81 1.6387 7 1 5 4 56.23 2.22 1.6360 12 0 3 2 56.33 1.24 1.6332 -6 4 3 4 56.35 1.60 1.6328 14 2 0 4 56.44 2.65 1.6302 -2 0 7 2 56.90 2.29 1.6183 -5 1 7 4 57.26 7.09 1.6090 -14 2 4 4 57.84 3.32 1.5941 -9 3 5 4 58.09 2.01 1.5879 2 2 6 4 58.14 1.53 1.5868 16 0 0 2 58.55 1.60 1.5764 -13 3 1 4 59.40 6.56 1.5559 14 2 1 4 59.67 1.01 1.5497 9 3 3 4 61.46 2.60 1.5088 -16 2 3 4 61.51 6.72 1.5075 -7 3 6 4 61.87 3.31 1.4997 12 2 3 4 62.07 1.52 1.4953 -2 2 7 4 62.35 1.05 1.4894 -8 2 7 4 63.36 1.34 1.4679 -9 3 6 4 63.61 1.85 1.4627 14 2 2 4 64.03 1.25 1.4542 -2 4 5 4 64.73 1.06 1.4401 1 5 2 4 65.04 1.03 1.4339 -16 0 6 2 65.17 1.69 1.4315 0 4 5 4 65.23 1.38 1.4302 -12 4 2 4 65.70 1.45 1.4212 -14 0 7 2 66.62 1.71 1.4039 12 4 0 4 66.98 2.71 1.3972 -9 1 8 4 67.03 7.57 1.3962 -7 5 1 4 67.14 4.12 1.3943 7 3 5 4 67.72 2.81 1.3837 0 0 8 2 68.27 1.54 1.3739 -19 1 3 4 68.36 1.71 1.3722 5 1 7 4 69.09 1.01 1.3595 -12 0 8 2 69.63 1.36 1.3503 -7 5 3 4 70.03 1.22 1.3435 14 0 4 2 70.13 1.67 1.3418 4 2 7 4 70.27 3.22 1.3395 -16 2 6 4 70.54 1.27 1.3351 -14 4 2 4 70.90 4.49 1.3291 -14 2 7 4 70.93 1.28 1.3287 -14 4 1 4 71.14 1.25 1.3252 9 5 0 4 71.75 1.26 1.3156 0 4 6 4 72.07 2.05 1.3105 7 5 2 4 72.16 1.05 1.3091 -12 4 5 4 72.67 1.89 1.3012 -7 5 4 4 72.86 1.44 1.2982 0 2 8 4 73.20 1.18 1.2930 7 1 7 4 73.28 2.53 1.2918 -14 4 4 4 74.79 2.58 1.2694 -7 1 9 4 75.10 3.44 1.2649 14 2 4 4 75.18 1.55 1.2638 14 4 1 4 76.08 2.83 1.2510 0 6 0 2 76.50 1.23 1.2453 -3 3 8 4 76.51 1.54 1.2451 -21 1 2 4 77.02 1.60 1.2382 -16 4 3 4 77.26 1.05 1.2349 5 5 4 4 77.35 1.22 1.2336 -20 2 1 4 77.39 1.87 1.2332 12 4 3 4 78.30 1.08 1.2211 12 0 6 2 79.09 1.53 1.2108 -21 1 5 4 81.19 2.22 1.1848 0 6 3 4 83.86 1.00 1.1537 -16 0 9 2 84.63 1.63 1.1452 -7 3 9 4 85.16 1.26 1.1394 -16 4 6 4 85.34 1.09 1.1374 -23 1 4 4 85.76 1.60 1.1330 -14 4 7 4 87.02 1.00 1.1197 -23 1 1 4 87.62 1.93 1.1136 0 4 8 4 89.78 1.30 1.0924 14 4 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.