Co2 H40 N2 O44 V10 Baudrin E, Denis S, Touboul M, Nowogorocki G European Journal of Solid State and Inorganic Chemistry 34 (1997) 1011-1026 Synthesis, crystal structure and thermal properties of (NH4)2Co2V10O28*16(H2O) _cod_database_code 1004121 _database_code_amcsd 0012612 CELL PARAMETERS: 8.8360 10.8650 11.0520 65.180 74.120 71.570 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 901.311 Density (g/cm3): 2.578 MAX. ABS. INTENSITY / VOLUME**2: 11.21034635 RIR: 1.416 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.94 51.51 9.8959 0 0 1 2 9.22 79.47 9.5957 0 1 0 2 10.23 36.15 8.6452 0 1 1 2 10.70 100.00 8.2698 1 0 0 2 11.94 94.99 7.4143 1 1 1 2 12.41 3.83 7.1299 1 1 0 2 12.78 4.89 6.9281 1 0 1 2 15.04 11.15 5.8892 -1 0 1 2 15.68 21.39 5.6529 -1 1 0 2 17.09 5.55 5.1894 1 1 2 2 17.12 10.68 5.1799 1 2 1 2 17.24 1.04 5.1426 -1 1 1 2 17.93 23.10 4.9480 0 0 2 2 18.09 2.03 4.9044 -1 -1 1 2 18.49 17.54 4.7978 0 2 0 2 18.87 6.11 4.7037 1 -1 1 2 19.13 1.92 4.6403 1 2 0 2 19.55 5.06 4.5398 1 2 2 2 20.30 1.76 4.3749 2 1 1 2 20.55 5.03 4.3226 0 2 2 2 21.35 3.25 4.1621 2 1 0 2 21.49 14.49 4.1349 2 0 0 2 22.63 6.73 3.9298 -1 1 2 2 22.76 1.81 3.9069 2 2 1 2 23.04 1.23 3.8607 0 -1 2 2 23.28 4.25 3.8205 -1 2 1 2 23.37 1.68 3.8059 0 -2 1 2 24.01 15.19 3.7071 2 2 2 2 24.55 3.65 3.6265 -1 -2 1 2 24.66 2.56 3.6108 -2 0 1 2 24.88 1.18 3.5790 1 3 1 2 24.98 4.53 3.5649 2 2 0 2 25.14 1.29 3.5425 0 1 3 2 25.22 4.10 3.5313 1 2 3 2 25.34 14.37 3.5143 -2 1 0 2 25.45 9.03 3.5001 1 3 2 2 25.72 4.36 3.4640 2 0 2 2 25.76 1.52 3.4580 -2 -1 1 2 25.81 4.33 3.4524 -1 -1 2 2 26.62 2.49 3.3484 0 2 3 2 26.94 3.01 3.3098 1 -2 1 2 26.97 4.71 3.3061 -2 1 1 2 27.03 10.46 3.2986 0 0 3 2 27.11 2.50 3.2891 0 3 2 2 27.48 3.58 3.2456 1 3 0 2 27.89 4.65 3.1986 0 3 0 2 28.23 7.95 3.1613 2 3 2 2 29.94 8.24 2.9843 -2 -2 1 2 30.32 1.76 2.9481 0 -2 2 2 30.35 2.08 2.9446 -2 0 2 2 30.38 2.02 2.9418 3 1 1 2 30.78 7.97 2.9047 -1 0 3 2 30.98 10.64 2.8862 2 3 3 2 31.10 2.28 2.8756 -1 3 1 2 31.81 20.97 2.8128 2 0 3 2 32.02 2.11 2.7951 -2 2 1 2 32.25 2.90 2.7755 3 0 1 2 32.41 12.83 2.7626 0 -3 1 2 32.48 8.34 2.7566 3 0 0 2 32.56 1.03 2.7501 -1 -3 1 2 32.59 14.73 2.7473 -1 3 2 2 33.96 4.74 2.6400 0 1 4 2 34.34 1.25 2.6113 -1 -1 3 2 34.47 1.08 2.6017 3 3 2 2 34.89 3.61 2.5713 -2 2 2 2 35.00 2.72 2.5634 3 3 1 2 35.11 3.41 2.5559 0 4 2 2 35.13 1.02 2.5548 0 4 1 2 35.67 4.57 2.5169 3 1 3 2 35.73 1.66 2.5130 2 1 4 2 36.44 3.80 2.4658 -1 3 3 2 36.51 1.19 2.4608 1 4 0 2 36.65 5.42 2.4522 -2 -2 2 2 37.29 2.28 2.4115 2 -1 3 2 37.45 12.29 2.4017 0 4 3 2 37.86 10.06 2.3766 3 3 0 2 39.00 1.69 2.3094 3 0 3 2 39.26 16.64 2.2949 2 0 4 2 39.99 1.75 2.2547 -2 -1 3 2 40.88 1.30 2.2073 -3 -1 2 2 41.34 1.37 2.1840 3 1 4 2 41.39 1.05 2.1815 -1 -4 1 2 41.79 8.73 2.1613 0 4 4 2 42.04 1.48 2.1492 1 1 5 2 42.08 2.27 2.1473 -1 3 4 2 42.63 22.85 2.1208 -3 -3 1 2 42.72 3.01 2.1165 -1 4 3 2 42.83 1.71 2.1112 -2 -3 2 2 43.95 2.30 2.0601 3 4 0 2 43.97 2.52 2.0594 -3 -2 2 2 44.16 2.55 2.0508 -2 3 3 2 44.27 5.20 2.0460 3 -1 3 2 44.68 4.41 2.0281 2 -1 4 2 45.06 5.51 2.0121 3 0 4 2 45.16 3.68 2.0079 0 5 3 2 45.87 1.20 1.9785 -4 -1 1 2 46.01 1.12 1.9727 3 3 5 2 47.04 2.97 1.9319 -1 4 4 2 47.60 1.44 1.9102 -2 4 2 2 48.04 1.28 1.8941 -2 4 0 2 48.25 4.58 1.8863 0 5 4 2 48.32 8.37 1.8836 3 1 5 2 48.80 2.20 1.8663 -1 5 2 2 48.93 3.77 1.8614 -3 -4 1 2 49.08 2.02 1.8563 4 1 4 2 50.16 1.33 1.8187 -2 4 3 2 50.21 3.67 1.8169 3 -3 1 2 50.49 1.45 1.8076 3 -1 4 2 50.95 6.99 1.7924 -4 -3 1 2 51.04 4.38 1.7895 2 6 2 2 52.31 1.35 1.7490 3 0 5 2 52.86 1.09 1.7320 4 0 4 2 53.32 6.21 1.7180 5 3 3 2 53.47 4.55 1.7137 -3 1 4 2 53.49 7.41 1.7132 -1 5 4 2 55.65 2.40 1.6515 -1 -3 4 2 56.25 1.03 1.6355 -4 0 3 2 56.39 2.87 1.6316 0 -2 5 2 58.69 1.05 1.5731 3 -4 1 2 58.90 1.34 1.5679 3 -3 3 2 59.10 1.06 1.5632 4 0 5 2 59.54 7.23 1.5528 2 4 7 2 60.45 1.43 1.5313 2 7 2 2 61.21 1.67 1.5143 3 7 3 2 62.20 1.21 1.4925 5 0 4 2 63.08 1.06 1.4737 5 -1 3 2 63.40 2.37 1.4670 -4 1 4 2 63.63 1.93 1.4624 -1 -4 4 2 63.69 1.93 1.4611 0 -3 5 2 63.83 3.07 1.4583 6 3 3 2 64.10 1.18 1.4527 6 2 3 2 64.62 1.04 1.4423 -3 -3 4 2 64.97 1.11 1.4355 5 3 6 2 65.30 1.39 1.4290 -4 2 4 2 65.34 2.51 1.4282 -3 5 0 2 65.37 1.43 1.4275 5 6 2 2 66.28 1.45 1.4102 2 0 7 2 66.50 1.03 1.4060 2 7 6 2 67.97 3.73 1.3792 4 -4 1 2 69.30 1.06 1.3560 2 8 3 2 70.36 2.96 1.3381 3 8 3 2 70.82 1.30 1.3305 -4 1 5 2 70.88 1.12 1.3294 3 5 8 2 74.67 1.14 1.2711 5 7 6 2 77.23 1.56 1.2353 -1 1 8 2 77.27 1.03 1.2348 7 4 4 2 77.44 1.12 1.2324 -6 2 1 2 78.99 1.26 1.2121 0 -7 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.