Airdite Kang H Y, Lee W C, Wang S L Inorganic Chemistry 31 (1992) 4743-4748 Hydrothermal synthesis and structural characterization of four layered vanadyl(IV) phosphate hydrates A(VO)2(PO4)2*4H2O (A=Co,Ca,Sr,Pb) Locality: synthetic _database_code_amcsd 0012706 CELL PARAMETERS: 9.0260 9.0100 12.8410 90.000 100.190 90.000 SPACE GROUP: Cc X-RAY WAVELENGTH: 1.541838 Cell Volume: 1027.813 Density (g/cm3): 3.124 MAX. ABS. INTENSITY / VOLUME**2: 12.23164841 RIR: 1.275 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.00 12.32 6.3259 1 1 0 2 14.01 42.24 6.3192 0 0 2 1 14.85 39.32 5.9656 -1 1 1 2 16.44 22.36 5.3915 1 1 1 2 18.55 26.40 4.7821 -1 1 2 2 19.71 5.32 4.5050 0 2 0 2 19.99 10.96 4.4418 2 0 0 1 20.93 8.43 4.2435 0 2 1 2 21.09 7.19 4.2132 1 1 2 2 22.34 6.22 3.9803 -2 0 2 1 23.86 34.80 3.7299 -1 1 3 2 24.26 5.82 3.6683 0 2 2 2 26.49 3.78 3.3646 2 0 2 1 26.86 28.64 3.3188 1 1 3 2 28.21 50.70 3.1636 -2 2 1 2 28.21 9.44 3.1629 2 2 0 2 28.24 42.74 3.1596 0 0 4 1 29.02 2.15 3.0770 0 2 3 2 29.96 6.89 2.9828 -2 2 2 2 29.97 95.42 2.9811 2 2 1 2 29.98 4.58 2.9807 -1 1 4 2 31.39 10.93 2.8494 -3 1 1 2 31.44 12.26 2.8451 1 3 0 2 31.72 2.68 2.8212 -2 0 4 1 31.81 4.18 2.8132 3 1 0 2 31.85 3.18 2.8100 -1 3 1 2 32.59 2.93 2.7473 -3 1 2 2 32.65 2.77 2.7426 1 3 1 2 33.21 47.33 2.6978 -2 2 3 2 33.23 4.38 2.6958 2 2 2 2 33.25 10.97 2.6942 1 1 4 2 33.79 6.59 2.6530 3 1 1 2 33.81 8.68 2.6512 -1 3 2 2 34.68 2.46 2.5868 0 2 4 2 35.26 13.62 2.5454 -3 1 3 2 35.32 11.53 2.5410 1 3 2 2 36.58 4.00 2.4563 -1 1 5 2 37.10 5.96 2.4231 3 1 2 2 37.12 6.17 2.4223 -1 3 3 2 37.62 2.70 2.3910 -2 2 4 2 37.65 2.07 2.3890 2 2 3 2 37.75 1.73 2.3832 2 0 4 1 39.13 4.71 2.3020 -3 1 4 2 39.20 4.82 2.2982 1 3 3 2 40.03 3.50 2.2525 0 4 0 2 40.05 2.40 2.2515 1 1 5 2 40.60 11.49 2.2218 -4 0 2 1 40.69 5.88 2.2176 0 4 1 2 40.94 1.75 2.2044 0 2 5 2 41.49 6.59 2.1767 3 1 3 2 41.49 6.09 2.1765 -1 3 4 2 42.61 5.44 2.1217 0 4 2 2 42.89 5.42 2.1086 3 3 0 2 42.93 1.43 2.1066 2 2 4 2 42.94 16.33 2.1064 0 0 6 1 43.50 4.17 2.0804 -3 3 2 2 43.54 8.99 2.0786 -1 1 6 2 43.95 4.39 2.0602 -3 1 5 2 44.02 4.82 2.0571 1 3 4 2 44.21 1.72 2.0487 -2 0 6 1 44.44 4.02 2.0386 3 3 1 2 44.93 11.07 2.0176 -4 2 1 2 45.13 10.38 2.0091 -2 4 1 2 45.13 7.24 2.0089 2 4 0 2 45.52 3.39 1.9927 -4 2 2 2 45.54 4.89 1.9920 4 2 0 2 45.62 9.97 1.9885 -3 3 3 2 45.63 9.49 1.9881 4 0 2 1 45.67 4.52 1.9864 0 4 3 2 46.31 1.17 1.9604 -2 4 2 2 46.33 3.40 1.9599 2 4 1 2 46.70 2.18 1.9452 -1 3 5 2 46.70 2.06 1.9450 3 1 4 2 47.12 1.35 1.9286 3 3 2 2 47.16 2.54 1.9271 1 1 6 2 47.28 2.25 1.9226 -4 2 3 2 47.31 2.54 1.9214 4 2 1 2 48.62 4.42 1.8725 -2 4 3 2 48.81 1.77 1.8658 -3 3 4 2 48.83 1.00 1.8649 -2 2 6 2 48.88 2.67 1.8634 2 2 5 2 49.51 2.95 1.8411 -3 1 6 2 49.58 3.95 1.8386 1 3 5 2 49.71 4.15 1.8341 0 4 4 2 50.11 2.23 1.8204 -4 2 4 2 50.15 2.98 1.8189 4 2 2 2 50.80 9.61 1.7972 3 3 3 2 50.81 5.50 1.7969 -1 1 7 2 51.18 1.73 1.7849 2 0 6 1 51.68 1.35 1.7689 -5 1 1 2 51.76 1.31 1.7660 1 5 0 2 51.97 3.12 1.7595 2 4 3 2 52.57 4.19 1.7408 -1 3 6 2 52.59 5.43 1.7404 3 1 5 2 52.93 4.09 1.7299 -3 3 5 2 53.27 1.76 1.7196 -5 1 3 2 53.89 1.29 1.7013 -4 2 5 2 53.95 1.11 1.6996 4 2 3 2 54.36 2.50 1.6876 5 1 1 2 54.43 3.44 1.6856 1 5 2 2 54.48 5.41 1.6843 -4 0 6 1 54.57 3.40 1.6817 0 4 5 2 54.59 3.79 1.6812 1 1 7 2 54.77 2.69 1.6759 0 2 7 2 55.34 4.20 1.6600 3 3 4 2 56.16 2.05 1.6379 -2 4 5 2 57.21 1.25 1.6103 5 1 2 2 57.84 2.29 1.5942 -4 4 1 2 57.85 3.39 1.5940 -3 3 6 2 58.34 9.05 1.5818 -4 4 2 2 58.35 8.86 1.5815 4 4 0 2 58.44 2.13 1.5793 -2 0 8 1 58.50 2.03 1.5777 -4 2 6 2 58.57 1.17 1.5760 4 2 4 2 58.91 2.18 1.5678 -5 1 5 2 59.02 3.20 1.5652 -1 5 4 2 59.82 2.27 1.5461 -4 4 3 2 59.85 1.85 1.5454 4 4 1 2 60.14 1.37 1.5385 0 4 6 2 60.59 1.10 1.5283 -3 5 2 2 60.63 1.95 1.5273 3 3 5 2 61.15 2.03 1.5156 -2 4 6 2 61.18 3.64 1.5148 2 4 5 2 61.77 2.01 1.5018 -6 0 2 1 62.25 2.44 1.4914 -4 4 4 2 62.26 2.42 1.4912 0 6 1 2 62.28 1.07 1.4908 0 2 8 2 62.29 2.21 1.4906 4 4 2 2 62.35 1.37 1.4893 2 2 7 2 62.76 1.37 1.4806 6 0 0 1 63.47 3.56 1.4657 -3 3 7 2 63.50 1.57 1.4650 3 5 2 2 63.70 1.05 1.4610 0 6 2 2 63.85 3.99 1.4578 -4 2 7 2 63.93 3.75 1.4562 4 2 5 2 64.89 1.52 1.4369 -3 5 4 2 65.53 7.04 1.4245 -6 2 1 2 65.63 6.27 1.4226 -2 6 1 2 65.63 1.89 1.4226 2 6 0 2 66.20 1.13 1.4117 2 0 8 1 66.35 1.27 1.4089 4 0 6 1 66.84 3.49 1.3997 -2 4 7 2 66.88 3.01 1.3989 2 4 6 2 69.62 2.95 1.3504 -3 1 9 2 69.70 2.00 1.3491 1 3 8 2 69.96 1.42 1.3447 4 2 6 2 70.20 1.56 1.3406 0 2 9 2 70.78 1.64 1.3311 5 1 5 2 70.82 3.01 1.3305 1 5 6 2 71.00 3.31 1.3276 -6 2 5 2 71.12 1.10 1.3256 -2 6 4 2 71.14 3.12 1.3252 2 6 3 2 73.19 1.50 1.2931 -2 4 8 2 73.49 2.11 1.2886 -1 3 9 2 73.52 1.70 1.2881 3 1 8 2 73.60 1.16 1.2870 -5 1 8 2 74.57 1.25 1.2727 -7 1 1 2 74.63 1.13 1.2718 -5 5 2 2 74.64 2.59 1.2715 6 2 3 2 74.69 2.07 1.2709 -2 6 5 2 74.70 1.10 1.2706 -1 7 1 2 74.99 1.19 1.2666 -7 1 3 2 75.04 1.16 1.2658 -5 3 7 2 75.08 1.77 1.2652 5 5 0 2 75.15 1.55 1.2642 1 7 1 2 75.59 1.07 1.2579 6 0 4 1 76.55 1.44 1.2445 -4 2 9 2 76.65 1.86 1.2432 4 2 7 2 77.41 1.43 1.2329 -3 1 10 2 77.49 1.78 1.2318 1 3 9 2 79.94 1.15 1.2000 -5 1 9 2 80.06 1.47 1.1986 -1 5 8 2 80.25 1.18 1.1962 2 4 8 2 80.49 1.00 1.1933 -5 3 8 2 80.61 1.70 1.1917 3 5 6 2 81.58 1.32 1.1801 -1 3 10 2 81.61 1.71 1.1797 3 1 9 2 83.07 1.02 1.1627 2 0 10 1 83.57 1.50 1.1570 -3 5 8 2 83.79 1.90 1.1545 0 6 7 2 84.15 2.06 1.1504 -5 5 6 2 84.16 1.48 1.1503 7 1 3 2 84.25 2.18 1.1493 -1 7 5 2 86.20 1.53 1.1283 -7 1 7 2 86.36 1.96 1.1266 5 5 4 2 86.40 2.07 1.1261 1 7 5 2 86.82 1.03 1.1218 0 8 1 2 86.84 1.55 1.1215 6 0 6 1 87.65 1.55 1.1133 0 2 11 2 87.89 1.66 1.1109 -8 0 4 1 87.92 1.05 1.1106 -2 4 10 2 87.93 1.74 1.1105 8 0 0 1 87.98 1.45 1.1100 2 4 9 2 88.10 2.30 1.1088 0 8 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.