Deveroite-(Ce) Ollendorff W, Weigel F Inorganic and Nuclear Chemistry Letters 5 (1969) 263-269 The crystal structure of some lanthanide oxalate decahydrates, Ln2(C2O4)3*10H2O, with Ln = La, Ce, Pr, and Nd Locality: synthetic _database_code_amcsd 0019971 CELL PARAMETERS: 11.3470 9.6300 10.3920 90.000 114.520 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1033.143 Density (g/cm3): 2.353 MAX. ABS. INTENSITY / VOLUME**2: 13.41495392 RIR: 1.857 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.57 65.49 10.3237 1 0 0 2 12.57 32.74 7.0419 1 1 0 4 13.12 67.11 6.7466 0 1 1 4 13.38 100.00 6.6156 -1 1 1 4 17.08 44.11 5.1902 -1 0 2 2 17.18 9.12 5.1618 2 0 0 2 17.71 86.23 5.0090 1 1 1 4 18.29 65.52 4.8511 -2 1 1 4 18.43 50.77 4.8150 0 2 0 2 19.51 1.90 4.5495 2 1 0 4 20.35 7.70 4.3637 1 2 0 4 20.70 5.96 4.2906 0 2 1 4 20.87 7.31 4.2563 -1 2 1 4 21.59 11.42 4.1153 -2 1 2 4 23.73 8.18 3.7493 1 0 2 2 24.89 12.67 3.5767 -3 0 2 2 25.23 28.38 3.5299 -1 2 2 4 25.49 3.18 3.4939 1 1 2 4 25.89 18.77 3.4412 3 0 0 2 26.95 7.84 3.3078 -2 2 2 4 27.93 5.72 3.1949 -2 1 3 4 29.13 14.41 3.0652 1 3 0 4 29.38 6.73 3.0396 0 3 1 4 29.47 9.55 3.0309 2 2 1 4 29.83 34.32 2.9953 0 1 3 4 30.48 14.12 2.9324 2 0 2 2 30.90 12.73 2.8943 -3 1 3 4 31.15 10.11 2.8712 -3 2 2 4 31.78 14.71 2.8158 1 3 1 4 31.87 16.09 2.8078 -4 0 2 2 31.97 9.16 2.7997 3 2 0 4 31.98 1.55 2.7985 -1 2 3 4 32.12 3.11 2.7868 -2 3 1 4 32.32 2.38 2.7701 -2 2 3 4 32.52 13.88 2.7532 3 1 1 4 32.86 3.76 2.7259 2 3 0 4 33.24 2.54 2.6956 -4 1 2 4 33.29 10.70 2.6911 -4 1 1 4 33.75 2.61 2.6556 0 3 2 4 34.00 4.51 2.6370 0 2 3 4 34.18 25.10 2.6233 -2 3 2 4 34.31 2.95 2.6139 1 1 3 4 34.56 9.32 2.5951 -2 0 4 2 34.95 6.43 2.5673 -3 2 3 4 35.85 4.40 2.5045 2 2 2 4 36.08 2.05 2.4892 -3 0 4 2 36.86 2.42 2.4384 1 3 2 4 37.06 3.94 2.4255 -4 2 2 4 37.31 2.88 2.4100 -3 1 4 4 37.35 1.36 2.4075 0 4 0 2 37.65 1.99 2.3890 -3 3 2 4 38.04 2.22 2.3655 1 2 3 4 38.07 2.39 2.3637 0 0 4 2 38.21 1.28 2.3556 3 0 2 2 38.59 1.85 2.3331 0 4 1 4 38.65 3.13 2.3298 -2 3 3 4 38.69 16.70 2.3275 -1 4 1 4 39.25 1.31 2.2956 0 1 4 4 39.38 7.96 2.2882 3 1 2 4 39.44 7.28 2.2844 -2 2 4 4 39.47 8.23 2.2828 -4 2 3 4 39.60 4.11 2.2760 -4 0 4 2 40.07 9.33 2.2503 -1 2 4 4 40.10 12.01 2.2489 0 3 3 4 40.34 1.31 2.2360 2 1 3 4 40.50 1.33 2.2272 1 4 1 4 40.92 2.25 2.2052 -3 3 3 4 40.97 8.16 2.2027 4 1 1 4 41.34 2.38 2.1840 -1 4 2 4 41.79 7.33 2.1616 -5 1 1 4 42.21 1.09 2.1408 3 3 1 4 42.24 13.54 2.1394 -5 1 3 4 42.64 7.89 2.1206 1 0 4 2 42.83 6.64 2.1113 -4 3 1 4 43.63 4.60 2.0745 2 2 3 4 43.66 1.17 2.0734 1 3 3 4 43.85 8.14 2.0647 5 0 0 2 44.01 5.63 2.0577 -4 2 4 4 44.21 16.78 2.0487 2 4 1 4 44.64 12.73 2.0301 -3 4 1 4 44.72 4.27 2.0266 -5 0 4 2 45.07 8.10 2.0114 4 3 0 4 45.09 1.52 2.0107 -3 1 5 4 45.48 1.06 1.9944 -1 3 4 4 45.75 1.42 1.9832 -5 1 4 4 46.01 1.31 1.9727 3 4 0 4 46.02 7.16 1.9723 -1 4 3 4 46.04 10.73 1.9714 -1 1 5 4 46.15 8.33 1.9671 -3 3 4 4 46.27 5.16 1.9622 -2 4 3 4 46.57 4.66 1.9503 4 0 2 2 46.81 9.81 1.9407 1 2 4 4 47.28 5.91 1.9227 -4 1 5 4 47.45 2.99 1.9159 3 1 3 4 47.72 3.03 1.9059 -2 2 5 4 47.79 3.78 1.9034 0 3 4 4 47.90 4.86 1.8991 3 3 2 4 47.94 3.62 1.8976 5 2 0 4 48.06 5.84 1.8933 1 5 0 4 48.19 3.87 1.8882 -6 0 2 2 48.75 1.54 1.8679 -5 2 4 4 49.18 1.13 1.8527 -5 3 2 4 49.27 2.95 1.8494 4 3 1 4 49.39 2.31 1.8453 3 4 1 4 49.90 1.38 1.8277 -4 4 2 4 49.98 1.18 1.8249 -5 3 1 4 50.37 1.65 1.8115 -5 3 3 4 50.49 1.48 1.8077 4 2 2 4 50.58 2.93 1.8045 2 5 0 4 50.67 3.97 1.8016 1 4 3 4 51.22 1.81 1.7837 0 5 2 4 51.52 5.25 1.7738 -2 5 2 4 51.80 1.27 1.7650 -2 4 4 4 51.82 5.07 1.7642 -4 4 3 4 51.95 1.35 1.7601 0 2 5 4 52.02 2.07 1.7579 -6 2 2 4 52.69 1.38 1.7371 5 2 1 4 53.24 1.40 1.7206 6 0 0 2 53.49 2.14 1.7132 1 5 2 4 53.52 1.05 1.7123 -6 2 1 4 53.62 1.19 1.7091 1 1 5 4 53.73 1.65 1.7060 -1 3 5 4 53.83 1.34 1.7031 -5 2 5 4 56.19 3.71 1.6371 -6 1 5 4 56.52 1.38 1.6282 -3 2 6 4 56.88 2.52 1.6188 2 3 4 4 56.93 1.39 1.6176 -5 0 6 2 58.31 1.35 1.5824 0 6 1 4 58.58 1.34 1.5758 0 0 6 2 58.74 1.30 1.5720 -2 4 5 4 58.96 1.54 1.5666 5 2 2 4 59.14 3.01 1.5623 -6 3 4 4 59.22 2.29 1.5603 6 1 1 4 59.40 2.09 1.5560 2 1 5 4 59.93 3.53 1.5436 4 5 0 4 60.12 2.85 1.5390 -7 1 1 4 60.26 1.14 1.5359 -1 5 4 4 60.37 3.62 1.5334 -5 2 6 4 60.81 4.66 1.5233 -3 5 4 4 61.80 1.85 1.5011 -7 2 4 4 61.96 1.00 1.4977 -4 3 6 4 61.96 2.85 1.4976 0 2 6 4 62.17 1.72 1.4931 0 5 4 4 62.27 2.12 1.4911 3 5 2 4 62.45 1.22 1.4871 0 4 5 4 62.58 3.26 1.4843 2 6 1 4 62.91 1.00 1.4774 -1 3 6 4 62.92 2.00 1.4771 -3 6 1 4 63.11 2.55 1.4731 5 4 1 4 63.34 2.04 1.4683 -5 5 2 4 63.85 2.62 1.4579 -6 4 1 4 63.88 1.54 1.4572 -4 1 7 4 64.02 1.70 1.4544 -1 6 3 4 64.08 1.96 1.4531 5 1 3 4 64.37 2.01 1.4473 -2 1 7 4 65.84 1.34 1.4184 6 3 1 4 65.85 1.62 1.4183 -3 2 7 4 66.01 1.55 1.4152 2 3 5 4 66.65 2.72 1.4032 -8 1 3 4 66.68 1.46 1.4026 4 2 4 4 67.94 1.43 1.3796 4 4 3 4 68.79 1.28 1.3647 -4 6 3 4 68.85 1.35 1.3637 1 7 0 4 70.04 1.99 1.3434 2 5 4 4 70.06 1.60 1.3431 -7 4 3 4 71.66 1.06 1.3169 -2 7 2 4 72.07 1.68 1.3105 -6 5 4 4 73.47 1.24 1.2888 -7 1 7 4 74.63 1.57 1.2717 -4 5 6 4 74.77 2.02 1.2696 -2 6 5 4 75.21 1.07 1.2634 -3 4 7 4 77.85 1.22 1.2270 3 4 5 4 79.55 1.12 1.2050 -6 2 8 4 83.16 1.17 1.1617 4 6 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.