Phosphoferrite Moore P B, Araki T Inorganic Chemistry 15 (1976) 316-321 A mixed-valence solid-solution series: Crystal structures of phosphoferrite, Fe3(H2O)3[PO4]2, and kryzhanovskite, Fe3(OH)3[PO4]2 Locality: synthetic _database_code_amcsd 0012680 CELL PARAMETERS: 9.4600 10.0240 8.6700 90.000 90.000 90.000 SPACE GROUP: Pbna X-RAY WAVELENGTH: 1.541838 Cell Volume: 822.150 Density (g/cm3): 3.324 MAX. ABS. INTENSITY / VOLUME**2: 14.50710259 RIR: 1.421 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.85 3.44 6.3917 1 0 1 4 16.45 20.48 5.3893 1 1 1 8 17.70 45.76 5.0120 0 2 0 2 18.76 30.66 4.7300 2 0 0 2 20.49 4.61 4.3350 0 0 2 2 20.77 30.45 4.2777 2 1 0 4 22.54 7.51 3.9440 1 2 1 8 23.19 1.58 3.8362 2 1 1 8 25.90 17.33 3.4400 2 2 0 4 27.20 2.91 3.2787 0 2 2 4 27.90 100.00 3.1975 2 2 1 8 27.92 36.91 3.1958 2 0 2 4 28.82 29.18 3.0979 1 2 2 8 29.33 6.16 3.0448 2 1 2 8 30.16 6.63 2.9634 3 0 1 4 30.18 4.93 2.9611 1 3 1 8 32.39 15.81 2.7639 1 0 3 4 32.82 35.75 2.7291 2 3 0 4 33.25 11.35 2.6947 2 2 2 8 33.64 26.58 2.6645 1 1 3 8 34.45 1.22 2.6032 2 3 1 8 35.18 1.49 2.5509 3 2 1 8 35.21 5.25 2.5486 1 3 2 8 35.87 9.58 2.5036 0 2 3 4 36.35 20.10 2.4713 3 1 2 8 37.15 27.33 2.4203 1 2 3 8 37.35 3.62 2.4075 0 4 1 4 38.59 11.36 2.3331 1 4 1 8 40.55 14.31 2.2247 4 1 1 8 40.70 16.87 2.2171 3 3 1 8 41.63 11.57 2.1696 0 4 2 4 41.67 3.78 2.1675 0 0 4 2 42.12 3.84 2.1455 2 4 1 8 42.43 2.80 2.1306 3 0 3 4 42.44 1.80 2.1297 1 3 3 8 42.76 14.05 2.1147 1 4 2 8 43.42 2.32 2.0840 3 1 3 8 43.58 1.32 2.0766 4 2 1 8 43.79 1.74 2.0673 1 1 4 8 44.70 8.46 2.0271 3 3 2 8 45.73 2.96 1.9842 2 3 3 8 46.02 3.98 1.9720 2 4 2 8 46.06 1.70 1.9705 2 0 4 4 46.30 16.47 1.9608 3 2 3 8 47.00 5.84 1.9335 2 1 4 8 47.08 6.49 1.9304 4 3 0 4 47.40 7.99 1.9181 4 2 2 8 47.52 9.35 1.9135 3 4 1 8 48.30 2.56 1.8842 4 3 1 8 49.30 5.52 1.8485 5 0 1 4 50.19 3.77 1.8178 5 1 1 8 50.83 4.53 1.7964 3 3 3 8 51.10 1.38 1.7874 3 4 2 8 51.12 1.34 1.7869 1 5 2 8 52.00 3.45 1.7585 3 1 4 8 52.78 4.81 1.7343 5 2 1 8 53.28 1.29 1.7192 4 2 3 8 53.64 5.77 1.7087 5 1 2 8 53.74 3.25 1.7056 1 0 5 4 54.03 5.74 1.6973 2 3 4 8 54.58 1.18 1.6814 1 1 5 8 54.96 2.06 1.6707 0 6 0 2 56.10 6.01 1.6394 0 4 4 4 56.13 3.85 1.6387 5 2 2 8 56.13 5.22 1.6387 0 2 5 4 56.71 1.28 1.6232 3 4 3 8 56.72 1.11 1.6228 1 5 3 8 56.93 3.47 1.6175 5 3 1 8 56.97 11.11 1.6164 1 6 1 8 57.01 1.56 1.6153 1 4 4 8 57.04 7.66 1.6147 1 2 5 8 57.34 1.52 1.6070 2 1 5 8 57.66 2.40 1.5988 4 4 2 8 57.69 1.36 1.5979 4 0 4 4 58.29 1.75 1.5829 5 0 3 4 58.49 2.05 1.5780 4 1 4 8 58.57 10.70 1.5761 3 5 2 8 58.60 1.33 1.5753 2 6 0 4 59.08 4.55 1.5636 5 1 3 8 59.28 2.67 1.5589 0 6 2 4 59.34 1.70 1.5575 6 1 0 4 59.41 2.19 1.5556 2 5 3 8 59.66 2.37 1.5499 2 6 1 8 59.70 12.40 1.5490 2 4 4 8 59.72 3.27 1.5484 2 2 5 8 60.16 2.75 1.5382 1 6 2 8 60.85 4.94 1.5224 4 2 4 8 60.98 2.78 1.5194 3 0 5 4 60.99 1.03 1.5191 1 3 5 8 61.58 13.03 1.5060 4 5 1 8 61.75 2.19 1.5023 3 1 5 8 62.43 1.56 1.4876 5 4 1 8 62.70 2.86 1.4819 6 2 1 8 63.97 3.40 1.4553 3 6 1 8 64.49 2.02 1.4450 0 0 6 2 64.66 5.94 1.4416 4 3 4 8 65.22 2.02 1.4305 5 3 3 8 65.46 1.35 1.4259 6 3 0 4 66.07 4.40 1.4141 1 1 6 8 66.29 1.08 1.4100 1 4 5 8 66.54 1.13 1.4053 2 5 4 8 67.65 1.88 1.3850 4 1 5 8 67.75 1.08 1.3831 3 3 5 8 67.81 1.18 1.3820 2 0 6 4 68.28 3.04 1.3737 1 2 6 8 68.43 3.22 1.3711 6 1 3 8 68.43 1.95 1.3710 5 2 4 8 68.46 3.18 1.3706 2 7 0 4 69.38 1.19 1.3545 6 3 2 8 70.34 1.86 1.3383 5 4 3 8 70.53 5.37 1.3353 7 0 1 4 70.71 1.32 1.3322 2 2 6 8 71.27 2.23 1.3232 0 6 4 4 71.53 1.26 1.3190 6 4 1 8 72.30 1.96 1.3068 2 7 2 8 72.64 1.50 1.3016 4 6 2 8 73.38 1.38 1.2903 7 2 1 8 74.40 2.00 1.2750 6 0 4 4 74.45 2.29 1.2743 2 6 4 8 74.65 1.17 1.2715 1 7 3 8 75.18 1.16 1.2638 2 5 5 8 76.81 1.14 1.2410 1 4 6 8 77.20 2.56 1.2357 6 2 4 8 78.06 1.74 1.2242 7 0 3 4 78.37 1.03 1.2201 3 6 4 8 79.70 1.04 1.2031 5 6 2 8 79.98 1.31 1.1996 2 8 1 8 80.42 3.28 1.1941 1 8 2 8 82.73 1.61 1.1665 2 8 2 8 83.01 2.20 1.1633 1 5 6 8 84.47 1.77 1.1469 4 5 5 8 84.49 1.31 1.1467 6 6 0 4 84.99 1.42 1.1412 1 8 3 8 85.19 1.37 1.1390 6 5 3 8 85.22 1.90 1.1387 5 4 5 8 88.70 1.13 1.1028 1 4 7 8 88.99 3.24 1.1000 7 4 3 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.