S4N4 LeLucia M L, Coppens P Inorganic Chemistry 17 (1978) 2336-2338 Crystal structure of tetrasulfur tetranitride (S4N4) at 120 K Locality: synthetic Note: T = 120 K _database_code_amcsd 0012686 CELL PARAMETERS: 8.7520 7.0840 8.6290 90.000 93.680 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 533.888 Density (g/cm3): 2.292 MAX. ABS. INTENSITY / VOLUME**2: 9.548813976 RIR: 1.356 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.97 19.63 6.3388 -1 0 1 2 14.90 20.03 5.9442 1 0 1 2 18.79 100.00 4.7238 -1 1 1 4 19.49 73.76 4.5535 1 1 1 4 20.34 32.67 4.3670 2 0 0 2 20.63 5.88 4.3056 0 0 2 2 24.19 15.88 3.6793 0 1 2 4 25.14 6.73 3.5420 0 2 0 2 25.58 8.19 3.4829 -2 1 1 4 26.63 7.16 3.3471 2 1 1 4 28.16 3.91 3.1694 -2 0 2 2 28.88 24.54 3.0920 -1 2 1 4 29.35 6.94 3.0428 1 2 1 4 30.07 9.55 2.9721 2 0 2 2 30.91 10.15 2.8930 -2 1 2 4 31.81 28.88 2.8133 -3 0 1 2 32.20 6.68 2.7804 -1 0 3 2 32.55 5.76 2.7509 2 2 0 4 32.67 25.60 2.7407 2 1 2 4 32.74 45.65 2.7354 0 2 2 4 33.11 9.26 2.7058 3 0 1 2 33.48 10.23 2.6764 1 0 3 2 33.69 2.94 2.6603 0 1 3 4 33.80 5.79 2.6517 -2 2 1 4 33.94 2.49 2.6412 -1 2 2 4 34.30 3.16 2.6147 -3 1 1 4 34.63 1.15 2.5903 2 2 1 4 34.66 7.16 2.5881 -1 1 3 4 34.76 10.98 2.5805 1 2 2 4 38.10 9.80 2.3619 -2 2 2 4 38.57 2.68 2.3345 -2 1 3 4 39.53 1.07 2.2795 1 3 0 4 39.58 2.81 2.2768 2 2 2 4 40.75 5.04 2.2142 2 1 3 4 40.78 8.13 2.2128 -1 3 1 4 41.13 4.29 2.1945 1 3 1 4 42.02 5.15 2.1502 3 2 1 4 42.80 7.64 2.1129 -3 0 3 2 43.72 2.47 2.0704 0 3 2 4 43.96 5.11 2.0598 0 1 4 4 44.57 1.11 2.0329 -1 1 4 4 44.67 2.69 2.0287 -1 3 2 4 44.76 5.15 2.0248 -3 1 3 4 45.22 1.54 2.0053 2 3 1 4 45.34 1.45 2.0000 4 1 1 4 45.35 1.25 1.9999 -4 0 2 2 45.79 2.67 1.9814 3 0 3 2 47.23 12.56 1.9246 -4 1 2 4 47.66 8.76 1.9082 3 1 3 4 47.91 3.09 1.8988 4 0 2 2 48.32 2.86 1.8836 2 0 4 2 49.01 4.43 1.8587 4 2 0 4 49.55 2.86 1.8397 0 2 4 4 49.71 3.25 1.8341 4 1 2 4 50.28 1.92 1.8146 -3 2 3 4 50.46 3.04 1.8087 -3 3 1 4 50.72 9.34 1.7998 -1 3 3 4 51.31 1.28 1.7806 1 2 4 4 51.36 2.36 1.7791 3 3 1 4 51.62 3.29 1.7707 1 3 3 4 52.74 4.54 1.7357 1 4 0 4 52.80 1.06 1.7337 -5 0 1 2 53.57 2.44 1.7107 -1 0 5 2 53.67 1.52 1.7077 -2 3 3 4 54.25 1.06 1.6909 5 0 1 2 55.38 1.15 1.6589 2 3 3 4 55.90 1.68 1.6447 5 1 1 4 56.16 1.17 1.6379 0 4 2 4 56.27 1.57 1.6348 3 1 4 4 56.86 1.72 1.6194 -2 4 1 4 57.41 2.82 1.6051 2 4 1 4 58.96 1.48 1.5666 5 2 0 4 59.56 4.85 1.5522 1 3 4 4 59.80 1.15 1.5465 -4 1 4 4 60.22 1.10 1.5366 -5 0 3 2 61.04 1.74 1.5181 -2 3 4 4 61.39 1.57 1.5101 1 2 5 4 62.45 1.66 1.4871 -2 2 5 4 63.14 4.49 1.4725 2 3 4 4 63.96 4.16 1.4557 6 0 0 2 66.75 3.64 1.4013 -3 2 5 4 66.96 1.10 1.3975 -5 3 1 4 67.22 1.29 1.3927 6 1 1 4 68.02 1.57 1.3782 1 5 1 4 68.23 1.13 1.3745 -5 1 4 4 68.35 1.60 1.3724 4 3 3 4 68.67 1.02 1.3669 -4 4 1 4 69.88 1.12 1.3461 -2 3 5 4 70.50 2.10 1.3358 3 2 5 4 70.92 1.02 1.3289 6 1 2 4 71.01 1.17 1.3274 2 5 1 4 71.09 3.28 1.3261 1 5 2 4 71.73 5.91 1.3158 -4 3 4 4 73.40 1.02 1.2900 4 1 5 4 76.02 1.62 1.2518 2 2 6 4 77.61 1.02 1.2302 4 2 5 4 77.68 1.73 1.2293 -2 5 3 4 80.46 1.57 1.1936 -5 2 5 4 81.54 1.65 1.1805 5 4 2 4 81.96 1.47 1.1756 -7 2 1 4 83.20 1.69 1.1612 -1 2 7 4 86.28 1.49 1.1274 2 6 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.