Ferroalluaudite Corbin D R, Whitney J F, Fultz W C, Stucky G D, Eddy M M, Cheetham A K Inorganic Chemistry 25 (1986) 2279-2280 Synthesis of open-framework transition-metal phosphates using organometallic precursors in acidic media. Preparation and structural characterization of Fe5P4O20H10 and NaFe3P3O12 Note: structure from ICSD _database_code_amcsd 0012695 CELL PARAMETERS: 11.9980 12.3280 6.5000 90.000 114.185 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 877.037 Density (g/cm3): 3.600 MAX. ABS. INTENSITY / VOLUME**2: 10.77887498 RIR: 0.975 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.81 8.44 8.1847 1 1 0 4 14.37 100.00 6.1640 0 2 0 2 16.20 34.35 5.4725 2 0 0 2 20.79 5.37 4.2733 0 2 1 4 21.02 18.09 4.2259 1 1 1 4 21.72 9.13 4.0924 2 2 0 4 22.30 1.92 3.9872 -2 2 1 4 23.12 16.48 3.8471 1 3 0 4 25.46 35.79 3.4983 3 1 0 4 27.74 4.30 3.2165 -2 0 2 2 28.71 88.72 3.1092 -1 1 2 4 28.97 11.02 3.0820 0 4 0 2 29.44 31.18 3.0340 1 3 1 4 30.14 22.23 2.9647 0 0 2 2 30.94 16.92 2.8900 -3 1 2 4 31.37 2.38 2.8516 -2 2 2 4 31.62 5.19 2.8294 -3 3 1 4 32.73 22.68 2.7362 4 0 0 2 32.75 12.33 2.7347 0 4 1 4 32.83 70.27 2.7282 3 3 0 4 33.37 74.16 2.6854 2 4 0 4 33.54 2.26 2.6718 0 2 2 4 33.76 8.77 2.6550 -2 4 1 4 34.30 36.17 2.6142 -4 0 2 2 34.51 3.15 2.5991 3 1 1 4 35.21 16.12 2.5487 1 1 2 4 35.46 43.76 2.5312 -1 3 2 4 35.91 28.80 2.5009 4 2 0 4 37.37 5.00 2.4067 -4 2 2 4 39.13 3.94 2.3023 -1 5 1 4 39.52 3.07 2.2800 2 4 1 4 40.09 6.44 2.2492 2 0 2 2 40.41 1.83 2.2323 3 3 1 4 41.78 1.57 2.1621 1 5 1 4 41.92 18.95 2.1553 5 1 0 4 42.07 3.42 2.1478 -4 4 1 4 42.80 29.88 2.1126 -3 1 3 4 43.70 1.46 2.0715 -1 1 3 4 44.07 4.61 2.0547 0 6 0 2 44.27 2.02 2.0462 4 2 1 4 44.34 19.26 2.0428 3 5 0 4 45.86 16.43 1.9786 -5 3 2 4 46.56 3.02 1.9507 -6 0 2 2 46.79 3.33 1.9414 0 6 1 4 47.04 5.49 1.9320 5 3 0 4 47.25 9.83 1.9236 2 6 0 4 47.55 3.15 1.9123 -2 6 1 4 47.85 6.75 1.9011 -3 3 3 4 47.93 6.77 1.8978 -3 5 2 4 48.11 2.07 1.8914 -6 2 1 4 48.67 1.44 1.8710 -1 3 3 4 50.00 4.92 1.8242 6 0 0 2 50.48 10.04 1.8079 3 5 1 4 50.56 9.21 1.8053 5 1 1 4 50.73 1.38 1.7996 1 1 3 4 51.00 3.79 1.7907 1 5 2 4 51.61 2.33 1.7708 -2 4 3 4 52.05 18.18 1.7572 3 3 2 4 52.05 2.16 1.7569 2 6 1 4 52.64 6.57 1.7388 1 7 0 4 53.98 4.09 1.6986 -1 7 1 4 54.73 3.95 1.6770 -6 2 3 4 54.98 2.06 1.6702 -6 4 1 4 55.06 1.80 1.6679 5 3 1 4 55.16 1.84 1.6650 -5 5 2 4 55.21 6.40 1.6638 0 4 3 4 55.22 4.93 1.6634 1 3 3 4 55.77 17.34 1.6483 -6 4 2 4 55.97 1.04 1.6430 4 6 0 4 56.08 2.22 1.6399 1 7 1 4 56.19 2.80 1.6369 5 5 0 4 56.91 1.41 1.6180 -3 5 3 4 57.01 7.09 1.6154 -4 6 2 4 57.18 1.27 1.6111 -3 1 4 4 57.35 19.72 1.6065 -2 0 4 2 57.64 8.97 1.5993 -1 5 3 4 57.68 1.31 1.5983 2 2 3 4 58.78 1.97 1.5708 -7 3 2 4 58.83 2.88 1.5698 6 4 0 4 58.88 1.42 1.5685 -7 1 3 4 59.46 1.10 1.5546 -2 2 4 4 59.60 3.76 1.5511 7 1 0 4 59.78 1.72 1.5470 -5 1 4 4 60.67 1.53 1.5265 3 5 2 4 61.08 3.53 1.5170 -6 4 3 4 61.09 2.12 1.5170 2 6 2 4 61.17 5.45 1.5152 -3 7 2 4 61.49 5.67 1.5079 -5 5 3 4 61.98 12.39 1.4973 -8 0 2 2 62.25 6.76 1.4915 0 8 1 4 62.56 4.00 1.4848 4 4 2 4 62.67 1.08 1.4824 0 0 4 2 62.87 1.29 1.4781 -2 8 1 4 62.98 2.52 1.4758 -7 3 3 4 63.34 10.57 1.4683 3 7 1 4 63.68 14.17 1.4614 7 3 0 4 63.79 6.06 1.4590 1 7 2 4 63.84 2.34 1.4580 2 4 3 4 63.85 6.20 1.4579 -5 3 4 4 63.97 3.59 1.4553 -1 3 4 4 63.99 3.54 1.4550 -8 2 2 4 64.48 1.43 1.4450 -6 2 4 4 65.33 1.05 1.4284 -6 6 1 4 65.46 3.74 1.4258 -4 4 4 4 65.52 1.35 1.4246 -2 4 4 4 65.53 2.33 1.4244 0 6 3 4 66.81 3.04 1.4003 6 4 1 4 66.85 2.13 1.3995 -7 5 2 4 67.34 1.65 1.3905 -7 1 4 4 67.38 1.17 1.3897 -2 8 2 4 68.36 4.22 1.3722 5 7 0 4 68.47 5.65 1.3702 -4 8 1 4 69.01 1.27 1.3610 -3 7 3 4 69.66 6.35 1.3498 -1 7 3 4 69.84 2.59 1.3468 -8 4 2 4 70.49 4.65 1.3359 0 4 4 4 70.88 5.06 1.3294 6 0 2 2 70.97 1.11 1.3281 -8 4 1 4 71.00 1.03 1.3276 4 2 3 4 71.41 1.92 1.3209 1 3 4 4 71.60 1.65 1.3179 -5 5 4 4 72.29 1.01 1.3071 -8 0 4 2 72.58 5.08 1.3025 2 0 4 2 72.77 1.06 1.2996 6 2 2 4 72.80 2.53 1.2991 -8 4 3 4 73.17 8.50 1.2935 -5 7 3 4 74.45 2.37 1.2743 2 2 4 4 75.79 2.10 1.2552 -2 8 3 4 78.33 1.89 1.2207 6 4 2 4 78.36 1.41 1.2203 -7 7 1 4 78.61 2.30 1.2171 -7 5 4 4 78.74 1.01 1.2153 0 8 3 4 78.84 1.01 1.2141 1 5 4 4 79.18 1.44 1.2097 -9 1 4 4 79.39 2.59 1.2070 0 10 1 4 79.52 1.19 1.2053 3 1 4 4 79.66 1.11 1.2035 7 5 1 4 79.77 1.44 1.2022 0 6 4 4 80.41 3.05 1.1943 -3 7 4 4 82.81 4.78 1.1657 -9 3 4 4 85.07 1.35 1.1404 8 4 1 4 85.10 1.53 1.1400 4 8 2 4 85.10 3.37 1.1400 -4 10 1 4 86.25 2.86 1.1278 2 8 3 4 88.95 3.03 1.1004 6 8 1 4 89.44 1.28 1.0957 -7 7 4 4 89.56 1.16 1.0945 10 0 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.