Sincosite Kang H Y, Lee W C, Wang S L Inorganic Chemistry 31 (1992) 4743-4748 Hydrothermal synthesis and structural characterization of four layered vanadyl(IV) phosphate hydrates A(VO)2(PO4)2*4H2O (A=Co,Ca,Sr,Pb) Locality: synthetic _database_code_amcsd 0012705 CELL PARAMETERS: 6.3484 6.3500 6.5970 106.810 94.090 90.020 SPACE GROUP: P1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 253.867 Density (g/cm3): 2.851 MAX. ABS. INTENSITY / VOLUME**2: 11.45841418 RIR: 1.309 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.99 9.05 6.3307 1 0 0 1 14.06 100.00 6.2975 0 0 1 1 14.58 12.81 6.0772 0 1 0 1 17.09 11.49 5.1890 0 -1 1 1 19.12 4.92 4.6412 -1 0 1 1 20.03 2.88 4.4330 -1 1 0 1 20.48 1.21 4.3368 1 1 0 1 20.62 24.65 4.3069 1 0 1 1 21.68 2.62 4.1000 -1 -1 1 1 23.10 13.43 3.8506 0 1 1 1 27.88 15.20 3.2004 0 -1 2 1 28.19 39.42 3.1654 2 0 0 1 28.34 28.22 3.1488 0 0 2 1 28.68 33.99 3.1126 0 -2 1 1 29.39 50.09 3.0386 0 2 0 1 30.65 35.52 2.9169 -2 0 1 1 30.76 9.77 2.9071 -1 0 2 1 32.17 6.00 2.7824 2 1 0 1 32.23 4.36 2.7775 1 -2 1 1 32.40 7.70 2.7632 -1 2 0 1 32.50 6.29 2.7551 -2 -1 1 1 32.60 25.41 2.7471 2 0 1 1 32.70 2.61 2.7390 1 0 2 1 32.98 1.04 2.7162 1 2 0 1 34.57 12.83 2.5945 0 -2 2 1 35.72 7.59 2.5138 0 1 2 1 36.36 3.65 2.4706 0 2 1 1 36.87 2.45 2.4375 -1 -2 2 1 37.85 3.61 2.3768 2 1 1 1 38.04 4.76 2.3655 1 -2 2 1 38.48 3.71 2.3392 -1 2 1 1 38.70 2.84 2.3265 -2 -1 2 1 38.81 4.22 2.3206 -2 0 2 1 40.35 8.65 2.2355 -2 -2 1 1 40.71 2.83 2.2165 -2 2 0 1 40.96 6.65 2.2036 2 -2 1 1 41.23 4.18 2.1897 0 -1 3 1 41.39 1.00 2.1815 2 -1 2 1 41.65 1.71 2.1684 2 2 0 1 41.95 1.01 2.1535 2 0 2 1 42.86 1.09 2.1102 3 0 0 1 43.09 11.44 2.0992 0 0 3 1 44.18 1.87 2.0500 -2 -2 2 1 44.24 6.38 2.0474 -3 0 1 1 44.44 3.54 2.0384 -1 0 3 1 44.73 1.74 2.0261 1 -1 3 1 44.74 5.26 2.0257 0 3 0 1 45.16 5.26 2.0077 -1 -3 1 1 45.17 5.71 2.0072 -3 1 0 1 45.22 5.63 2.0052 1 -3 1 1 45.50 5.79 1.9937 -2 2 1 1 45.69 5.15 1.9856 0 -3 2 1 45.83 7.89 1.9800 3 1 0 1 46.39 2.16 1.9574 3 0 1 1 46.59 6.70 1.9495 1 0 3 1 46.78 2.65 1.9418 -1 3 0 1 47.72 2.77 1.9059 2 1 2 1 47.75 5.20 1.9045 2 2 1 1 47.99 3.21 1.8959 1 -2 3 1 48.39 1.84 1.8810 1 -3 2 1 48.60 3.32 1.8733 -1 2 2 1 48.89 4.86 1.8628 -2 -1 3 1 49.91 1.51 1.8273 0 1 3 1 50.22 3.39 1.8168 -3 0 2 1 50.23 1.00 1.8162 -3 -1 2 1 51.22 4.73 1.7835 0 3 1 1 52.25 3.73 1.7508 -2 -2 3 1 52.45 1.74 1.7447 2 -1 3 1 52.94 2.99 1.7297 0 -3 3 1 53.15 2.05 1.7231 1 1 3 1 54.09 6.07 1.6954 3 0 2 1 54.27 2.08 1.6902 -2 2 2 1 54.30 1.69 1.6895 2 3 0 1 55.27 3.47 1.6620 2 -2 3 1 55.68 1.12 1.6507 1 -3 3 1 55.92 1.88 1.6442 0 -1 4 1 55.96 1.40 1.6433 -3 2 1 1 56.30 1.69 1.6340 -2 1 3 1 56.83 2.40 1.6200 -1 -1 4 1 57.46 1.11 1.6039 3 -2 2 1 58.19 6.22 1.5854 0 -4 1 1 58.30 7.20 1.5827 4 0 0 1 58.59 2.85 1.5755 -3 -1 3 1 59.12 4.29 1.5628 -4 0 1 1 59.39 4.35 1.5563 0 -4 2 1 59.78 2.34 1.5471 -3 0 3 1 59.83 1.79 1.5459 -2 -3 3 1 60.26 1.15 1.5357 2 1 3 1 60.98 2.45 1.5193 0 4 0 1 61.16 2.21 1.5154 0 3 2 1 61.46 1.71 1.5086 4 0 1 1 62.06 2.25 1.4956 -3 -3 1 1 62.20 2.14 1.4924 3 -3 1 1 62.24 2.51 1.4915 -1 3 2 1 63.31 1.61 1.4690 3 -1 3 1 63.40 1.30 1.4671 1 2 3 1 63.45 3.20 1.4660 0 -3 4 1 63.82 1.04 1.4584 -4 0 2 1 63.91 1.85 1.4566 1 3 2 1 64.44 1.04 1.4459 0 -4 3 1 64.47 1.58 1.4453 -1 -3 4 1 65.09 2.65 1.4331 -3 1 3 1 65.77 2.20 1.4199 2 -4 1 1 65.81 1.68 1.4190 -4 -2 1 1 65.95 3.36 1.4165 -4 2 0 1 66.01 3.00 1.4152 -2 -4 1 1 66.06 1.31 1.4143 -1 1 4 1 66.20 1.52 1.4117 1 -3 4 1 66.57 2.39 1.4046 -2 -4 2 1 66.68 1.60 1.4027 4 -2 1 1 68.94 1.04 1.3622 -4 2 1 1 69.96 1.16 1.3448 -3 -1 4 1 70.26 1.31 1.3398 2 3 2 1 70.55 2.68 1.3349 3 1 3 1 70.81 1.04 1.3306 -2 -4 3 1 71.09 1.21 1.3262 4 -2 2 1 72.72 1.34 1.3003 2 -4 3 1 73.02 1.14 1.2957 -1 -2 5 1 73.49 1.32 1.2886 -2 4 1 1 73.88 1.29 1.2827 -4 -2 3 1 74.56 1.53 1.2728 -1 3 3 1 74.97 1.14 1.2668 2 1 4 1 75.05 1.09 1.2657 1 -1 5 1 75.26 1.13 1.2626 -3 3 2 1 75.40 1.06 1.2607 -4 3 0 1 76.60 1.34 1.2438 -2 -1 5 1 76.62 1.25 1.2436 1 3 3 1 77.22 1.00 1.2354 -3 -3 4 1 79.43 1.47 1.2065 1 -3 5 1 79.83 1.72 1.2015 3 3 2 1 81.48 1.24 1.1813 2 -1 5 1 82.02 1.36 1.1748 3 -3 4 1 84.01 1.45 1.1520 -3 -1 5 1 84.77 1.26 1.1436 4 -3 3 1 85.69 1.28 1.1337 1 1 5 1 86.34 1.67 1.1268 -3 3 3 1 87.21 1.28 1.1178 -4 -4 1 1 88.92 1.05 1.1006 -3 -3 5 1 89.61 1.09 1.0940 -1 3 4 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.