Pb(VO)2(PO4)2*4(H2O) Kang H Y, Lee W C, Wang S L Inorganic Chemistry 31 (1992) 4743-4748 Hydrothermal synthesis and structural characterization of four layered vanadyl(IV) phosphate hydrates A(VO)2(PO4)2*4H2O (A=Co,Ca,Sr,Pb) Locality: synthetic _database_code_amcsd 0012707 CELL PARAMETERS: 9.0300 9.0210 12.8740 90.000 100.160 90.000 SPACE GROUP: Cc X-RAY WAVELENGTH: 1.541838 Cell Volume: 1032.266 Density (g/cm3): 3.867 MAX. ABS. INTENSITY / VOLUME**2: 30.40926574 RIR: 2.560 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.99 23.99 6.3314 1 1 0 2 14.83 100.00 5.9718 -1 1 1 2 16.42 68.20 5.3991 1 1 1 2 18.52 24.87 4.7896 -1 1 2 2 19.68 16.64 4.5105 0 2 0 2 19.98 26.86 4.4442 2 0 0 1 20.91 22.61 4.2493 0 2 1 2 21.05 3.35 4.2213 1 1 2 2 22.32 20.59 3.9837 -2 0 2 1 23.81 51.31 3.7373 -1 1 3 2 24.22 19.55 3.6745 0 2 2 2 26.45 12.93 3.3697 2 0 2 1 26.80 37.43 3.3262 1 1 3 2 28.17 36.38 3.1680 0 0 4 1 28.18 3.60 3.1663 -2 2 1 2 28.19 14.92 3.1657 2 2 0 2 28.96 9.00 3.0831 0 2 3 2 29.93 11.31 2.9859 -2 2 2 2 29.94 56.01 2.9844 2 2 1 2 31.38 20.22 2.8509 -3 1 1 2 31.41 20.61 2.8484 1 3 0 2 31.66 8.28 2.8261 -2 0 4 1 31.79 4.06 2.8149 3 1 0 2 31.81 4.21 2.8133 -1 3 1 2 32.57 3.34 2.7490 -3 1 2 2 32.61 3.61 2.7461 1 3 1 2 33.16 29.06 2.7014 -2 2 3 2 33.17 7.08 2.7006 1 1 4 2 33.19 8.72 2.6995 2 2 2 2 33.76 14.03 2.6553 3 1 1 2 33.76 15.75 2.6547 -1 3 2 2 34.60 7.54 2.5925 0 2 4 2 35.23 20.01 2.5477 -3 1 3 2 35.27 17.34 2.5447 1 3 2 2 36.49 8.86 2.4621 -1 1 5 2 37.06 6.34 2.4261 -1 3 3 2 37.06 6.07 2.4260 3 1 2 2 37.56 5.85 2.3948 -2 2 4 2 37.66 5.00 2.3882 2 0 4 1 39.08 4.86 2.3047 -3 1 4 2 39.13 5.77 2.3021 1 3 3 2 39.94 5.95 2.2571 1 1 5 2 40.58 8.89 2.2229 -4 0 2 1 40.60 2.46 2.2221 4 0 0 1 40.63 10.63 2.2204 0 4 1 2 40.84 3.93 2.2095 0 2 5 2 41.41 11.15 2.1803 -1 3 4 2 41.42 12.32 2.1799 3 1 3 2 42.53 1.50 2.1255 -3 3 1 2 42.55 1.03 2.1247 0 4 2 2 42.81 1.51 2.1122 -2 2 5 2 42.82 15.44 2.1120 0 0 6 1 42.85 4.06 2.1106 2 2 4 2 42.85 8.33 2.1105 3 3 0 2 43.43 4.47 2.0836 -1 1 6 2 43.46 7.53 2.0823 -3 3 2 2 43.88 6.61 2.0633 -3 1 5 2 43.93 7.32 2.0610 1 3 4 2 44.11 3.74 2.0531 -2 0 6 1 44.90 7.67 2.0188 -4 2 1 2 45.08 12.35 2.0113 -2 4 1 2 45.08 2.46 2.0111 2 4 0 2 45.49 5.29 1.9939 -4 2 2 2 45.50 6.10 1.9933 4 2 0 2 45.54 1.86 1.9919 -4 0 4 1 45.57 5.80 1.9906 -3 3 3 2 45.58 6.91 1.9901 4 0 2 1 45.60 7.73 1.9895 0 4 3 2 46.27 7.41 1.9622 2 4 1 2 46.60 1.48 1.9489 -1 3 5 2 46.62 1.15 1.9483 3 1 4 2 47.06 3.55 1.9309 3 3 2 2 47.24 3.42 1.9240 -4 2 3 2 47.27 3.62 1.9230 4 2 1 2 47.54 3.06 1.9127 0 2 6 2 48.56 7.44 1.8748 -2 4 3 2 48.73 2.56 1.8687 -2 2 6 2 48.75 3.53 1.8681 -3 3 4 2 48.77 2.96 1.8673 2 2 5 2 49.42 1.36 1.8442 -3 1 6 2 49.47 1.92 1.8424 1 3 5 2 50.06 3.76 1.8221 -4 2 4 2 50.10 4.20 1.8208 4 2 2 2 50.68 5.95 1.8014 -1 1 7 2 50.73 4.42 1.7997 3 3 3 2 51.05 2.19 1.7891 2 0 6 1 51.65 3.82 1.7697 -5 1 1 2 51.70 3.76 1.7681 1 5 0 2 51.89 5.69 1.7620 2 4 3 2 52.46 5.05 1.7444 -1 3 6 2 52.48 5.52 1.7438 3 1 5 2 53.24 3.76 1.7206 -5 1 3 2 53.30 3.24 1.7188 -1 5 2 2 53.82 2.42 1.7032 -4 2 5 2 53.87 2.10 1.7018 4 2 3 2 54.32 3.65 1.6888 5 1 1 2 54.36 4.18 1.6878 1 5 2 2 54.40 4.20 1.6866 -4 0 6 1 54.44 4.22 1.6855 1 1 7 2 54.46 4.48 1.6848 0 4 5 2 54.63 1.82 1.6800 0 2 7 2 55.19 1.09 1.6642 -2 2 7 2 55.23 1.94 1.6631 2 2 6 2 55.25 4.48 1.6627 3 3 4 2 55.56 2.35 1.6539 -3 1 7 2 55.62 2.75 1.6524 1 3 6 2 56.06 4.31 1.6404 -2 4 5 2 57.75 3.68 1.5965 -3 3 6 2 57.79 2.41 1.5955 -4 4 1 2 58.28 1.60 1.5831 -4 4 2 2 58.29 1.75 1.5830 -2 0 8 1 58.29 2.03 1.5829 4 4 0 2 58.42 2.57 1.5798 -4 2 6 2 58.48 2.17 1.5783 4 2 4 2 58.85 2.86 1.5692 -5 1 5 2 58.92 3.03 1.5675 -1 5 4 2 59.76 2.59 1.5475 -4 4 3 2 59.78 2.50 1.5469 4 4 1 2 60.00 2.23 1.5419 -5 3 2 2 60.04 2.46 1.5410 3 5 0 2 60.50 2.10 1.5303 5 3 0 2 60.52 2.57 1.5299 -3 5 2 2 60.87 2.09 1.5219 5 1 3 2 60.89 2.00 1.5214 1 5 4 2 61.06 4.01 1.5175 2 4 5 2 61.74 1.24 1.5024 -6 0 2 1 62.11 1.49 1.4945 0 2 8 2 62.15 1.22 1.4937 -2 2 8 2 62.17 1.86 1.4930 0 6 1 2 62.19 1.96 1.4927 2 2 7 2 62.72 1.53 1.4814 6 0 0 1 63.34 1.47 1.4682 -3 3 7 2 63.36 1.72 1.4680 -5 3 4 2 63.42 2.05 1.4667 3 5 2 2 63.60 1.39 1.4629 0 6 2 2 63.74 2.24 1.4600 -4 2 7 2 63.81 1.89 1.4586 4 2 5 2 64.81 1.98 1.4386 -3 5 4 2 64.81 1.59 1.4385 5 3 2 2 65.48 1.05 1.4254 -6 2 2 2 65.48 1.49 1.4254 -4 4 5 2 65.49 2.73 1.4253 -6 2 1 2 65.53 1.59 1.4246 4 4 3 2 65.54 2.97 1.4243 -2 6 1 2 65.54 1.07 1.4242 2 6 0 2 65.82 1.42 1.4188 -1 3 8 2 65.85 1.29 1.4183 3 1 7 2 66.15 1.64 1.4126 -1 1 9 2 66.20 1.92 1.4117 0 4 7 2 66.21 1.53 1.4116 4 0 6 1 66.43 1.15 1.4074 6 2 0 2 66.44 1.35 1.4071 3 3 6 2 66.70 3.33 1.4023 -2 4 7 2 67.86 1.33 1.3811 -5 1 7 2 68.23 1.05 1.3745 -6 2 4 2 69.45 2.53 1.3533 -3 1 9 2 69.51 1.99 1.3523 1 3 8 2 69.59 1.09 1.3510 -3 3 8 2 69.74 1.02 1.3484 -4 2 8 2 69.82 1.45 1.3471 4 2 6 2 70.27 1.10 1.3396 -5 3 6 2 70.29 1.20 1.3392 1 1 9 2 70.35 1.35 1.3383 3 5 4 2 70.66 1.65 1.3331 5 1 5 2 70.67 2.06 1.3329 1 5 6 2 70.94 1.45 1.3286 -6 2 5 2 71.03 1.79 1.3270 2 6 3 2 72.54 1.15 1.3031 -3 5 6 2 72.57 1.02 1.3026 5 3 4 2 73.06 1.17 1.2951 2 4 7 2 74.52 1.60 1.2733 -7 1 1 2 74.55 1.59 1.2728 -5 5 2 2 74.56 1.36 1.2728 6 2 3 2 74.56 1.34 1.2727 -2 6 5 2 74.57 1.02 1.2726 4 4 5 2 74.60 1.42 1.2722 -1 7 1 2 74.95 1.56 1.2672 -7 1 3 2 75.01 1.82 1.2663 5 5 0 2 75.04 1.53 1.2658 1 7 1 2 76.14 1.48 1.2503 -6 4 1 2 76.99 1.03 1.2385 -6 4 3 2 77.60 1.32 1.2303 -5 5 4 2 78.76 1.04 1.2151 6 4 1 2 78.94 1.20 1.2128 5 5 2 2 79.79 1.15 1.2019 -5 1 9 2 79.87 1.11 1.2009 -1 5 8 2 80.00 1.08 1.1993 -2 4 9 2 80.35 1.00 1.1950 -5 3 8 2 80.40 1.20 1.1944 0 4 9 2 80.45 1.20 1.1938 3 5 6 2 81.30 1.10 1.1834 -6 4 5 2 81.34 1.39 1.1829 -1 3 10 2 81.38 1.56 1.1825 3 1 9 2 82.45 1.02 1.1698 7 3 0 2 82.51 1.03 1.1691 3 7 1 2 83.39 1.10 1.1590 -3 5 8 2 84.03 1.29 1.1517 -5 5 6 2 84.07 1.17 1.1514 7 1 3 2 84.10 1.17 1.1510 -1 7 5 2 86.11 1.17 1.1293 -7 1 7 2 86.23 1.18 1.1280 5 5 4 2 86.24 1.12 1.1279 1 7 5 2 87.73 1.06 1.1125 2 4 9 2 87.96 1.31 1.1102 0 8 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.