LaCa2GeS4Cl3 Gitzendanner R, DiSalvo F Inorganic Chemistry 35 (1996) 2623-2626 Synthesis and structure of a new quinary sulfide halide: LaCa2GeS4Cl3 _cod_database_code 1005026 _database_code_amcsd 0012717 CELL PARAMETERS: 9.7311 9.7311 6.3366 90.000 90.000 120.000 SPACE GROUP: P6_3mc X-RAY WAVELENGTH: 1.541838 Cell Volume: 519.650 Density (g/cm3): 3.363 MAX. ABS. INTENSITY / VOLUME**2: 27.61929764 RIR: 2.674 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.50 15.34 8.4274 1 0 0 6 17.51 7.16 5.0646 1 0 1 6 18.23 2.62 4.8656 1 1 0 6 21.08 37.28 4.2137 2 0 0 6 25.38 100.00 3.5087 2 0 1 6 28.01 1.13 3.1853 2 1 0 12 28.17 13.68 3.1683 0 0 2 1 30.13 26.43 2.9656 1 0 2 6 31.43 38.50 2.8459 2 1 1 12 31.86 4.79 2.8091 3 0 0 6 33.76 11.48 2.6550 1 1 2 6 34.94 56.13 2.5681 3 0 1 6 35.45 43.67 2.5323 2 0 2 6 36.95 62.09 2.4328 2 2 0 6 38.52 1.27 2.3373 3 1 0 12 40.14 15.28 2.2463 2 1 2 12 41.16 2.77 2.1929 3 1 1 12 42.93 8.46 2.1068 4 0 0 6 43.03 7.82 2.1019 3 0 2 6 44.21 5.83 2.0488 1 0 3 6 45.36 23.58 1.9992 4 0 1 6 47.00 4.06 1.9334 3 2 0 12 47.10 18.48 1.9296 2 2 2 6 48.19 32.35 1.8882 2 0 3 6 48.39 3.33 1.8809 3 1 2 12 49.28 6.61 1.8492 3 2 1 12 49.57 2.36 1.8390 4 1 0 12 51.76 10.78 1.7661 4 1 1 12 51.94 6.00 1.7603 2 1 3 12 52.13 3.31 1.7544 4 0 2 6 54.34 6.75 1.6882 3 0 3 6 55.70 9.82 1.6504 3 2 2 12 56.50 6.09 1.6288 5 0 1 6 56.76 13.05 1.6219 3 3 0 6 57.90 3.11 1.5926 4 2 0 12 57.99 3.04 1.5905 4 1 2 12 58.24 1.94 1.5841 0 0 4 1 58.94 6.91 1.5671 3 1 3 12 59.88 12.72 1.5446 4 2 1 12 61.57 1.67 1.5063 1 1 4 6 62.24 9.32 1.4917 4 0 3 6 62.41 7.04 1.4880 5 0 2 6 62.65 1.09 1.4828 2 0 4 6 63.16 1.45 1.4722 5 1 1 12 65.44 7.44 1.4261 3 2 3 12 65.61 3.04 1.4230 4 2 2 12 65.85 3.50 1.4184 2 1 4 12 66.58 1.24 1.4046 6 0 0 6 67.54 1.89 1.3870 4 1 3 12 67.93 3.12 1.3799 3 0 4 6 68.41 1.83 1.3713 6 0 1 6 69.44 2.49 1.3535 4 3 1 12 71.00 3.32 1.3275 2 2 4 6 71.48 9.67 1.3199 5 2 1 12 71.63 1.05 1.3174 5 0 3 6 73.72 2.38 1.2852 6 1 0 12 73.79 2.91 1.2840 6 0 2 6 74.64 2.93 1.2716 4 2 3 12 74.79 6.06 1.2694 4 3 2 12 75.93 1.79 1.2532 1 0 5 6 76.77 2.25 1.2415 5 2 2 12 77.60 4.93 1.2303 5 1 3 12 77.97 4.66 1.2254 3 2 4 12 78.87 2.62 1.2136 2 0 5 6 80.68 1.32 1.1909 6 1 2 12 81.35 1.40 1.1828 7 0 1 6 81.79 5.31 1.1775 2 1 5 12 82.47 1.34 1.1696 6 0 3 6 83.80 2.58 1.1543 5 0 4 6 84.25 1.73 1.1493 6 2 1 12 85.36 2.79 1.1372 5 2 3 12 86.47 1.16 1.1254 5 3 2 12 86.47 1.03 1.1254 7 0 2 6 86.69 1.86 1.1231 4 2 4 12 87.36 1.30 1.1162 7 1 0 12 89.20 1.41 1.0979 6 1 3 12 89.57 1.38 1.0944 5 1 4 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.