Cs5 H6 O35 Re W9 Ortega F, Pope M, Evans H Inorganic Chemistry 36 (1997) 2166-2169 Tungstorhenate heteropolyanions.2.Synthesis and characterization of enneatungstorhenates (V), -(VI), and -(VII) _cod_database_code 1008825 _database_code_amcsd 0016694 CELL PARAMETERS: 10.1940 11.5030 9.6820 100.550 115.810 99.130 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 967.654 Density (g/cm3): 5.259 MAX. ABS. INTENSITY / VOLUME**2: 64.23822691 RIR: 3.977 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.12 100.00 10.8906 0 1 0 2 10.01 8.10 8.8379 1 0 0 2 10.53 95.27 8.4029 -1 0 1 2 10.58 11.58 8.3580 0 0 1 2 11.06 64.60 7.9969 -1 1 0 2 11.37 27.43 7.7820 0 -1 1 2 13.50 6.45 6.5610 -1 1 1 2 14.51 14.01 6.1049 1 1 0 2 15.08 3.98 5.8742 0 1 1 2 16.28 17.67 5.4453 0 2 0 2 16.98 1.94 5.2218 1 -1 1 2 17.65 4.82 5.0242 -2 0 1 2 17.76 4.03 4.9954 1 0 1 2 18.64 8.94 4.7591 -1 0 2 2 18.97 2.03 4.6771 -1 -1 2 2 19.16 16.13 4.6317 -1 -2 1 2 19.54 15.54 4.5432 -2 1 0 2 19.88 4.58 4.4660 1 -2 1 2 20.45 1.84 4.3434 -2 -1 1 2 20.49 5.25 4.3346 0 -1 2 2 21.15 5.51 4.2015 -2 0 2 2 21.26 10.38 4.1790 0 0 2 2 21.35 7.91 4.1622 1 2 0 2 21.67 5.63 4.1012 -1 1 2 2 21.83 10.25 4.0711 1 1 1 2 22.23 2.32 3.9985 -2 2 0 2 22.39 27.51 3.9709 -2 2 1 2 22.46 1.73 3.9588 -2 -1 2 2 22.52 3.05 3.9486 -1 -2 2 2 22.86 17.98 3.8910 0 -2 2 2 22.91 2.43 3.8821 -2 1 2 2 23.68 11.45 3.7573 2 1 0 2 23.79 2.92 3.7399 0 -3 1 2 23.86 10.44 3.7295 -1 3 0 2 24.89 4.99 3.5769 0 1 2 2 25.58 1.69 3.4828 2 -1 1 2 25.71 5.36 3.4656 -2 -2 1 2 26.19 6.31 3.4032 1 -1 2 2 26.41 13.46 3.3743 -2 -2 2 2 26.52 6.67 3.3606 -3 1 1 2 26.85 19.98 3.3209 -3 0 1 2 26.96 9.81 3.3070 2 0 1 2 26.99 2.18 3.3037 -1 2 2 2 27.04 26.46 3.2977 -1 3 1 2 27.18 2.87 3.2805 -2 2 2 2 27.28 19.48 3.2691 1 -2 2 2 27.60 12.55 3.2319 0 -3 2 2 27.63 18.60 3.2279 1 0 2 2 27.85 5.91 3.2032 1 2 1 2 27.95 13.34 3.1928 -1 -1 3 2 28.06 8.99 3.1804 -3 1 2 2 28.14 19.77 3.1714 -1 -3 2 2 28.31 11.24 3.1526 -2 3 1 2 28.55 27.95 3.1263 -2 0 3 2 28.62 1.39 3.1193 -1 0 3 2 28.69 19.24 3.1116 -3 2 1 2 29.00 16.42 3.0791 1 3 0 2 29.19 3.19 3.0590 -3 1 0 2 29.26 21.67 3.0525 2 2 0 2 29.48 3.39 3.0303 0 3 1 2 29.58 10.85 3.0197 -3 -1 1 2 29.67 5.45 3.0112 -1 -2 3 2 30.31 13.89 2.9484 2 -3 1 2 30.67 1.41 2.9153 1 -3 2 2 30.79 6.62 2.9042 0 -1 3 2 30.96 3.37 2.8888 -3 2 2 2 31.11 2.01 2.8745 -2 -2 3 2 31.30 12.42 2.8575 1 1 2 2 31.65 4.56 2.8266 0 -2 3 2 31.67 5.01 2.8249 -1 4 0 2 32.11 3.89 2.7873 -2 -3 2 2 32.33 5.40 2.7695 -2 -3 1 2 32.89 1.92 2.7228 -3 3 1 2 33.26 7.51 2.6938 -3 1 3 2 33.59 1.08 2.6683 3 1 0 2 33.61 7.35 2.6665 -1 3 2 2 33.62 1.13 2.6656 -3 3 0 2 34.15 2.84 2.6256 2 -1 2 2 34.20 3.82 2.6215 -3 -2 1 2 34.58 2.12 2.5940 0 -3 3 2 34.92 2.24 2.5696 1 3 1 2 34.93 4.57 2.5686 -1 -4 2 2 34.94 4.64 2.5682 -1 4 1 2 35.30 1.26 2.5427 -2 4 1 2 35.42 4.16 2.5345 -2 -3 3 2 35.46 2.60 2.5312 3 -2 1 2 35.74 8.22 2.5121 -4 0 2 2 35.88 6.84 2.5030 -4 1 1 2 35.92 2.48 2.4999 2 2 1 2 36.00 1.92 2.4947 2 3 0 2 36.46 1.54 2.4645 1 -1 3 2 36.52 2.09 2.4604 2 -3 2 2 36.77 3.60 2.4446 -4 0 1 2 37.08 1.65 2.4247 1 4 0 2 37.13 1.57 2.4215 0 3 2 2 37.21 2.56 2.4161 -2 -1 4 2 37.53 1.53 2.3963 0 4 1 2 37.81 4.18 2.3795 -2 0 4 2 38.24 6.97 2.3537 1 0 3 2 38.51 2.71 2.3379 -4 1 3 2 38.55 2.61 2.3354 -3 4 1 2 38.76 4.78 2.3233 -1 -4 3 2 39.14 8.26 2.3014 -3 0 4 2 39.27 1.05 2.2940 -1 0 4 2 39.37 1.87 2.2888 -4 1 0 2 39.45 4.58 2.2839 1 -5 1 2 39.87 1.01 2.2611 -1 5 0 2 39.98 5.42 2.2551 -2 4 2 2 40.39 12.55 2.2330 2 -4 2 2 40.90 10.62 2.2066 -3 1 4 2 41.02 1.19 2.2004 -1 4 2 2 41.09 3.91 2.1969 -2 -4 3 2 41.28 2.29 2.1870 -3 3 3 2 41.46 1.21 2.1781 0 5 0 2 41.50 22.19 2.1759 3 -4 1 2 41.51 2.29 2.1756 -2 -3 4 2 41.90 2.26 2.1563 2 -5 1 2 42.19 2.83 2.1419 -1 3 3 2 42.33 3.23 2.1353 -4 -2 3 2 42.46 1.68 2.1292 -1 -5 2 2 42.96 1.91 2.1054 -2 5 1 2 43.30 3.55 2.0895 0 0 4 2 43.41 1.68 2.0846 0 -3 4 2 43.48 8.83 2.0811 2 4 0 2 43.64 4.89 2.0740 -4 -1 4 2 44.02 3.77 2.0571 2 -1 3 2 44.14 4.31 2.0516 -4 1 4 2 44.15 2.75 2.0514 -4 4 1 2 44.17 6.11 2.0506 -2 2 4 2 44.45 1.33 2.0383 -5 1 2 2 44.52 9.67 2.0350 3 3 0 2 44.67 1.55 2.0284 -4 3 3 2 44.76 1.41 2.0245 2 -3 3 2 45.10 3.17 2.0102 4 -2 1 2 45.13 2.41 2.0090 -5 0 2 2 45.16 1.37 2.0079 -1 -5 3 2 45.17 2.39 2.0073 3 2 1 2 45.42 9.26 1.9968 4 -1 1 2 45.61 1.48 1.9890 2 -5 2 2 45.79 1.70 1.9814 -3 -4 3 2 45.84 6.35 1.9794 -4 -2 4 2 46.28 1.18 1.9618 -5 2 1 2 46.52 4.86 1.9521 -1 2 4 2 46.68 3.04 1.9460 3 -5 1 2 47.03 3.12 1.9324 -3 -4 1 2 47.21 1.22 1.9252 1 -5 3 2 47.44 1.14 1.9164 -5 -1 3 2 47.47 7.90 1.9152 1 -6 1 2 47.49 1.02 1.9145 -3 -1 5 2 47.71 1.05 1.9062 -2 -5 1 2 48.04 7.21 1.8940 -3 0 5 2 48.69 1.53 1.8700 0 -6 2 2 48.87 1.11 1.8637 3 1 2 2 49.49 1.26 1.8416 -4 -3 4 2 49.55 1.06 1.8396 -2 -3 5 2 49.60 2.63 1.8379 2 4 1 2 49.93 1.16 1.8264 -5 -1 1 2 50.18 2.46 1.8179 -5 3 3 2 50.40 3.41 1.8105 -1 -3 5 2 50.52 1.38 1.8065 1 -4 4 2 50.66 1.30 1.8018 4 1 1 2 51.48 5.10 1.7753 3 4 0 2 51.76 5.10 1.7661 -5 4 2 2 51.87 1.75 1.7627 2 -6 2 2 52.05 2.64 1.7570 -1 3 4 2 52.33 2.64 1.7483 -3 -5 2 2 52.55 1.02 1.7414 4 -2 2 2 52.56 1.66 1.7412 -5 -2 4 2 53.18 1.18 1.7224 4 -3 2 2 53.30 1.93 1.7187 0 4 3 2 53.45 4.45 1.7143 0 -3 5 2 53.63 4.19 1.7088 3 2 2 2 53.68 1.20 1.7074 -5 4 0 2 54.00 3.77 1.6980 -5 -2 1 2 54.27 1.42 1.6903 -6 1 2 2 54.38 1.24 1.6872 2 2 3 2 54.47 4.13 1.6847 -5 4 3 2 54.48 1.49 1.6842 -2 -6 2 2 54.57 1.06 1.6817 3 -4 3 2 54.71 3.74 1.6778 0 6 1 2 54.79 1.97 1.6755 2 -1 4 2 54.96 2.92 1.6706 -5 -3 3 2 55.47 1.36 1.6565 5 -2 1 2 55.57 2.21 1.6537 -5 1 5 2 55.77 3.63 1.6482 0 -4 5 2 56.12 1.76 1.6388 -3 6 2 2 56.55 1.13 1.6275 -1 -6 4 2 56.73 1.55 1.6228 0 3 4 2 56.86 1.30 1.6192 -5 -2 5 2 56.99 1.19 1.6159 0 -6 4 2 57.06 1.93 1.6141 0 -7 1 2 57.17 2.70 1.6112 -3 -1 6 2 57.43 1.26 1.6045 1 2 4 2 57.55 1.77 1.6015 -3 -2 6 2 58.01 1.02 1.5898 1 -2 5 2 58.13 1.82 1.5869 1 5 2 2 58.30 1.70 1.5828 5 0 1 2 58.95 2.21 1.5666 -4 -5 3 2 59.09 1.98 1.5633 -1 -7 2 2 59.48 2.04 1.5541 2 -5 4 2 59.58 1.45 1.5517 -2 3 5 2 59.76 1.54 1.5473 -3 -5 5 2 59.91 1.74 1.5439 -3 -6 3 2 60.21 1.30 1.5369 2 3 3 2 60.73 1.78 1.5249 -6 -2 4 2 60.74 1.19 1.5248 -6 0 5 2 60.80 1.40 1.5234 -1 -3 6 2 60.99 2.68 1.5192 -6 -1 1 2 61.17 1.90 1.5152 0 6 2 2 61.29 2.07 1.5125 -5 -4 4 2 61.41 1.39 1.5099 -6 -2 2 2 61.52 1.45 1.5074 -4 -3 6 2 62.31 3.82 1.4900 -1 0 6 2 62.35 1.12 1.4892 -2 6 3 2 63.02 2.36 1.4749 4 -4 3 2 63.15 2.07 1.4724 -4 7 0 2 63.16 3.55 1.4721 -6 4 0 2 63.17 1.09 1.4718 2 -7 3 2 63.33 2.92 1.4685 0 4 4 2 63.46 2.12 1.4659 3 2 3 2 63.63 1.30 1.4623 0 -7 4 2 63.65 1.50 1.4619 -6 5 2 2 63.86 1.12 1.4576 2 -6 4 2 63.89 1.54 1.4570 0 7 1 2 64.09 4.73 1.4530 -4 4 5 2 64.18 1.35 1.4512 5 -1 2 2 64.33 1.45 1.4481 -7 2 3 2 64.52 1.50 1.4444 -6 4 4 2 64.63 3.13 1.4421 -6 -3 4 2 64.83 1.55 1.4381 -7 2 2 2 64.95 1.48 1.4359 1 -8 1 2 65.43 1.03 1.4264 -5 -4 1 2 65.54 1.04 1.4243 -6 5 3 2 65.55 1.23 1.4241 1 -7 4 2 65.85 2.56 1.4183 0 -8 2 2 65.88 1.64 1.4178 -1 5 4 2 65.96 1.32 1.4163 -7 3 3 2 66.01 1.01 1.4152 -5 2 6 2 66.11 1.28 1.4133 0 -4 6 2 66.24 1.68 1.4108 -5 6 3 2 66.35 1.00 1.4088 -4 -6 3 2 66.37 1.01 1.4085 0 -8 1 2 66.58 2.13 1.4046 5 0 2 2 67.66 1.78 1.3847 6 -1 1 2 68.41 1.22 1.3713 -7 0 5 2 68.44 2.12 1.3708 -7 1 5 2 68.92 1.53 1.3625 2 0 5 2 69.02 1.27 1.3607 -2 -2 7 2 70.00 1.23 1.3440 1 -2 6 2 70.28 1.36 1.3395 -2 -6 6 2 70.34 1.06 1.3383 -4 5 5 2 70.85 1.77 1.3300 -4 8 0 2 71.28 1.79 1.3230 -2 0 7 2 71.28 1.12 1.3230 1 -1 6 2 72.55 1.05 1.3030 1 -8 4 2 72.58 1.10 1.3025 2 1 5 2 72.71 2.75 1.3005 -3 -7 5 2 73.12 1.00 1.2942 -5 -3 7 2 74.08 1.06 1.2799 3 -4 5 2 75.21 1.07 1.2633 2 7 1 2 75.85 1.12 1.2544 1 7 2 2 75.93 1.38 1.2531 5 -7 2 2 75.97 1.63 1.2527 -8 0 3 2 76.54 1.04 1.2447 -8 1 2 2 77.50 1.19 1.2316 -7 -3 2 2 79.11 1.71 1.2106 -3 8 3 2 80.53 1.34 1.1927 -2 6 5 2 80.57 1.35 1.1923 0 3 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.