Sanidine Gualtieri A F Journal of Applied Crystallography 33 (2000) 267-278 Accuracy of XRPD QPA using the combined Rietveld-RIR method Locality: Latera, Viterbo, Italy _database_code_amcsd 0012862 CELL PARAMETERS: 8.5357 13.0313 7.1754 90.000 115.985 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 717.440 Density (g/cm3): 2.576 MAX. ABS. INTENSITY / VOLUME**2: 5.910699673 RIR: 0.747 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.39 5.77 6.6118 1 1 0 4 13.59 6.97 6.5156 0 2 0 2 13.73 2.09 6.4500 0 0 1 2 15.14 7.74 5.8515 -1 1 1 4 19.36 1.78 4.5839 0 2 1 4 21.13 59.87 4.2045 -2 0 1 2 22.60 19.25 3.9339 1 1 1 4 23.18 4.08 3.8364 2 0 0 2 23.54 79.22 3.7800 1 3 0 4 24.59 15.33 3.6199 -1 3 1 4 25.21 11.33 3.5328 -2 2 1 4 25.76 49.78 3.4584 -1 1 2 4 26.97 100.00 3.3059 2 2 0 4 27.23 58.42 3.2744 -2 0 2 2 27.38 28.60 3.2578 0 4 0 2 27.66 78.59 3.2250 0 0 2 2 29.87 57.04 2.9917 1 3 1 4 30.55 7.81 2.9258 -2 2 2 4 30.75 24.45 2.9079 0 4 1 4 30.94 10.79 2.8903 0 2 2 4 32.37 22.34 2.7658 -1 3 2 4 34.59 18.35 2.5935 -3 1 2 4 34.84 35.63 2.5752 -2 4 1 4 34.86 3.40 2.5739 2 2 1 4 35.27 9.72 2.5446 1 1 2 4 35.78 9.46 2.5097 3 1 0 4 36.17 3.89 2.4833 2 4 0 4 37.13 9.15 2.4215 -1 5 1 4 37.83 11.30 2.3783 -3 3 1 4 38.85 5.62 2.3181 -1 1 3 4 39.89 2.17 2.2600 -3 3 2 4 40.50 1.12 2.2272 -2 2 3 4 40.96 4.51 2.2035 1 5 1 4 41.58 23.75 2.1719 0 6 0 2 42.56 10.33 2.1242 2 4 1 4 42.90 3.30 2.1082 -4 0 1 2 43.03 4.78 2.1022 -4 0 2 2 43.88 2.11 2.0632 2 0 2 2 43.98 2.30 2.0588 3 1 1 4 43.99 5.00 2.0583 0 6 1 4 45.33 12.86 2.0007 -4 2 2 4 46.15 11.36 1.9669 2 2 2 4 46.56 2.79 1.9505 -3 3 3 4 47.32 2.69 1.9209 -3 5 1 4 47.39 10.32 1.9182 4 0 0 2 47.75 6.11 1.9047 -4 0 3 2 48.14 2.27 1.8900 2 6 0 4 48.43 1.77 1.8797 3 3 1 4 49.27 6.64 1.8495 1 1 3 4 49.54 2.36 1.8401 4 2 0 4 49.58 1.70 1.8388 1 5 2 4 49.88 1.33 1.8282 -4 2 3 4 49.96 3.19 1.8255 3 5 0 4 50.42 4.08 1.8099 -2 6 2 4 50.67 8.81 1.8015 0 6 2 4 50.89 8.90 1.7944 0 4 3 4 50.92 21.47 1.7935 -2 0 4 2 51.64 6.10 1.7700 -4 4 1 4 51.75 2.73 1.7664 -4 4 2 4 52.50 4.05 1.7430 2 4 2 4 53.38 1.48 1.7164 1 3 3 4 54.24 1.55 1.6912 -5 1 2 4 54.86 5.72 1.6735 -3 5 3 4 55.62 2.90 1.6523 -1 7 2 4 56.49 1.94 1.6289 0 8 0 2 56.52 6.67 1.6281 3 5 1 4 56.85 1.23 1.6195 -5 1 3 4 57.05 1.02 1.6143 -1 3 4 4 58.09 5.67 1.5879 -4 2 4 4 59.01 5.82 1.5653 0 2 4 4 59.48 1.43 1.5540 2 2 3 4 60.60 2.05 1.5280 0 6 3 4 60.61 7.58 1.5279 -5 3 3 4 61.28 7.16 1.5128 -4 6 1 4 61.88 20.50 1.4994 2 8 0 4 63.13 3.23 1.4728 -5 1 4 4 63.72 2.56 1.4606 -1 7 3 4 63.82 1.01 1.4584 -2 8 2 4 64.04 1.15 1.4540 0 8 2 4 64.39 2.98 1.4469 5 3 0 4 64.44 3.57 1.4459 1 1 4 4 64.85 1.93 1.4377 4 6 0 4 64.92 8.13 1.4363 2 4 3 4 65.14 2.02 1.4320 -4 6 3 4 65.39 2.11 1.4272 -5 5 2 4 65.62 1.84 1.4228 1 9 0 4 65.71 6.42 1.4211 -6 0 2 2 66.78 6.26 1.4009 4 0 2 2 67.44 2.69 1.3887 -4 0 5 2 67.74 2.05 1.3833 -5 5 3 4 67.76 3.09 1.3829 -2 6 4 4 67.95 1.42 1.3796 1 3 4 4 68.48 1.04 1.3702 -6 2 3 4 68.67 1.13 1.3668 -1 1 5 4 69.17 2.03 1.3582 -4 2 5 4 69.95 2.38 1.3449 -6 2 1 4 70.08 5.46 1.3427 -1 9 2 4 71.27 2.23 1.3232 -6 0 4 2 71.32 1.04 1.3224 5 5 0 4 72.08 5.00 1.3104 -1 3 5 4 72.34 1.78 1.3063 -2 4 5 4 72.53 1.46 1.3032 -5 1 5 4 72.54 1.39 1.3031 0 10 0 2 72.64 1.73 1.3016 5 3 1 4 72.85 1.57 1.2984 0 8 3 4 72.92 2.25 1.2973 2 0 4 2 73.09 1.34 1.2947 0 6 4 4 73.47 1.12 1.2890 -4 8 1 4 73.56 9.65 1.2876 -4 8 2 4 73.60 1.05 1.2869 4 4 2 4 74.15 2.17 1.2788 6 0 0 2 74.17 9.92 1.2785 2 8 2 4 74.24 2.31 1.2774 -4 4 5 4 74.73 1.86 1.2702 -3 9 2 4 75.00 2.57 1.2664 -6 4 1 4 75.07 1.08 1.2654 0 2 5 4 75.81 1.04 1.2549 6 2 0 4 75.84 3.06 1.2545 -3 5 5 4 75.87 3.07 1.2540 -5 3 5 4 78.65 1.20 1.2165 3 5 3 4 79.10 1.68 1.2108 -2 10 2 4 79.25 1.01 1.2087 5 5 1 4 79.29 1.14 1.2082 0 10 2 4 80.59 1.18 1.1920 -2 6 5 4 83.77 3.92 1.1547 -4 8 4 4 84.56 3.81 1.1460 0 8 4 4 84.93 1.01 1.1419 -2 10 3 4 86.83 2.96 1.1217 4 4 3 4 87.71 1.41 1.1127 -1 9 4 4 89.64 1.22 1.0937 6 4 1 4 89.79 1.64 1.0923 7 1 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.