data_global
_amcsd_formula_title 'F3 H2 N Na O4 Sb'
loop_
_publ_author_name
'Bourgault M'
'Ducourant B'
'Mascherpa Corral D'
'Fourcade R'
_journal_name_full 'Journal of Fluorine Chemistry'
_journal_volume 17 
_journal_year 1981
_journal_page_first 305
_journal_page_last 315
_publ_section_title
;
 Structure cristalline de Na Sb F3 (N O3) (H2 O). Etude de la
 liaison hydrogene O-H-X (X=Cl, Br, (N O3) )
 _cod_database_code 1008120
;
_database_code_amcsd 0016062
_chemical_formula_sum 'Sb Na F3 O4 N'
_cell_length_a 18.18
_cell_length_b 11.505
_cell_length_c 5.660
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 90
_cell_volume 1183.851
_exptl_crystal_density_diffrn      3.139
_symmetry_space_group_name_H-M 'P b c a'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  'x,1/2-y,1/2+z'
  '-x,1/2+y,1/2-z'
  '1/2-x,1/2+y,z'
  '1/2+x,1/2-y,-z'
  '1/2+x,y,1/2-z'
  '1/2-x,-y,1/2+z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Sb1   0.36646   0.60123   0.16200
Na1   0.48410   0.14330   0.81830
F1   0.44600   0.69310   0.02800
F2   0.40740   0.46990   0.99800
F3   0.43870   0.55190   0.40200
O1   0.08860   0.69990   0.14500
O2   0.22660   0.56980   0.86000
O3   0.32840   0.64840   0.75700
O4   0.23210   0.68530   0.55800
N1   0.26140   0.63370   0.72300
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Sb1 0.00850 0.01360 0.02640 -0.00050 -0.01030 0.00040
Na1 0.01380 0.02410 0.02450 -0.00440 0.00410 0.00230
F1 0.01090 0.02640 0.03070 -0.02130 0.01680 -0.00510
F2 0.01520 0.02140 0.04020 0.01540 0.00080 0.02590
F3 0.01670 0.02910 0.02840 -0.00590 -0.01830 -0.00160
O1 0.01230 0.02940 0.02730 0.00340 0.00410 0.00720
O2 0.02100 0.02780 0.03790 0.02950 -0.01690 0.00850
O3 0.00980 0.04140 0.03930 0.00840 -0.00770 -0.01340
O4 0.01780 0.04330 0.03220 0.00320 0.00590 -0.02460
N1 0.01500 0.01950 0.02890 0.00580 0.00870 -0.00380