Fe2 Na3 O12 P3 Fanjat N, Soubeyroux J Journal of Magnetism and Magnetic Materials 104 (1992) 933-934 Powder neutron diffraction study of Fe2Na3(P O4)3 in the low temperature phase _cod_database_code 1008509 _database_code_amcsd 0016402 CELL PARAMETERS: 15.0700 8.7400 8.7240 90.000 125.100 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 940.098 Density (g/cm3): 3.289 MAX. ABS. INTENSITY / VOLUME**2: 6.399428484 RIR: 0.634 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.41 17.93 7.1303 1 1 0 4 14.35 62.24 6.1744 -1 1 1 4 20.32 44.16 4.3700 0 2 0 2 20.32 52.91 4.3699 1 1 1 4 20.36 90.64 4.3620 -2 0 2 2 20.39 33.30 4.3552 -3 1 1 4 23.88 62.77 3.7269 0 2 1 4 23.93 41.88 3.7192 3 1 0 4 23.94 94.62 3.7164 -3 1 2 4 24.95 10.16 3.5688 0 0 2 2 24.98 14.31 3.5651 2 2 0 4 28.92 48.30 3.0872 -2 2 2 4 28.97 42.40 3.0824 4 0 0 2 31.56 4.27 2.8353 1 3 0 4 31.56 5.24 2.8348 2 2 1 4 31.63 10.58 2.8287 -4 2 1 4 31.68 41.60 2.8241 -5 1 2 4 32.39 54.58 2.7641 0 2 2 4 32.42 83.39 2.7615 3 1 1 4 32.45 100.00 2.7592 -3 1 3 4 35.58 11.92 2.5230 1 3 1 4 35.58 2.69 2.5230 2 0 2 2 35.62 86.32 2.5202 -3 3 1 4 35.64 4.95 2.5188 4 2 0 4 35.71 1.01 2.5143 -5 1 3 4 35.75 47.04 2.5117 -6 0 2 2 37.84 2.22 2.3774 -2 2 3 4 37.85 4.62 2.3768 3 3 0 4 37.87 3.46 2.3760 -3 3 2 4 41.32 5.24 2.1850 2 2 2 4 41.40 6.48 2.1810 -4 0 4 2 41.47 1.27 2.1776 -6 2 2 4 43.30 7.72 2.0895 1 3 2 4 43.31 3.31 2.0893 0 4 1 4 43.32 2.44 2.0887 3 1 2 4 43.32 2.53 2.0885 -2 4 1 4 43.35 9.46 2.0873 4 2 1 4 43.35 3.65 2.0872 -3 1 4 4 43.41 2.25 2.0846 -5 3 2 4 43.42 1.31 2.0840 -5 1 4 4 43.44 2.57 2.0833 -6 2 1 4 43.46 10.86 2.0823 -6 2 3 4 43.49 1.43 2.0807 -7 1 2 4 43.94 7.36 2.0605 1 1 3 4 43.97 3.30 2.0595 2 4 0 4 44.00 2.76 2.0581 -3 3 3 4 44.15 3.66 2.0513 -7 1 3 4 46.47 16.44 1.9542 -1 3 3 4 46.53 23.49 1.9517 5 1 1 4 46.54 9.63 1.9514 -4 2 4 4 46.57 6.42 1.9502 -5 3 3 4 46.63 2.56 1.9478 -7 1 1 4 48.28 1.07 1.8849 -1 1 4 4 48.36 4.51 1.8822 5 3 0 4 48.48 2.28 1.8778 -7 1 4 4 48.88 34.72 1.8635 0 4 2 4 48.90 6.95 1.8627 -2 2 4 4 48.94 17.17 1.8612 -4 4 2 4 48.98 11.54 1.8596 6 2 0 4 49.02 31.40 1.8582 -6 2 4 4 51.19 18.43 1.7844 0 0 4 2 52.90 5.78 1.7307 1 5 0 4 52.92 2.10 1.7303 -2 4 3 4 52.96 1.29 1.7289 -4 4 3 4 53.00 2.43 1.7278 -5 3 4 4 53.04 3.88 1.7266 7 1 0 4 53.12 2.36 1.7241 -8 2 3 4 53.45 5.29 1.7143 1 3 3 4 53.48 7.84 1.7133 4 2 2 4 53.56 23.35 1.7110 -5 1 5 4 53.66 1.72 1.7080 -8 2 2 4 55.65 8.55 1.6517 1 5 1 4 55.65 5.34 1.6517 2 4 2 4 55.68 26.64 1.6509 -3 5 1 4 55.70 5.19 1.6501 5 3 1 4 55.76 11.04 1.6485 -6 4 2 4 55.79 6.29 1.6478 -7 3 1 4 55.83 1.75 1.6467 -7 1 5 4 55.87 4.71 1.6456 -8 2 4 4 55.91 11.34 1.6445 -9 1 3 4 57.25 3.38 1.6093 0 4 3 4 57.27 1.71 1.6086 3 5 0 4 57.30 2.23 1.6080 5 1 2 4 57.33 1.03 1.6070 6 2 1 4 57.36 1.13 1.6064 -6 4 1 4 57.37 1.09 1.6060 -6 4 3 4 57.42 5.65 1.6047 -7 3 4 4 57.43 3.94 1.6045 -8 2 1 4 57.52 1.33 1.6022 -9 1 4 4 59.92 1.00 1.5436 -4 4 4 4 60.03 4.00 1.5412 8 0 0 2 61.48 1.03 1.5083 -5 5 2 4 61.62 1.75 1.5052 -8 2 5 4 61.90 6.78 1.4990 -1 1 5 4 61.92 13.20 1.4986 -2 4 4 4 61.92 2.38 1.4985 3 5 1 4 61.94 2.50 1.4982 -3 5 3 4 61.98 1.43 1.4973 -5 5 1 4 62.00 9.21 1.4969 6 4 0 4 62.00 1.70 1.4969 -5 3 5 4 62.01 7.63 1.4965 7 1 1 4 62.03 8.91 1.4962 -6 4 4 4 62.12 7.14 1.4941 -9 1 1 4 62.17 8.05 1.4930 -9 1 5 4 63.91 1.08 1.4567 0 6 0 2 63.91 1.86 1.4566 3 3 3 4 63.91 1.44 1.4566 -1 5 3 4 63.94 4.23 1.4560 -3 3 5 4 63.99 4.69 1.4550 -5 5 3 4 64.04 3.43 1.4540 -6 0 6 2 64.07 1.57 1.4534 8 2 0 4 64.15 7.64 1.4517 -9 3 3 4 64.19 8.41 1.4510 -10 0 2 2 65.38 1.67 1.4273 2 4 3 4 65.40 2.09 1.4270 -2 6 1 4 65.45 1.47 1.4261 5 5 0 4 65.56 1.33 1.4239 -7 1 6 4 65.61 1.48 1.4228 -9 3 2 4 65.64 3.87 1.4224 -9 3 4 4 65.86 11.86 1.4181 2 2 4 4 65.90 8.32 1.4174 4 4 2 4 65.94 1.12 1.4167 -4 0 6 2 67.83 1.35 1.3817 -2 6 2 4 67.88 1.30 1.3808 6 2 2 4 68.09 2.13 1.3771 -10 2 2 4 69.24 3.82 1.3569 0 2 5 4 69.25 1.46 1.3568 3 1 4 4 69.26 2.08 1.3566 2 6 1 4 69.29 3.09 1.3562 -3 1 6 4 69.33 2.15 1.3554 6 4 1 4 69.38 2.07 1.3546 -6 4 5 4 69.39 5.08 1.3544 -7 5 2 4 69.52 1.96 1.3522 -9 1 6 4 69.61 3.41 1.3507 -11 1 4 4 69.73 2.82 1.3487 -1 3 5 4 69.73 1.05 1.3486 0 6 2 4 69.76 7.32 1.3481 5 1 3 4 69.79 4.97 1.3476 -4 2 6 4 69.94 1.99 1.3450 -8 2 6 4 69.98 1.54 1.3443 -9 3 5 4 71.63 1.63 1.3174 -2 0 6 2 71.66 5.68 1.3170 4 6 0 4 71.74 7.82 1.3156 -7 5 1 4 73.07 4.42 1.2949 -4 6 3 4 73.27 1.35 1.2919 -10 2 1 4 73.34 2.63 1.2909 -11 1 2 4 75.34 1.70 1.2615 2 6 2 4 75.34 1.47 1.2615 4 0 4 2 75.35 1.53 1.2614 -2 2 6 4 75.44 7.97 1.2601 -6 6 2 4 75.49 2.50 1.2594 8 4 0 4 76.75 1.04 1.2418 4 6 1 4 76.81 1.15 1.2410 -6 6 1 4 76.83 1.65 1.2407 7 5 0 4 77.08 1.79 1.2373 -11 1 6 4 77.16 3.24 1.2362 2 4 4 4 77.20 1.67 1.2356 5 3 3 4 77.26 1.39 1.2349 -5 5 5 4 78.98 1.67 1.2123 1 3 5 4 80.36 2.02 1.1949 -1 7 2 4 80.79 4.94 1.1896 0 0 6 2 81.01 3.85 1.1869 -8 4 6 4 83.95 1.00 1.1527 -1 3 6 4 83.95 1.93 1.1526 1 7 2 4 83.97 1.44 1.1524 5 1 4 4 84.40 1.81 1.1476 -1 5 5 4 84.42 1.40 1.1475 3 7 1 4 84.44 1.97 1.1473 -3 7 3 4 84.52 4.97 1.1463 8 2 2 4 86.20 2.18 1.1283 -1 7 3 4 86.48 1.52 1.1253 -11 -3 1 4 87.69 2.40 1.1129 -7 5 6 4 87.80 2.42 1.1118 11 1 0 4 89.76 1.56 1.0925 0 8 0 2 89.77 1.70 1.0925 4 4 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.