As6 In4 K4 Birdwishtell T, Klein C, Jeffries T, Stevens E, O'Connor C Journal of Materials Chemistry 1 (1991) 555-558 Synthesis and crystal structures of the layered I-III-V Zintl phases, K4In4X6, where X=As, Sb _cod_database_code 1008525 _database_code_amcsd 0016418 CELL PARAMETERS: 14.3230 7.1060 15.7950 90.000 90.300 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1607.581 Density (g/cm3): 4.401 MAX. ABS. INTENSITY / VOLUME**2: 55.26670309 RIR: 4.089 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.20 100.00 7.8974 0 0 2 2 12.36 8.07 7.1614 2 0 0 2 12.77 15.50 6.9311 -1 0 2 2 12.83 17.90 6.9005 1 0 2 2 14.99 2.91 5.9089 -1 1 1 4 15.02 4.60 5.8994 1 1 1 4 17.58 3.78 5.0442 2 1 0 4 20.86 2.57 4.2582 -2 1 2 4 20.93 1.42 4.2439 2 1 2 4 21.70 1.03 4.0952 -3 0 2 2 21.80 2.09 4.0763 3 0 2 2 21.93 2.45 4.0524 1 1 3 4 22.52 1.95 3.9487 0 0 4 2 23.12 6.20 3.8477 -3 1 1 4 23.40 1.75 3.8016 1 0 4 2 24.48 5.37 3.6356 2 1 3 4 25.06 3.78 3.5530 0 2 0 2 25.10 1.59 3.5482 -3 1 2 4 25.19 3.75 3.5358 3 1 2 4 25.70 11.39 3.4664 0 2 1 4 25.71 1.47 3.4656 -2 0 4 2 25.82 1.67 3.4503 2 0 4 2 26.46 1.39 3.3682 1 2 1 4 26.54 2.26 3.3590 -1 1 4 4 26.59 1.07 3.3520 1 1 4 4 27.40 1.08 3.2547 4 0 2 2 27.53 37.47 3.2402 0 2 2 4 27.90 13.64 3.1977 4 1 0 4 28.03 9.72 3.1828 2 2 0 4 28.12 8.84 3.1728 -3 1 3 4 28.24 9.36 3.1596 3 1 3 4 28.45 6.34 3.1369 -4 1 1 4 28.51 2.22 3.1312 4 1 1 4 28.62 1.34 3.1187 2 2 1 4 28.66 16.14 3.1149 -2 1 4 4 28.76 7.78 3.1037 2 1 4 4 29.28 6.62 3.0507 -3 0 4 2 29.43 5.16 3.0350 3 0 4 2 30.10 13.25 2.9688 -4 1 2 4 30.20 18.12 2.9591 4 1 2 4 30.25 2.85 2.9545 -2 2 2 4 30.30 1.94 2.9497 2 2 2 4 30.35 2.48 2.9451 0 2 3 4 31.02 6.28 2.8831 1 2 3 4 31.59 7.94 2.8323 -1 1 5 4 31.65 5.51 2.8271 1 1 5 4 31.93 3.78 2.8033 -3 1 4 4 32.07 5.01 2.7911 3 1 4 4 32.70 2.11 2.7388 -4 1 3 4 32.84 9.73 2.7274 4 1 3 4 33.21 5.30 2.6974 -5 0 2 2 33.33 3.78 2.6884 5 0 2 2 33.41 1.87 2.6817 -2 1 5 4 33.70 3.87 2.6595 -4 0 4 2 33.88 1.70 2.6456 4 0 4 2 33.94 5.73 2.6412 0 2 4 4 34.06 2.19 2.6325 0 0 6 2 34.25 1.10 2.6179 5 1 1 4 34.51 3.35 2.5990 -1 2 4 4 34.55 1.72 2.5958 1 2 4 4 35.60 5.09 2.5218 -5 1 2 4 35.71 4.59 2.5144 5 1 2 4 36.06 1.17 2.4907 -4 1 4 4 36.21 3.13 2.4809 -2 2 4 4 36.23 2.48 2.4794 4 1 4 4 36.29 4.45 2.4754 -3 1 5 4 36.29 7.05 2.4752 2 2 4 4 36.42 6.49 2.4666 2 0 6 2 37.39 5.02 2.4051 -4 2 2 4 37.47 3.41 2.4000 4 2 2 4 37.86 1.31 2.3766 -5 1 3 4 38.52 11.12 2.3373 -2 1 6 4 38.64 7.89 2.3302 2 1 6 4 38.95 3.58 2.3120 -1 3 1 4 38.96 1.53 2.3115 1 3 1 4 38.98 1.59 2.3104 -3 0 6 2 39.37 2.53 2.2883 -6 0 2 2 39.49 1.79 2.2817 6 0 2 2 39.84 4.21 2.2629 6 1 0 4 40.29 2.56 2.2384 6 1 1 4 40.85 5.90 2.2093 -5 1 4 4 41.04 5.05 2.1994 5 1 4 4 41.57 1.01 2.1725 6 1 2 4 41.74 3.91 2.1638 -2 3 2 4 42.06 1.06 2.1484 -5 2 2 4 42.52 3.92 2.1263 -4 0 6 2 42.54 3.36 2.1252 1 1 7 4 42.74 4.61 2.1157 4 0 6 2 43.21 1.29 2.0937 -1 2 6 4 43.75 2.11 2.0693 -2 3 3 4 44.02 1.30 2.0569 2 1 7 4 44.17 5.14 2.0504 -3 3 2 4 44.22 8.64 2.0480 3 3 2 4 44.23 2.45 2.0476 -6 0 4 2 44.45 1.99 2.0381 6 0 4 2 44.48 1.19 2.0370 -4 1 6 4 44.62 8.69 2.0309 -2 2 6 4 44.73 8.91 2.0262 2 2 6 4 45.10 1.98 2.0104 1 3 4 4 45.75 6.59 1.9832 -7 0 2 2 45.79 3.68 1.9814 6 2 0 4 45.87 5.45 1.9782 7 0 2 2 45.94 19.62 1.9755 4 3 0 4 46.08 1.98 1.9696 -3 3 3 4 46.33 2.99 1.9596 4 3 1 4 46.44 3.96 1.9555 -2 3 4 4 46.50 1.03 1.9528 2 3 4 4 46.51 1.08 1.9524 -7 1 1 4 46.70 3.86 1.9452 -5 2 4 4 46.87 3.70 1.9384 5 2 4 4 47.47 3.32 1.9152 4 3 2 4 47.85 1.63 1.9008 2 0 8 2 48.23 2.34 1.8870 -1 1 8 4 48.29 3.74 1.8845 1 1 8 4 48.47 2.12 1.8780 1 3 5 4 48.57 1.01 1.8745 -5 1 6 4 48.67 1.64 1.8709 -3 3 4 4 48.77 1.86 1.8673 3 3 4 4 49.52 3.86 1.8408 -2 1 8 4 49.65 2.49 1.8362 2 1 8 4 49.97 1.50 1.8253 -5 2 5 4 50.10 1.46 1.8206 -7 0 4 2 50.17 1.51 1.8183 5 2 5 4 50.33 2.68 1.8128 7 0 4 2 51.41 1.25 1.7772 5 3 2 4 51.44 3.08 1.7765 0 4 0 2 51.51 1.00 1.7741 -6 2 4 4 51.55 1.49 1.7730 -6 0 6 2 51.63 1.82 1.7702 -3 1 8 4 51.68 1.27 1.7688 -4 3 4 4 51.71 1.33 1.7679 6 2 4 4 52.37 2.02 1.7469 1 3 6 4 52.73 1.73 1.7361 8 1 0 4 52.82 2.76 1.7332 0 4 2 4 52.83 1.77 1.7328 -4 0 8 2 53.09 1.32 1.7251 4 0 8 2 53.23 1.78 1.7209 -1 4 2 4 53.55 4.20 1.7113 -2 3 6 4 54.02 2.48 1.6974 -8 1 2 4 54.15 2.82 1.6938 8 1 2 4 54.25 2.39 1.6908 1 1 9 4 54.52 2.77 1.6833 0 4 3 4 54.65 1.57 1.6795 -2 2 8 4 54.77 3.49 1.6760 2 2 8 4 55.66 1.03 1.6513 -8 1 3 4 56.81 1.48 1.6206 3 2 8 4 57.21 2.01 1.6102 -1 4 4 4 57.24 1.01 1.6094 1 4 4 4 58.42 1.24 1.5798 6 2 6 4 60.35 1.09 1.5338 -1 1 10 4 60.42 1.06 1.5322 1 1 10 4 62.73 1.52 1.4812 -5 2 8 4 63.01 3.43 1.4753 5 2 8 4 63.29 1.09 1.4694 -3 1 10 4 65.26 2.56 1.4296 -9 2 2 4 65.33 1.72 1.4283 8 3 0 4 65.39 1.98 1.4272 9 2 2 4 68.52 1.00 1.3694 -8 2 6 4 68.76 1.78 1.3652 -9 2 4 4 69.00 2.19 1.3610 9 2 4 4 69.02 1.71 1.3607 5 4 5 4 70.95 1.11 1.3284 10 2 0 4 71.33 1.44 1.3222 -7 2 8 4 71.71 2.21 1.3162 0 0 12 2 71.79 1.17 1.3149 -2 5 4 4 72.50 1.67 1.3038 -9 3 2 4 72.58 1.42 1.3024 4 5 2 4 73.30 1.20 1.2915 2 3 10 4 74.86 1.55 1.2684 -3 3 10 4 75.80 1.75 1.2549 -6 4 6 4 75.91 1.54 1.2535 -7 0 10 2 75.93 1.09 1.2532 8 3 6 4 76.04 1.27 1.2516 6 4 6 4 76.36 1.57 1.2471 7 0 10 2 77.52 1.12 1.2314 2 5 6 4 78.29 1.01 1.2212 6 5 0 4 78.68 1.07 1.2161 7 3 8 4 78.96 1.05 1.2125 -5 5 4 4 80.47 1.19 1.1936 12 0 0 2 81.41 1.30 1.1821 -7 2 10 4 81.50 1.98 1.1810 0 6 1 4 84.24 1.50 1.1494 1 5 8 4 88.06 1.00 1.1092 10 3 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.