In4 K4 Sb6 Birdwishtell T, Klein C, Jeffries T, Stevens E, O'Connor C Journal of Materials Chemistry 1 (1991) 555-558 Synthesis and crystal structures of the layered I-III-V Zintl phases, K4In4X6, where X=As, Sb _cod_database_code 1008526 _database_code_amcsd 0016419 CELL PARAMETERS: 15.2880 7.5440 16.7900 90.000 90.540 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1936.350 Density (g/cm3): 4.617 MAX. ABS. INTENSITY / VOLUME**2: 56.83927516 RIR: 4.008 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.54 100.00 8.3946 0 0 2 2 11.58 11.56 7.6437 2 0 0 2 11.98 14.58 7.3877 -1 0 2 2 12.08 15.69 7.3291 1 0 2 2 14.09 2.24 6.2839 -1 1 1 4 14.13 5.94 6.2658 1 1 1 4 16.51 4.64 5.3693 2 1 0 4 17.31 1.96 5.1240 -2 1 1 4 19.57 1.62 4.5369 -2 1 2 4 19.75 2.01 4.4947 0 1 3 4 20.30 3.86 4.3744 -3 0 2 2 20.47 6.27 4.3379 3 0 2 2 20.55 3.08 4.3210 -1 1 3 4 20.64 5.91 4.3034 1 1 3 4 21.17 8.69 4.1973 0 0 4 2 21.66 15.43 4.1027 -3 1 1 4 21.74 3.06 4.0876 3 1 1 4 21.91 1.04 4.0573 -1 0 4 2 23.03 10.06 3.8617 2 1 3 4 23.66 1.50 3.7606 3 1 2 4 24.09 1.07 3.6938 -2 0 4 2 24.18 13.94 3.6803 0 2 1 4 24.29 1.10 3.6646 2 0 4 2 24.87 2.40 3.5797 -1 2 1 4 24.90 3.47 3.5764 1 2 1 4 24.92 1.50 3.5733 -1 1 4 4 25.01 1.03 3.5600 1 1 4 4 25.52 1.65 3.4907 -4 0 2 2 25.70 3.24 3.4660 4 0 2 2 25.90 32.31 3.4406 0 2 2 4 26.14 9.25 3.4093 4 1 0 4 26.34 13.44 3.3835 -3 1 3 4 26.35 19.11 3.3826 2 2 0 4 26.54 10.75 3.3582 3 1 3 4 26.64 9.51 3.3466 -4 1 1 4 26.73 3.24 3.3356 4 1 1 4 26.87 1.17 3.3186 -2 2 1 4 26.87 11.05 3.3175 -2 1 4 4 26.91 1.38 3.3133 2 2 1 4 27.05 5.72 3.2963 2 1 4 4 27.40 9.23 3.2549 -3 0 4 2 27.66 7.55 3.2249 3 0 4 2 28.17 9.49 3.1680 -4 1 2 4 28.34 12.53 3.1495 4 1 2 4 28.41 6.43 3.1420 -2 2 2 4 28.49 5.11 3.1329 2 2 2 4 28.54 2.39 3.1279 0 2 3 4 29.11 2.35 3.0676 -1 2 3 4 29.17 6.20 3.0612 1 2 3 4 29.65 10.88 3.0127 -1 1 5 4 29.75 7.25 3.0028 1 1 5 4 29.90 2.68 2.9886 -3 1 4 4 30.14 4.01 2.9653 3 1 4 4 30.59 3.52 2.9225 -4 1 3 4 30.82 13.09 2.9008 4 1 3 4 31.03 7.65 2.8816 -5 0 2 2 31.23 5.56 2.8642 5 0 2 2 31.31 1.58 2.8566 -3 2 2 4 31.33 3.62 2.8555 -2 1 5 4 31.51 4.36 2.8392 -4 0 4 2 31.52 1.89 2.8385 2 1 5 4 31.81 2.04 2.8127 4 0 4 2 31.90 7.31 2.8056 0 2 4 4 31.98 3.80 2.7982 0 0 6 2 32.08 1.25 2.7901 5 1 1 4 32.41 1.74 2.7626 -1 2 4 4 33.28 2.97 2.6919 -5 1 2 4 33.47 3.79 2.6777 5 1 2 4 33.97 3.61 2.6391 -2 2 4 4 33.98 4.98 2.6383 -3 1 5 4 34.02 1.63 2.6355 4 1 4 4 34.11 8.88 2.6284 2 2 4 4 34.23 3.70 2.6197 2 0 6 2 35.02 3.80 2.5620 -4 2 2 4 35.16 3.12 2.5522 4 2 2 4 35.38 2.61 2.5370 -5 1 3 4 35.64 2.53 2.5192 5 1 3 4 36.10 10.66 2.4882 -2 1 6 4 36.30 7.00 2.4747 2 1 6 4 36.49 1.85 2.4626 -3 0 6 2 36.60 3.84 2.4552 -1 3 1 4 36.62 1.76 2.4541 1 3 1 4 36.77 2.45 2.4445 -6 0 2 2 36.97 2.65 2.4317 6 0 2 2 37.25 3.98 2.4139 6 1 0 4 37.60 1.25 2.3924 -6 1 1 4 37.70 3.73 2.3864 6 1 1 4 38.16 4.69 2.3581 -5 1 4 4 38.49 4.42 2.3391 5 1 4 4 38.72 1.12 2.3254 -6 1 2 4 39.18 4.26 2.2993 -2 3 2 4 39.35 1.26 2.2899 -5 2 2 4 39.51 1.11 2.2811 5 2 2 4 39.71 1.32 2.2696 -1 3 3 4 39.74 6.30 2.2680 -4 0 6 2 39.93 5.27 2.2576 1 1 7 4 40.12 8.18 2.2477 4 0 6 2 40.38 3.19 2.2337 3 3 1 4 41.04 3.85 2.1993 -2 3 3 4 41.28 3.01 2.1872 -6 0 4 2 41.33 2.28 2.1845 2 1 7 4 41.42 5.67 2.1801 -3 3 2 4 41.51 10.02 2.1756 3 3 2 4 41.52 2.13 2.1749 -5 1 5 4 41.58 1.37 2.1719 -4 1 6 4 41.64 2.24 2.1690 6 0 4 2 41.81 13.57 2.1605 -2 2 6 4 41.99 12.66 2.1517 2 2 6 4 42.34 2.46 2.1346 1 3 4 4 42.68 8.76 2.1184 -7 0 2 2 42.83 8.31 2.1113 6 2 0 4 42.89 7.58 2.1087 7 0 2 2 43.06 15.98 2.1007 4 3 0 4 43.19 3.38 2.0946 -3 3 3 4 43.32 2.80 2.0886 3 3 3 4 43.38 1.70 2.0858 -4 3 1 4 43.44 5.35 2.0831 4 3 1 4 43.47 2.08 2.0818 -1 0 8 2 43.54 4.84 2.0787 -2 3 4 4 43.65 6.55 2.0737 -5 2 4 4 43.94 6.84 2.0607 5 2 4 4 44.51 1.99 2.0354 4 3 2 4 44.90 1.55 2.0189 2 0 8 2 45.18 2.03 2.0068 -1 1 8 4 45.30 3.49 2.0021 1 1 8 4 45.49 4.22 1.9941 1 3 5 4 46.07 1.26 1.9704 6 2 3 4 46.07 1.81 1.9701 -4 3 3 4 46.11 1.05 1.9684 -6 1 5 4 46.31 1.10 1.9604 -2 2 7 4 46.35 2.47 1.9591 -2 1 8 4 46.57 1.16 1.9503 2 1 8 4 46.60 1.10 1.9492 -2 3 5 4 46.68 1.39 1.9458 -5 2 5 4 46.70 1.79 1.9449 -7 0 4 2 47.02 1.85 1.9324 5 2 5 4 47.09 2.56 1.9299 7 0 4 2 48.15 1.21 1.8897 5 3 2 4 48.25 4.28 1.8860 0 4 0 2 48.27 1.62 1.8852 -3 1 8 4 48.35 1.84 1.8825 -4 3 4 4 48.60 1.04 1.8735 3 1 8 4 49.11 1.79 1.8551 1 3 6 4 49.19 1.13 1.8524 8 1 0 4 49.34 2.11 1.8469 -4 0 8 2 49.54 2.00 1.8401 0 4 2 4 49.76 1.44 1.8323 4 0 8 2 50.14 1.74 1.8194 -2 3 6 4 50.35 1.87 1.8124 -8 1 2 4 50.55 2.04 1.8054 8 1 2 4 50.71 1.28 1.8003 -1 1 9 4 50.83 3.76 1.7964 1 1 9 4 51.11 3.65 1.7872 0 4 3 4 51.12 1.80 1.7866 -2 2 8 4 51.17 1.32 1.7851 -4 3 5 4 51.33 2.94 1.7800 2 2 8 4 51.58 1.07 1.7719 7 1 5 4 51.85 1.52 1.7634 -8 1 3 4 52.97 1.01 1.7286 -7 2 4 4 53.06 1.33 1.7258 -1 3 7 4 53.22 1.01 1.7211 3 2 8 4 53.88 1.18 1.7014 6 3 3 4 55.80 1.10 1.6476 9 1 1 4 56.10 1.02 1.6395 3 3 7 4 56.30 1.34 1.6341 1 4 5 4 57.00 1.44 1.6157 8 1 5 4 57.37 1.10 1.6061 2 4 5 4 58.47 2.34 1.5784 -5 2 8 4 58.94 4.84 1.5670 5 2 8 4 60.71 2.85 1.5254 -9 2 2 4 60.89 1.26 1.5215 8 3 0 4 60.92 2.96 1.5208 9 2 2 4 61.23 1.02 1.5138 -5 3 7 4 61.57 1.06 1.5061 7 0 8 2 62.76 1.06 1.4806 9 1 5 4 63.89 2.25 1.4571 -9 2 4 4 64.29 2.55 1.4490 9 2 4 4 64.46 1.27 1.4454 5 4 5 4 65.26 1.12 1.4297 -5 3 8 4 65.36 1.07 1.4277 -4 2 10 4 65.43 1.19 1.4263 -3 5 2 4 66.28 1.33 1.4101 -7 2 8 4 66.87 2.43 1.3991 0 0 12 2 67.37 1.80 1.3900 -9 3 2 4 67.73 1.14 1.3834 4 5 2 4 68.39 1.14 1.3717 2 3 10 4 69.68 1.16 1.3494 -3 3 10 4 70.41 1.70 1.3372 -7 0 10 2 70.48 1.09 1.3360 -6 4 6 4 70.70 1.08 1.3325 8 3 6 4 71.16 1.77 1.3250 7 0 10 2 73.26 1.25 1.2921 7 3 8 4 73.44 1.05 1.2893 -5 5 4 4 74.48 1.23 1.2739 12 0 0 2 75.88 2.59 1.2538 0 6 1 4 78.33 1.81 1.2206 1 5 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.