Minium Gavarri J R, Weigel D, Hewat A W Journal of Solid State Chemistry 23 (1978) 327-339 Oxydes de plomb. IV. Evolution structurale de l'oxyde Pb3O4 entre 240 et 5 K et mecanisme de la transition Locality: synthetic Sample: T = 240 K _database_code_amcsd 0013354 CELL PARAMETERS: 8.8189 8.8068 6.5636 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 509.770 Density (g/cm3): 8.932 MAX. ABS. INTENSITY / VOLUME**2: 212.8595598 RIR: 7.760 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.21 22.06 6.2316 1 1 0 4 20.14 1.36 4.4095 2 0 0 2 20.17 1.17 4.4034 0 2 0 2 24.32 2.70 3.6602 2 0 1 4 24.34 1.38 3.6567 0 2 1 4 26.37 100.00 3.3799 2 1 1 8 26.39 97.16 3.3779 1 2 1 8 27.17 10.00 3.2818 0 0 2 2 28.65 26.95 3.1158 2 2 0 4 30.79 73.41 2.9037 1 1 2 8 32.10 48.47 2.7884 3 1 0 4 32.14 48.73 2.7853 1 3 0 4 34.05 26.28 2.6327 2 0 2 4 34.07 27.07 2.6314 0 2 2 4 36.76 2.19 2.4449 3 2 0 4 36.78 1.30 2.4436 2 3 0 4 39.33 3.78 2.2911 3 2 1 8 39.34 3.68 2.2900 2 3 1 8 39.90 10.23 2.2596 2 2 2 8 40.93 1.45 2.2047 4 0 0 2 40.99 1.56 2.2017 0 4 0 2 43.57 2.07 2.0772 3 3 0 4 44.56 10.94 2.0335 4 1 1 8 44.61 11.09 2.0313 1 4 1 8 46.04 10.98 1.9714 4 2 0 4 46.08 10.89 1.9698 2 4 0 4 46.31 1.86 1.9606 3 2 2 8 46.32 1.11 1.9600 2 3 2 8 47.53 18.56 1.9131 2 1 3 8 47.54 19.58 1.9127 1 2 3 8 49.83 23.27 1.8301 4 0 2 4 49.88 23.42 1.8284 0 4 2 4 50.97 1.05 1.7918 4 1 2 8 52.11 52.17 1.7552 3 3 2 8 52.94 2.20 1.7294 5 1 0 4 53.02 2.11 1.7272 1 5 0 4 53.87 1.07 1.7020 3 4 1 8 54.28 1.37 1.6899 4 2 2 8 54.32 1.43 1.6889 2 4 2 8 56.04 12.96 1.6409 0 0 4 2 56.44 1.19 1.6304 3 2 3 8 56.45 1.19 1.6300 2 3 3 8 58.06 12.24 1.5886 5 2 1 8 58.12 13.13 1.5871 2 5 1 8 59.32 9.61 1.5579 4 4 0 4 60.51 5.57 1.5300 5 1 2 8 60.54 3.82 1.5294 4 1 3 8 60.58 5.64 1.5285 1 5 2 8 60.58 4.35 1.5284 1 4 3 8 61.32 2.12 1.5119 5 3 0 4 61.36 2.21 1.5109 3 5 0 4 63.10 1.17 1.4733 5 3 1 8 63.27 5.72 1.4698 6 0 0 2 63.37 6.12 1.4678 0 6 0 2 64.14 4.72 1.4519 2 2 4 8 65.99 1.85 1.4156 6 1 1 8 66.07 11.15 1.4142 3 1 4 8 66.08 1.86 1.4139 1 6 1 8 66.09 11.26 1.4138 1 3 4 8 68.31 1.49 1.3732 5 3 2 8 68.35 1.44 1.3724 3 5 2 8 69.81 3.44 1.3472 5 4 1 8 69.83 3.55 1.3468 4 5 1 8 72.04 6.21 1.3109 5 2 3 8 72.10 6.35 1.3100 2 5 3 8 73.85 3.96 1.2832 6 2 2 8 73.93 4.02 1.2820 2 6 2 8 75.36 4.42 1.2612 4 2 4 8 75.39 4.39 1.2608 2 4 4 8 76.42 1.40 1.2463 5 5 0 4 76.48 4.24 1.2455 2 1 5 8 76.49 3.94 1.2454 1 2 5 8 79.27 1.04 1.2085 6 1 3 8 79.36 1.03 1.2074 1 6 3 8 80.73 1.13 1.1904 5 1 4 8 80.79 1.09 1.1896 1 5 4 8 82.79 5.07 1.1658 7 1 2 8 82.85 2.09 1.1651 5 4 3 8 82.88 2.01 1.1649 4 5 3 8 82.91 5.28 1.1645 1 7 2 8 83.50 4.43 1.1577 7 3 0 4 83.60 4.58 1.1566 3 7 0 4 84.59 6.14 1.1456 6 4 2 8 84.64 6.47 1.1450 4 6 2 8 86.05 5.86 1.1298 4 4 4 8 87.11 1.34 1.1188 4 1 5 8 87.15 1.26 1.1184 1 4 5 8 87.79 1.41 1.1119 5 3 4 8 87.83 1.48 1.1115 3 5 4 8 89.52 3.96 1.0948 6 0 4 4 89.61 4.24 1.0940 0 6 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.