Minium Gavarri J R, Weigel D, Hewat A W Journal of Solid State Chemistry 23 (1978) 327-339 Oxydes de plomb. IV. Evolution structurale de l'oxyde Pb3O4 entre 240 et 5 K et mecanisme de la transition Locality: synthetic Sample: T = 200 K _database_code_amcsd 0013355 CELL PARAMETERS: 8.8179 8.8032 6.5620 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 509.380 Density (g/cm3): 8.939 MAX. ABS. INTENSITY / VOLUME**2: 212.7743734 RIR: 7.751 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.22 22.16 6.2300 1 1 0 4 20.14 1.30 4.4089 2 0 0 2 20.17 1.17 4.4016 0 2 0 2 24.32 2.62 3.6596 2 0 1 4 24.35 1.40 3.6554 0 2 1 4 26.37 100.00 3.3793 2 1 1 8 26.39 98.08 3.3768 1 2 1 8 27.18 10.04 3.2810 0 0 2 2 28.66 27.16 3.1150 2 2 0 4 30.80 73.72 2.9030 1 1 2 8 32.10 48.83 2.7880 3 1 0 4 32.15 48.88 2.7843 1 3 0 4 34.06 26.74 2.6321 2 0 2 4 34.08 27.10 2.6306 0 2 2 4 36.77 2.02 2.4444 3 2 0 4 36.79 1.41 2.4428 2 3 0 4 39.33 3.73 2.2906 3 2 1 8 39.36 3.69 2.2893 2 3 1 8 39.91 10.27 2.2590 2 2 2 8 40.94 1.48 2.2045 4 0 0 2 41.01 1.54 2.2008 0 4 0 2 43.58 2.10 2.0767 3 3 0 4 44.56 11.19 2.0332 4 1 1 8 44.63 11.24 2.0305 1 4 1 8 46.05 11.11 1.9711 4 2 0 4 46.10 11.02 1.9691 2 4 0 4 46.32 1.75 1.9602 3 2 2 8 46.34 1.18 1.9594 2 3 2 8 47.54 18.88 1.9126 2 1 3 8 47.55 19.66 1.9122 1 2 3 8 49.83 23.47 1.8298 4 0 2 4 49.90 23.67 1.8277 0 4 2 4 52.12 52.91 1.7547 3 3 2 8 52.95 2.19 1.7292 5 1 0 4 53.04 2.15 1.7266 1 5 0 4 53.89 1.06 1.7014 3 4 1 8 54.29 1.40 1.6896 4 2 2 8 54.34 1.41 1.6884 2 4 2 8 56.06 13.14 1.6405 0 0 4 2 56.45 1.19 1.6300 3 2 3 8 56.47 1.20 1.6295 2 3 3 8 58.07 12.59 1.5884 5 2 1 8 58.14 13.19 1.5866 2 5 1 8 59.34 9.74 1.5575 4 4 0 4 60.52 5.70 1.5298 5 1 2 8 60.55 4.00 1.5291 4 1 3 8 60.60 4.37 1.5279 1 4 3 8 60.60 5.73 1.5279 1 5 2 8 61.33 2.21 1.5116 5 3 0 4 61.38 2.24 1.5104 3 5 0 4 63.12 1.05 1.4730 5 3 1 8 63.28 5.93 1.4696 6 0 0 2 63.40 6.18 1.4672 0 6 0 2 64.16 4.81 1.4515 2 2 4 8 66.00 1.86 1.4155 6 1 1 8 66.08 11.35 1.4139 3 1 4 8 66.11 11.40 1.4134 1 3 4 8 66.11 1.89 1.4133 1 6 1 8 68.32 1.48 1.3729 5 3 2 8 68.37 1.44 1.3720 3 5 2 8 69.83 3.56 1.3469 5 4 1 8 69.86 3.64 1.3465 4 5 1 8 72.06 6.38 1.3106 5 2 3 8 72.12 6.46 1.3096 2 5 3 8 73.86 4.07 1.2830 6 2 2 8 73.96 4.13 1.2816 2 6 2 8 75.38 4.52 1.2609 4 2 4 8 75.42 4.49 1.2604 2 4 4 8 76.44 1.43 1.2460 5 5 0 4 76.50 4.29 1.2452 2 1 5 8 76.51 4.07 1.2451 1 2 5 8 79.29 1.05 1.2083 6 1 3 8 79.39 1.05 1.2070 1 6 3 8 80.75 1.14 1.1901 5 1 4 8 80.82 1.12 1.1893 1 5 4 8 82.81 5.23 1.1656 7 1 2 8 82.88 2.16 1.1648 5 4 3 8 82.90 2.10 1.1645 4 5 3 8 82.95 5.38 1.1640 1 7 2 8 83.52 4.56 1.1575 7 3 0 4 83.64 4.71 1.1562 3 7 0 4 84.61 6.40 1.1453 6 4 2 8 84.67 6.59 1.1447 4 6 2 8 86.08 6.01 1.1295 4 4 4 8 87.14 1.38 1.1185 4 1 5 8 87.18 1.32 1.1181 1 4 5 8 87.82 1.48 1.1116 5 3 4 8 87.86 1.51 1.1112 3 5 4 8 89.54 4.15 1.0946 6 0 4 4 89.65 4.34 1.0936 0 6 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.